#------------------------------------------------------------------------------
#$Date: 2008-01-26 13:05:32 +0000 (Sat, 26 Jan 2008) $
#$Revision: 19 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000817.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000817
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1025
_journal_page_last  1027
loop_
_publ_author_name
 'Okamoto, K.'
 'Hidaka, J.'
 'Fukagawa, M.'
 'Kanamori, K.'
_chemical_formula_moiety  'C6 H12 N1 O9 V1,4(H2 O1)'
_chemical_formula_sum  'C6 H20 N1 O13 V'
_chemical_formula_weight  365.17
_symmetry_cell_setting  triclinic
_symmetry_space_group_name_H-M  'P -1'
_symmetry_space_group_name_Hall  ?
_cell_length_a  7.929(2)
_cell_length_b  8.716(3)
_cell_length_c  10.914(3)
_cell_angle_alpha  98.77(2)
_cell_angle_beta  90.30(2)
_cell_angle_gamma  105.79(2)
_cell_volume  716.4(8)
_cell_formula_units_Z  2
_exptl_crystal_density_diffrn  1.693
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  380
_exptl_absorpt_coefficient_mu  0.73
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 V .04843(8) .35835(7) .22604(6)
 N .3041(4) .2995(4) .2162(3)
 O(1) .0071(4) .1389(3) .2808(3)
 O(2) .1109(5) -.0253(4) .3787(3)
 O(3) .1265(4) .3699(4) .0470(3)
 O(4) .2670(5) .2753(5) -.1101(3)
 O(5) .2222(4) .5371(4) .3449(3)
 O(6) .4970(4) .6850(4) .3959(4)
 O(7) -.0194(4) .5634(3) .1875(3)
 O(8) -.1095(4) .3822(4) .3765(3)
 O(9) -.1884(5) .2283(5) .1291(3)
 O(10) .1492(4) .3000(4) .6107(3)
 O(11) .3955(4) .0309(4) .7825(3)
 O(12) .3142(4) .8759(4) .5374(3)
 O(13) .2751(6) .8004(7) .1097(4)
 C(1) .1315(5) .0940(5) .3264(4)
 C(2) .3134(5) .2002(5) .3136(4)
 C(3) .2313(5) .2884(5) .0002(4)
 C(4) .3096(5) .2089(5) .0911(4)
 C(5) .3882(5) .5681(5) .3346(4)
 C(6) .4467(5) .4521(5) .2377(4)