data_2000827
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1054
_journal_page_last  1057
loop_
_publ_author_name
 'Kaneko, F.'
 'Kobayashi, M.'
 'Kitagawa, Y.'
 'Matsuura, Y.'
 'Sato, K.'
 'Suzuki, M.'
_chemical_formula_sum  'C18 H34 O2'
_chemical_formula_weight  282.47
_symmetry_cell_setting  orthorhombic
_symmetry_space_group_name_H-M  'P b c a'
_symmetry_space_group_name_Hall  '-P 2ac 2ab'
_cell_length_a  7.3110(10)
_cell_length_b  5.5650(10)
_cell_length_c  88.010(10)
_cell_angle_alpha  90.
_cell_angle_beta  90.
_cell_angle_gamma  90.
_cell_volume  3581.1(8)
_cell_formula_units_Z  8
_exptl_crystal_density_diffrn  1.05
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  1264
_exptl_absorpt_coefficient_mu  0.474
_diffrn_radiation_type  Cu
_diffrn_radiation_wavelength  1.5418
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 C(1) .0339(4) -.2294(4) .01625(3)
 C(2) .0623(3) -.4192(4) .02790(2)
 C(3) -.0296(4) -.3842(6) .04291(3)
 C(4) .0328(6) -.5767(7) .05414(4)
 C(5) -.0470(5) -.5539(7) .06984(4)
 C(6) .0227(5) -.7425(6) .08055(4)
 C(7) .0249(6) -.7243(7) .09535(4)
 C(8) -.0399(5) -.5170(6) .10464(4)
 C(9) .0359(5) -.5089(6) .12053(4)
 C(10) -.0396(6) -.3074(7) .13035(4)
 C(11) .0387(5) -.2994(6) .14611(4)
 C(12) -.0393(5) -.1009(6) .15601(4)
 C(13) .0378(5) -.0925(6) .17198(4)
 C(14) -.0393(5) .1057(6) .18193(3)
 C(15) .0397(5) .1104(6) .19785(4)
 C(16) -.0385(5) .3065(6) .20796(4)
 C(17) .0422(5) .3099(6) .22371(3)
 C(18) -.0362(5) .5066(6) .23380(4)
 O(1) .1268(6) -.2659(7) .00378(4)
 O(2) -.0652(7) -.0563(8) .01819(5)
 H(1) .033(5) -.574(7) .0233(4)
 H(2) .167(5) -.427(7) .0295(4)
 H(3) -.002(5) -.212(9) .0468(5)
 H(4) -.181(5) -.397(6) .0402(4)
 H(5) .007(5) -.739(7) .0502(4)
 H(6) .177(5) -.563(6) .0564(4)
 H(7) -.037(4) -.373(7) .0748(4)
 H(8) -.186(5) -.570(7) .0678(4)
 H(9) .076(5) -.895(8) .0747(4)
 H(10) .074(5) -.865(8) .1015(4)
 H(11) -.006(5) -.372(8) .1005(5)
 H(12) -.152(5) -.526(7) .1058(4)
 H(13) .012(4) -.671(7) .1266(4)
 H(14) .161(4) -.503(6) .1194(3)
 H(15) -.018(4) -.166(7) .1250(4)
 H(16) -.180(4) -.308(5) .1300(3)
 H(17) .024(4) -.460(7) .1516(4)
 H(18) .161(4) -.278(6) .1451(3)
 H(19) -.005(5) .063(8) .1507(5)
 H(20) -.173(4) -.124(5) .1567(3)
 H(21) .019(4) -.258(7) .1772(4)
 H(22) .157(4) -.074(6) .1712(4)
 H(23) -.028(4) .258(7) .1765(4)
 H(24) -.165(4) .095(5) .1816(3)
 H(25) .009(4) -.050(7) .2029(4)
 H(26) .171(4) .138(5) .1970(3)
 H(27) -.024(4) -.534(7) .2025(4)
 H(28) -.167(4) .285(5) .2085(3)
 H(29) .018(5) .144(8) .2282(4)
 H(30) .169(5) .327(7) .2237(4)
 H(31) -.155(5) .491(7) .2339(4)
 H(32) .028(6) .503(7) .2432(5)
 H(33) -.019(5) .683(8) .2288(5)
 H(34) .107(6) -.163(8) -.0035(5)