#------------------------------------------------------------------------------
#$Date: 2008-11-20 19:58:43 +0000 (Thu, 20 Nov 2008) $
#$Revision: 481 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000843.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000843
_journal_name_full 'Acta Crystallographica Section C'
_journal_year  1992
_journal_volume 48
_journal_page_first  1105
_journal_page_last  1107
loop_
_publ_author_name
 'Kumar, N.R.S.'
 'Nethaji, M.'
_chemical_formula_sum  'Cl4 Fe1 H14 N4 O2'
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_h-m  'P 1 21/c 1'
_symmetry_space_group_name_hall  '-P 2ybc'
_cell_length_a  8.0270(10)
_cell_length_b  5.725(2)
_cell_length_c  11.430(2)
_cell_angle_alpha  90.
_cell_angle_beta  97.080(10)
_cell_angle_gamma  90.
_cell_volume  521.3(2)
_cell_formula_units_z  2
_exptl_crystal_density_diffrn  1.910
_exptl_crystal_density_meas  1.92
_exptl_crystal_f_000  304
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71069
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 Fe .00000 .00000 .00000
 N1 .2098(2) -.1576(2) .11890(10)
 N2 .3021(2) -.3565(2) .08310(10)
 Cl1 -.00858(5) -.31310(10)
        -.14494(3)
 Cl2 .46301(5) -.31440(10)
       .35879(3)
 O1 .18990(10)
    .1856(2) -.08370(10)
 H11 .274(3) -.051(4) .133(2)
 H12 .182(3) -.196(4) .180(2)
 H21 .377(4) -.417(6) .137(3)
 H22 .342(4) -.344(6) .014(3)
 H23 .228(4) -.475(4) .068(3)
 H11w .270(3) .110(6) -.098(3)
 H12w .146(4) .242(6) -.142(3)