data_2000830
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1063
_journal_page_last  1065
loop_
_publ_author_name
 'Lokaj, J.'
 'Sivy, P.'
 'Kettmann, V.'
_chemical_formula_sum  'C10 H10 O4'
_chemical_formula_weight  194.2
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 21/c'
_symmetry_space_group_name_Hall  ?
_cell_length_a  9.266(7)
_cell_length_b  14.570(10)
_cell_length_c  7.404(5)
_cell_angle_alpha  90.
_cell_angle_beta  108.60(6)
_cell_angle_gamma  90.
_cell_volume  947(2)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  1.362
_exptl_crystal_density_meas  1.350(10)
_exptl_crystal_F_000  408
_exptl_absorpt_coefficient_mu  0.66
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71069
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 C(1) .5289(3) .7181(2) .1762(4)
 C(2) .6513(3) .7813(2) .1958(4)
 C(3) .5964(3) .8646(2) .1846(3)
 C(4) .4362(2) .8599(2) .1576(3)
 C(5) .3339(2) .92410(10)
         .1464(3)
 C(6) .1730(2) .90860(10)
         .1217(3)
 C(7) .0790(3) .8632(2) -.0364(3)
 C(8) .1261(3) .8290(2) -.1970(4)
 C(9) .1112(3) .9429(2) .2575(3)
 C(10) .2054(3) .9955(2) .4234(4)
 O(1) .5240(2) .63650(10)
         .1813(3)
 O(2) .3977(2) .76810(10)
         .1506(2)
 O(3) -.0636(2) .84860(10)
       -.0538(2)
 O(4) -.0272(2) .92960(10)
       .2431(3)
 H(C2) .755(2)   .7636(15) .213(3)
 H(C3) .640(3)   .9223(16) .189(3)
 H(C5) .368(2)   .9861(14) .158(3)
 H1(C8) .222(3)   .8557(17) -.206(3)
 H2(C8) .053(3)   .8352(17) -.311(3)
 H3(C8) .152(3)   .7701(19) -.175(4)
 H1(C10) .145(3)   1.0173(16) .507(3)
 H2(C10) .283(3)   .9620(17) .506(3)
 H3(C10) .258(3)   1.0468(17) .395(4)
 H(O3) -.082(3)   .881(2)   .070(4)