data_2000811
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  991
_journal_page_last  993
loop_
_publ_author_name
 'Chiang, H.-C.'
 'Lin, S.-M.'
 'Ueng, C.-H.'
_chemical_formula_sum  'C4 H11 Ge1 N1 O4'
_chemical_formula_weight  209.6
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 1 21/n 1'
_symmetry_space_group_name_Hall  '-P 2yn'
_cell_length_a  5.161(2)
_cell_length_b  12.251(4)
_cell_length_c  11.266(3)
_cell_angle_alpha  90.
_cell_angle_beta  94.87(2)
_cell_angle_gamma  90.
_cell_volume  709.8(3)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  1.96
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  424
_exptl_absorpt_coefficient_mu  4.21
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.7093
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 Ge .00293(9) .14709(4) .15760(5)
 N -.2573(8) .2551(3) .2346(4)
 O1 .1873(7) .2690(3) .1369(3)
 O2 .0305(7) .0852(3) .3021(3)
 O3 .2311(6) .0566(3) .0972(3)
 O4 -.2650(7) .1140(3) .0566(3)
 C1 -.0885(13) .1377(5) .3943(5)
 C2 -.3217(12) .1995(5) .3463(5)
 C3 -.1161(12) .3585(4) .2543(6)
 C4 .0595(13) .3696(4) .1561(6)
 HN -.428 .258 .192
 HO3 .418 .087 .105
 HO4 -.204 .073 .013
 H1A -.139 .085 .456
 H1B .038 .193 .436
 H2A -.469 .147 .329
 H2B -.374 .255 .405
 H3A -.246 .422 .256
 H3B -.014 .357 .334
 H4A .186 .431 .173
 H4B -.052 .391 .078