#------------------------------------------------------------------------------ #$Date: 2008-01-13 22:15:36 +0000 (Sun, 13 Jan 2008) $ #$Revision: 14 $ #$URL: svn://www.crystallography.net/cod/cif/2/2000841.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2000841 _journal_name_full 'Acta Cryst.' _journal_year 1992 _journal_volume C48 _journal_page_first 1101 _journal_page_last 1102 loop_ _publ_author_name 'Hong, M.' 'Huang, Z.' 'Lei, X.' 'Jiang, F.' 'Liu, H.' _chemical_formula_moiety 'C10 H20 Au1 N2 S4,F6 Sb1' _chemical_formula_sum 'C10 H20 Au1 F6 N2 S4 Sb1' _chemical_formula_weight 1458.55 _symmetry_cell_setting triclinic _symmetry_space_group_name_H-M 'P -1' _symmetry_space_group_name_Hall '-P 1' _cell_length_a 14.533(3) _cell_length_b 18.004(5) _cell_length_c 8.538(2) _cell_angle_alpha 100.370(10) _cell_angle_beta 105.92(5) _cell_angle_gamma 74.69(3) _cell_volume 2058.06 _cell_formula_units_Z 4 _exptl_crystal_density_diffrn 2.353 _exptl_crystal_density_meas ? _exptl_crystal_F_000 1368 _exptl_absorpt_coefficient_mu 8.87 _diffrn_radiation_type Mo _diffrn_radiation_wavelength 0.71073 loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z Au(1) .94780(5) .60835(4) .65278(9) Au(2) .35591(5) -.10628(4) .53398(8) Sb(1) .56350(10) .34575(8) .8224(2) Sb(2) .15720(10) .13515(9) 1.0282(2) S(1) 1.1055(4) .6304(3) .7275(6) S(2) .7873(4) .5928(3) .5806(6) S(3) .9869(4) .6066(3) .4050(6) S(4) .9109(4) .6105(3) .9015(6) S(5) .1858(4) -.0749(3) .4922(6) S(6) .3276(3) -.1498(3) .7533(6) S(7) .5258(3) -.1327(3) .5857(5) S(8) .3869(4) -.0656(3) .3133(6) F(21) .4980(10) .4080(10) .974(2) F(22) .665(2) .317(2) .977(2) F(23) .5100(10) .2710(10) .827(2) F(24) .6110(10) .4220(10) .803(2) F(25) .6300(10) .2818(9) .674(2) F(26) .463(2) .379(2) .661(3) F(31) .7560(10) -.1878(9) .831(2) F(32) .7420(10) -.0610(10) 1.032(2) F(33) .8320(10) -.0775(9) .803(2) F(34) .0540(10) .2063(9) .095(2) F(35) .8520(10) .8060(10) .133(2) F(36) .0680(10) .0820(10) .890(2) N(10) .1700(10) .6306(9) .460(2) N(20) .7210(10) .6086(9) .850(2) N(30) .1350(10) -.1208(8) .735(2) N(40) .5820(10) -.0966(8) .342(2) C(10) .9010(10) .3780(10) .480(2) C(11) .7370(10) .3510(10) .425(3) C(12) .658(2) .4250(10) .392(3) C(13) .162(2) .6190(10) .282(3) C(14) .120(2) .699(2) .211(3) C(20) .7930(10) .6050(10) .789(2) C(21) .6200(10) .6040(10) .748(2) C(22) .554(2) .684(2) .731(3) C(23) .730(2) .6250(10) 1.037(2) C(24) .762(2) .5460(10) 1.106(3) C(30) .2020(10) -.1160(10) .671(2) C(31) .1570(10) -.1630(10) .883(2) C(32) .159(2) -.1040(10) 1.036(3) C(33) .0300(10) -.0870(10) .658(2) C(34) -.016(2) -.148(2) .536(3) C(40) .5110(10) -.0970(10) .402(2) C(41) .5620(10) -.0660(10) .178(2) C(42) .559(2) -.1350(10) .040(2) C(43) .6860(10) -.1230(10) .430(2) C(44) .724(2) .7890(10) .400(3)