#------------------------------------------------------------------------------
#$Date: 2008-01-26 13:05:32 +0000 (Sat, 26 Jan 2008) $
#$Revision: 19 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000805.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000805
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  973
_journal_page_last  975
loop_
_publ_author_name
 'Averbuch-Pouchot, M.T.'
 'Durif, A.'
_chemical_formula_sum  'H16 N2 O13 P2 Te1'
_chemical_formula_weight  441.677
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 21/n'
_symmetry_space_group_name_Hall  ?
_cell_length_a  7.651(2)
_cell_length_b  21.790(10)
_cell_length_c  6.689(2)
_cell_angle_alpha  90.
_cell_angle_beta  113.85(3)
_cell_angle_gamma  90.
_cell_volume  1020.0(10)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  2.876
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  864
_exptl_absorpt_coefficient_mu  1.766
_diffrn_radiation_type  Ag
_diffrn_radiation_wavelength  0.5608
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 Te .0 .0 .0
 P(1) .53030(10)
      .78307(4) .01560(10)
 P(2) .62690(10)
      .87860(3) .34550(10)
 O(1) .2736(3) .00410(10)
         .1386(4)
 O(2) .5283(3) .56020(10)
         .3058(4)
 O(3) .0070(3) .93490(10)
         .1943(4)
 O(E11) .8934(4) .68820(10)
        .3071(4)
 O(E21) .4441(3) .74790(10)
        .1443(4)
 O(E31) .6798(4) .74450(10)
        -.0341(4)
 O(E12) .7366(3) .43150(10)
        .1111(4)
 O(E22) .4202(3) .89460(10)
        .2678(4)
 O(E32) .6820(3) .83590(10)
        .5498(4)
 O(L12) .6626(3) .83710(10)
        .1664(3)
 N(1) .5767(4) .68370(10)
         .5463(5)
 N(2) .6392(4) .0666(2) .3292(5)
 H(1N1) .056(7) .792(3) .937(8)
 H(2N1) .835(3) .060(10)
        .168(9)
 H(3N1) .078(8) .792(3) .137(9)
 H(4N1) .507(9) .339(3) .430(10)
 H(1N2) .520(10)
      .042(3) .250(10)
 H(2N2) .890(10)
      .577(4) .040(10)
 H(3N2) .730(10)
      .050(4) .310(10)
 H(4N2) .629(9) .102(3) .250(10)
 H(1) .317(8) .963(3) .177(9)
 H(2) .062(8) .052(3) .325(9)
 H(3) .890(10)
    .938(3) .250(10)
 H(P1) .777(8) .221(3) .456(9)
 H(P2) .206(8) .194(3) .423(9)