data_2000834
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1074
_journal_page_last  1076
loop_
_publ_author_name
 'Englehardt, U.'
 'Stromburg, B.'
_chemical_formula_sum  'C18 H22 N4 O4 P2'
_chemical_formula_weight  420.346
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_cell_length_a  6.995(2)
_cell_length_b  14.902(5)
_cell_length_c  9.803(4)
_cell_angle_alpha  90.
_cell_angle_beta  110.33(3)
_cell_angle_gamma  90.
_cell_volume  958.0(10)
_cell_formula_units_Z  2
_exptl_crystal_density_diffrn  1.457
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  440
_exptl_absorpt_coefficient_mu  0.25
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71069
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 P .45200(10)
      .94268(4) .12364(7) .0374(4)
 O(1) .3275(3) .87500(10)
         .1596(2) .0500(10)
 O(2) .6317(3) .98400(10)
         .25700(10)
         .0420(10)
 N(1) .3202(3) 1.03290(10)
       .0413(2) .0370(10)
 N(2) .5611(3) .90580(10)
         .0119(2) .0370(10)
 C(1) .7843(4) .92620(10)
         .3479(2) .038(2)
 C(2) .9489(5) .9047(2) .3105(3) .048(2)
 C(3) 1.0950(5) .8485(2) .3986(3) .055(2)
 C(4) 1.0749(5) .8149(2) .5230(3) .053(2)
 C(5) .9102(5) .8383(2) .5600(3) .057(3)
 C(6) .7626(5) .8947(2) .4730(3) .050(2)
 C(7) .2268(5) 1.0921(2) .1207(3) .048(2)
 C(8) .6127(5) .8362(2) -.1894(3) .050(2)
 C(9) .4778(5) .8336(2) -.0966(3) .048(2)