data_2000753
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1234
_journal_page_last  1237
loop_
_publ_author_name
 'Suwinska, K.'
_chemical_formula_moiety  'C16 H36 N2 O4,2(F6 P1)'
_chemical_formula_sum  'C16 H36 F12 N2 O4 P2'
_chemical_formula_weight  610.4
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_cell_length_a  6.7000(10)
_cell_length_b  20.911(9)
_cell_length_c  9.609(2)
_cell_angle_alpha  90.
_cell_angle_beta  104.24(2)
_cell_angle_gamma  90.
_cell_volume  1305.0(10)
_cell_formula_units_Z  2
_exptl_crystal_density_diffrn  1.553
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  632
_exptl_absorpt_coefficient_mu  2.5843
_diffrn_radiation_type  Cu
_diffrn_radiation_wavelength  1.54178
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 N(1) .0729(3) .14170(10)
         .1093(2)
 C(2) .1690(4) .07940(10)
         .1751(3)
 C(3) .0617(4) .04450(10)
         .2716(3)
 O(4) -.1183(3) .01510(10)
       .1896(2)
 C(5) -.2171(5) -.0240(2) .2745(3)
 C(6) -.4046(4) -.0524(2) .1787(3)
 O(7) -.3657(3) -.08756(9) .0606(2)
 C(8) -.2562(5) -.1448(2) .0962(3)
 C(9) -.2199(4) -.17580(10)
        -.0361(3)
 C(10) -.1294(4) .1298(2) .0052(4)
 C(11) .0395(5) .1855(2) .2255(4)
 P .34900(10)
      -.16176(4) .48171(8)
 F(1) .5776(3) -.14380(10)
       .4876(2)
 F(2) .1201(3) -.18120(10)
       .4767(2)
 F(3) .4050(9) -.1544(4) .6454(6)
 F(4) .4446(10) -.2159(3) .5891(8)
 F(5) .4361(11) -.2269(4) .5334(10)
 F(6) .3664(13) -.2312(3) .5239(11)
 F(7) .3680(9) -.2137(4) .3624(8)
 F(8) .3249(8) -.1891(3) .3318(5)
 F(9) .2883(9) -.1641(4) .3125(6)
 F(10) .2665(8) -.1094(3) .3712(7)
 F(11) .2457(15) -.0924(4) .4548(12)
 F(12) .3189(11) -.0922(3) .4333(9)
 F(13) .3414(11) -.1132(3) .6047(9)
 F(14) .3620(7) -.1351(3) .6414(6)
 H(2a) .307(3) .0890(10)
        .224(2)
 H(2b) .178(3) .0550(10)
        .101(2)
 H(3a) .033(3) .0690(10)
        .346(3)
 H(3b) .164(4) .0140(10)
        .333(3)
 H(5a) -.248(4) .0010(10)
         .353(3)
 H(5b) -.125(4) -.0610(10)
       .328(3)
 H(6a) -.503(4) -.0170(10)
       .139(3)
 H(6b) -.470(4) -.0810(10)
       .238(3)
 H(8a) -.335(4) -.1780(10)
       .137(3)
 H(8b) -.132(4) -.1380(10)
       .165(3)
 H(9a) -.346(4) -.1820(10)
       -.108(3)
 H(9b) -.169(4) -.2150(10)
       -.023(3)
 H(10a) -.108(4) .0980(10)
       -.064(3)
 H(10b) -.237(4) .1170(10)
       .052(3)
 H(10c) -.177(4) .1680(10)
       -.040(3)
 H(11a) .164(5) .193(2) .286(4)
 H(11b) .005(5) .227(2) .181(3)
 H(11c) -.078(4) .1700(10)
       .250(3)