#------------------------------------------------------------------------------
#$Date: 2010-01-30 13:59:17 +0000 (Sat, 30 Jan 2010) $
#$Revision: 966 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000752.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2000752
loop_
_publ_author_name
'Chen, C.'
'Xu, D.'
'Xu, Y.'
'Cheng, C.'
'Ling, R.'
_publ_section_title
;
 Structure of
 <i>catena</i>-poly[{(2,2'-bipyridyl)(diperchlorato)copper(II)}-\m-4,4'-bipyridyl]
;
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1231
_journal_page_last               1233
_journal_volume                  48
_journal_year                    1992
_chemical_formula_sum            'C20 H16 Cl2 Cu N4 O8'
_[local]_cod_chemical_formula_sum_orig 'C20 H16 Cl2 Cu1 N4 O8'
_chemical_formula_weight         574.5
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_H-M   'P b c n'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   12.413(3)
_cell_length_b                   14.645(3)
_cell_length_c                   12.287(2)
_cell_volume                     2233.6(8)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    1.312
_exptl_crystal_density_diffrn    1.708
_exptl_crystal_F_000             1164
_[local]_cod_data_source_file    as0546.cif
_[local]_cod_data_source_block   as0546a
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
Cu .0 .19151(5) .25
Cl .29770(10) .18700(10) .19910(10)
O(1) .1883(4) .1834(5) .1749(5)
O(2) .3391(7) .1000(4) .1954(6)
O(3) .3466(7) .2431(5) .1281(7)
O(4) .3000(5) .2209(4) .3094(5)
N(1) .0524(3) .0892(3) .3428(3)
N(2) .0279(4) .2910(3) .3600(3)
C(1) .0358(4) .0058(3) .3018(4)
C(2) .0801(5) -.0729(4) .3443(5)
C(3) .1428(5) -.0638(4) .4352(6)
C(4) .1589(5) .0203(4) .4815(5)
C(5) .1125(5) .0962(4) .4324(4)
C(6) .0890(5) .3633(4) .3333(5)
C(7) .0798(4) .4464(3) .3865(5)
C(8) .0072(5) .4556(3) .4723(4)
C(9) -.0496(5) .3782(3) .5035(5)
C(10) -.0372(5) .2987(3) .4449(4)
H(2) .0688 -.1346 .3240
H(3) .1773 -.1191 .4696
H(4) .2028 .0262 .5509
H(5) .1259 .1594 .4658
H(6) .1436 .3568 .2708
H(7) .1259 .5002 .3641
H(9) -.1000 .3803 .5689
H(10) -.0811 .2435 .4681
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
Cu O(1) 2.516(7)
Cu N(2) 2.017(4)
N(1) C(5) 1.334(7)
N(2) C(10) 1.324(7)
C(1) C(2) 1.379(8)
C(3) C(4) 1.371(9)
C(6) C(7) 1.386(8)
C(9) C(10) 1.376(9)
Cl O(2) 1.375(8)
Cl O(4) 1.444(6)
Cu N(1) 1.992(4)
N(1) C(1) 1.337(7)
N(2) C(6) 1.343(7)
C(2) C(3) 1.368(9)
C(4) C(5) 1.390(9)
C(7) C(8) 1.393(8)
C(8) C(9) 1.389(8)
Cl O(1) 1.390(8)
Cl O(3) 1.344(9)
_cod_database_code 2000752