data_2000825
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1051
_journal_page_last  1054
loop_
_publ_author_name
 'Yamaguchi, K.'
 'Matsumura, G.'
 'Tanno, M.'
 'Sueyoshi, S.'
 'Miyata, N.'
_chemical_formula_sum  'C14 H21 N3 O2'
_chemical_formula_weight  263.34
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 21/a'
_symmetry_space_group_name_Hall  ?
_cell_length_a  13.8540(10)
_cell_length_b  9.0710(10)
_cell_length_c  11.808(4)
_cell_angle_alpha  90.
_cell_angle_beta  92.140(10)
_cell_angle_gamma  90.
_cell_volume  1482.9(3)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  1.179
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  568
_exptl_absorpt_coefficient_mu  0.614
_diffrn_radiation_type  Cu
_diffrn_radiation_wavelength  1.54050
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 N(1) 1.00700(10)
       .50360(10)
       .29370(10)
 C(2) .99180(10)
      .6514(2) .24180(10)
 O(3) .92920(10)
      .66410(10)
         .16830(10)
 N(4) 1.05340(10)
       .75370(10)
       .27990(10)
 N(5) .95010(10)
      .4517(2) .37230(10)
 O(6) .89290(10)
      .54410(10)
         .40860(10)
 C(7) 1.07840(10)
       .4073(2) .25010(10)
 C(8) 1.09250(10)
       .4030(2) .13530(10)
 C(9) 1.16310(10)
       .3121(2) .0936(2)
 C(10) 1.22010(10)
     .2244(2) .16620(10)
 C(11) 1.20390(10)
     .2300(2) .2809(2)
 C(12) 1.13410(10)
     .3207(2) .32450(10)
 C(13) 1.2975(2) .1272(3) .1212(2)
 C(14) 1.05590(10)
     .8967(2) .2174(2)
 C(15) .9638(2) .9848(3) .2284(2)
 C(16) 1.0830(2) .8741(3) .0955(2)
 C(17) 1.12290(10)
     .7318(2) .3769(2)
 C(18) 1.2250(2) .7192(4) .3376(3)
 C(19) 1.1100(2) .8521(3) .4658(2)
 H(8) 1.0530(10)
      .464(2) .081(2)
 H(9) 1.1720(10)
      .306(2) .014(2)
 H(11) 1.2460(10)
       .173(2) .335(2)
 H(12) 1.1250(10)
       .327(2) .408(2)
 H(13A) 1.289(2) .107(3) .047(2)
 H(13B) 1.3070(10)
     .036(3) .166(2)
 H(13C) 1.361(2) .170(3) .130(2)
 H(14) 1.1110(10)
       .947(2) .257(2)
 H(15A) .9070(10)
       .943(3) .189(2)
 H(15B) .9490(10)
       .994(3) .306(2)
 H(15C) .974(2) 1.073(3) .197(2)
 H(16A) 1.034(2) .823(3) .050(2)
 H(16B) 1.147(2) .821(3) .093(2)
 H(16C) 1.0890(10)
     .962(3) .056(2)
 H(17) 1.1060(10)
       .633(2) .414(2)
 H(18A) 1.230(2) .652(3) .277(2)
 H(18B) 1.247(2) .810(3) .299(2)
 H(18C) 1.259(2) .704(3) .393(2)
 H(19A) 1.155(2) .826(3) .531(2)
 H(19B) 1.038(2) .859(3) .483(2)
 H(19C) 1.127(2) .941(3) .440(2)