data_2000803
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1361
_journal_page_last  1362
_publ_section_title
; ?
;
loop_
_publ_author_name
 'Jones, P.G.'
 'Bembenek, E.'
_chemical_formula_sum  'Ag2 C4 N4 S4 Zn1'
_chemical_formula_weight  513.4
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'C 1 2/c 1'
_symmetry_space_group_name_Hall  '-C 2yc'
_cell_length_a  19.720(9)
_cell_length_b  7.703(3)
_cell_length_c  7.753(3)
_cell_angle_alpha  90.
_cell_angle_beta  96.57(4)
_cell_angle_gamma  90.
_cell_volume  1170.0(7)
_cell_formula_units_Z  4
_cell_measurement_reflns_used  49
_cell_measurement_theta_min  10
_cell_measurement_theta_max  11.5
_cell_measurement_temperature  178
_exptl_crystal_description  'Prism'
_exptl_crystal_colour  'Colourless'
_exptl_crystal_size_max  0.9
_exptl_crystal_size_mid  0.7
_exptl_crystal_size_min  0.4
_exptl_crystal_size_rad  ?
_exptl_crystal_density_diffrn  2.915
_exptl_crystal_density_meas  ?
_exptl_absorpt_coefficient_mu  6.0
_exptl_absorpt_correction_type  'empirical \y scans'
_exptl_absorpt_correction_T_min  0.23
_exptl_absorpt_correction_T_max  0.99
_diffrn_radiation_type  'MoK\a'
_diffrn_radiation_wavelength  0.71069
_diffrn_measurement_device  'Siemens R3'
_diffrn_measurement_method  '\w'
_diffrn_reflns_number  5383
_diffrn_reflns_av_R_equivalents  0.04
_diffrn_reflns_theta_max  27.5
_diffrn_reflns_limit_h_min  -25
_diffrn_reflns_limit_h_max  25
_diffrn_reflns_limit_k_min  0
_diffrn_reflns_limit_k_max  10
_diffrn_reflns_limit_l_min  0
_diffrn_reflns_limit_l_max  10
_diffrn_standards_number  3
_diffrn_standards_interval_count  147
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%  +-1.5
_reflns_number_total  1351
_reflns_number_observed  1328
_reflns_observed_criterion  F>4\s(F)
_refine_ls_structure_factor_coef  F
_refine_ls_R_factor_obs  0.026
_refine_ls_wR_factor_obs  0.030
_refine_ls_goodness_of_fit_obs  1.6
_refine_ls_number_reflns  1328
_refine_ls_number_parameters  70
_refine_ls_hydrogen_treatment  ?
_refine_ls_weighting_scheme  '1/[\s^2^(F)+0.0001F^2^]'
_refine_ls_shift/esd_max  0.002
_refine_diff_density_max  1.0
_refine_diff_density_min  -0.9
_refine_ls_extinction_method  ?
_refine_ls_extinction_coef  ?
_atom_type_scat_source  IntTabIV
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 Ag .205260(10)
     .09578(2) .26763(2) .02510(10)
 Zn .50000 .16483(4) .25000 .01670(10)
 S(1) .29939(3) -.11251(6) .38966(6) .01750(10)
 S(2) .13289(3) .10224(6) .53246(6) .0192(2)
 N(1) .42556(10) .0178(2)   .3142(2)   .0237(5)
 N(2) .04535(10) -.1725(2)   .4213(2)   .0208(5)
 C(1) .37350(11) -.0371(2)   .3417(2)   .0168(5)
 C(2) .08141(11) -.0582(3)   .4664(2)   .0168(5)