data_2000847
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1112
_journal_page_last  1114
loop_
_publ_author_name
 'Reuter, H.'
 'Schroder, D.'
_chemical_formula_moiety  'C1 H3 Cl3 O1 Sn1,2(C1 H4 O1)'
_chemical_formula_sum  'C3 H11 Cl3 O3 Sn1'
_chemical_formula_weight  320.19
_symmetry_cell_setting  triclinic
_symmetry_space_group_name_H-M  'P -1'
_symmetry_space_group_name_Hall  ?
_cell_length_a  7.552(2)
_cell_length_b  8.114(2)
_cell_length_c  9.714(4)
_cell_angle_alpha  93.88(2)
_cell_angle_beta  102.04(3)
_cell_angle_gamma  114.80(2)
_cell_volume  520.3(4)
_cell_formula_units_Z  2
_exptl_crystal_density_diffrn  2.045
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  308
_exptl_absorpt_coefficient_mu  2.957
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 Sn(1) .45002(7) .57653(6) .34561(5) .0280(10)
 Cl(1) .6617(3) .8234(3) .2526(3) .0530(10)
 Cl(2) .1796(4) .4338(3) .1391(2) .0500(10)
 Cl(3) .3029(4) .7501(3) .4415(2) .0440(10)
 O(1) .6666(7) .6353(6) .5404(5) .031(2)
 O(2) .5743(9) .4103(8) .2685(6) .046(3)
 O(3) .3675(12) .0634(9) .2311(8) .071(4)
 C(1) .8745(13) .7680(14) .5659(11) .069(4)
 C(2) .729(2)   .4444(18) .1988(18) .109(9)
 C(3) .2337(2) -.0461(16) .1057(14) .088(6)