#------------------------------------------------------------------------------
#$Date: 2008-01-26 13:05:32 +0000 (Sat, 26 Jan 2008) $
#$Revision: 19 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000818.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000818
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1027
_journal_page_last  1029
loop_
_publ_author_name
 'Davies, J.A.'
 'Pinkerton, A.A.'
 'Vilmer, M.'
_chemical_formula_sum  'C10 H30 Cl2 Pd1 O3 P4'
_symmetry_cell_setting  orthorhombic
_symmetry_space_group_name_H-M  'Pbca'
_symmetry_space_group_name_Hall  ?
_cell_length_a  14.332(3)
_cell_length_b  16.592(3)
_cell_length_c  17.420(3)
_cell_angle_alpha  90.
_cell_angle_beta  90.
_cell_angle_gamma  90.
_cell_volume  4142(3)
_cell_formula_units_Z  8
_exptl_crystal_density_diffrn  1.60
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  2032
_exptl_absorpt_coefficient_mu  1.45
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.70930
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 Pd1 .39587(2) .22741(2) .351500(10)
 C11 .23868(7) .20258(8) .38343(6)
 C12 .36333(8) .18350(8) .22378(6)
 P1 .54426(7) .24495(6) .31210(6)
 P2 .41181(7) .26389(6) .47506(6)
 P3 .59204(8) .07279(7) .36083(7)
 P4 .34228(8) .43198(7) .43644(7)
 O1 .6231(2) .1055(2) .4354(2)
 O2 .4328(3) .4358(2) .3973(3)
 O3 .4231(4) -.0035(3) .1791(4)
 C1 .3787(3) .1805(3) .5365(2)
 C2 .3327(3) .3446(2) .4985(2)
 C3 .5192(3) .2944(3) .5191(3)
 C4 .5468(3) .3077(3) .2265(2)
 C5 .5902(3) .1471(2) .2856(2)
 C6 .6392(3) .2878(3) .3657(3)
 C7 .4793(3) .0287(3) .3683(3)
 C8 .6632(4) -.0055(3) .3225(4)
 C9 .2470(4) .4255(4) .3722(4)
 C10 .3140(5) .5156(3) .4960(4)
 H1 .345 .362 .550
 H2 .271 .325 .495
 H3 .653 .155 .269
 H4 .554 .126 .244
 H5 .386 .197 .588
 H6 .315 .167 .527
 H7 .417 .135 .527
 H8 .509 .307 .572
 H9 .564 .252 .515
 H10 .542 .341 .493
 H11 .610 .315 .210
 H12 .512 .282 .187
 H13 .520 .359 .237
 H14 .694 .288 .335
 H15 .624 .342 .379
 H16 .649 .257 .411
 H17 .479 -.010 .408
 H18 .433 .068 .378
 H19 .467 .003 .321
 H20 .668 -.048 .359
 H21 .637 -.026 .276
 H22 .723 .016 .313
 H23 .250 .469 .335
 H24 .255 .376 .344
 H25 .194 .426 .400
 H26 .317 .566 .466
 H27 .252 .508 .512
 H28 .357 .515 .533