#------------------------------------------------------------------------------
#$Date: 2008-11-20 19:58:43 +0000 (Thu, 20 Nov 2008) $
#$Revision: 481 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000848.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000848
_journal_name_full 'Acta Crystallographica Section C'
_journal_year  1992
_journal_volume 48
_journal_page_first  1114
_journal_page_last  1116
loop_
_publ_author_name
 'Geremia, S.'
 'Rahman, A.'
 'Zangrando, E.'
_chemical_formula_moiety  'C13 H23 Co1 F3 N4 O3,F6 P1'
_chemical_formula_sum  'C13 H23 Co1 F9 N4 O3 P1'
_chemical_formula_weight  544.2
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_cell_length_a  6.906(3)
_cell_length_b  14.545(3)
_cell_length_c  21.236(9)
_cell_angle_alpha  90.
_cell_angle_beta  99.05(2)
_cell_angle_gamma  90.
_cell_volume  2106.0(10)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  1.72
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  1104
_exptl_absorpt_coefficient_mu  0.98
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.7107
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 Co .18196(7) .76086(3) .40027(2)
 F1 .4486(5) .5260(2) .3345(2)
 F2 .4393(6) .5593(2) .4313(2)
 F3 .1762(5) .5313(2) .3682(2)
 O1 -.1868(4) .7061(2) .3328(2)
 O2 -.0950(4) .6357(2) .4380(2)
 O3 .0283(4) .8588(2) .44270(10)
 N1 -.0302(4) .7586(2) .3321(2)
 N2 .0817(5) .6742(2) .4528(2)
 N3 .3912(4) .7635(2) .4712(2)
 N4 .2738(5) .8530(2) .3476(2)
 C1 -.1824(8) .8251(4) .2302(2)
 C2 -.0219(6) .8152(3) .2855(2)
 C3 .1607(6) .8688(3) .2949(2)
 C4 .2027(9) .9351(4) .2451(2)
 C5 .4652(6) .8994(3) .3649(2)
 C6 .5185(6) .9095(3) .4365(2)
 C7 .5653(6) .8211(3) .4723(2)
 C8 .5130(8) .6962(4) .5769(3)
 C9 .3670(6) .7094(3) .5174(2)
 C10 .1830(6) .6583(3) .5083(2)
 C11 .1146(9) .5972(3) .5566(2)
 C12 .3301(6) .6710(3) .3541(2)
 C13 .3460(7) .5746(3) .3724(2)
 P .9262(2) .10923(9) .37065(6)
 F4 .8640(6) .0128(3) .3416(2)
 F5 1.0015(7) .1980(3) .4092(2)
 F6 .7150(10)
      .1121(6) .3872(5)
 F7 1.1380(10)
    .1023(6) .3580(4)
 F8 .985(2) .0533(6) .4365(4)
 F9 .8550(10)
      .1668(7) .3141(3)
 F6A .7900(10)
    .1044(5) .4217(3)
 F7A 1.0420(10)
     .1208(6) .3147(4)
 F8A 1.0840(10)
     .0509(6) .4138(6)
 F9A .768(2) .1650(10)
      .3317(5)
 H1 -.2897 .7821 .2345
 H2 -.2343 .8884 .2284
 H3 -.1327 .8118 .1904
 H4 .3317 .9649 .2586
 H5 .2086 .9027 .2044
 H6 .1019 .9828 .2375
 H7 .6283 .7350 .5759
 H8 .4528 .7131 .6147
 H9 .5541 .6313 .5813
 H10 -.0165 .5723 .5389
 H11 .2054 .5483 .5686
 H12 .0983 .6347 .5948
 H13 .5695 .8621 .3490
 H14 .4603 .9606 .3441
 H15 .4054 .9394 .4524
 H16 .6338 .9520 .4454
 H17 .6226 .8339 .5176
 H18 .6658 .7860 .4526
 H19 .3609 .7185 .3856
 H20 .2940 .6884 .3107
 H(02) -.1250 .6464 .4030
 H(031) .0430 .9160 .4316
 H(032) .0430 .8535 .4862