#------------------------------------------------------------------------------
#$Date: 2008-11-20 19:58:43 +0000 (Thu, 20 Nov 2008) $
#$Revision: 481 $
#$URL: svn://www.crystallography.net/cod/cif/2/2002030.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2002030
_journal_name_full 'Acta Crystallographica Section C'
_journal_year 1993
_journal_volume 49
_journal_page_first 16
_journal_page_last 19
loop_
_publ_author_name
'Deshayes, L.'
'Keller, N.'
'Lance, M.'
'Nierlich, M.'
'Vigner, D.'
_chemical_formula_moiety ?
_chemical_formula_sum 'C28 H44 N2 O20 U1'
_chemical_formula_weight 966.69
_symmetry_cell_setting monoclinic
_symmetry_space_group_name_H-M 'P 21/n'
_symmetry_space_group_name_Hall ?
_cell_length_a 10.891(3)
_cell_length_b 8.312(2)
_cell_length_c 20.507(6)
_cell_angle_alpha  90
_cell_angle_beta 97.21(2)
_cell_angle_gamma  90
_cell_volume 1842.0(10)
_cell_formula_units_Z 2
_exptl_crystal_density_diffrn 1.74
_exptl_crystal_density_meas ?
_exptl_crystal_F_000 956
_exptl_absorpt_coefficient_mu 4.256
_diffrn_radiation_type Mo
_diffrn_radiation_wavelength 0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
U .0 .0 .0
O(21) -.0572(4) .1673(6) -.0464(2)
O(22) .1244(4) -.0827(7) -.0843(2)
O(23) .2140(4) .1181(7) .0094(3)
O(24) .1076(4) .1800(8) .0861(3)
O(25) .2894(5) .2841(8) .0861(3)
N .2929(5) .6972(8) .4378(3)
O(3) .9642(4) .3305(6) .1794(2)
O(6) .7639(5) .4414(7) .0972(3)
O(9) .6312(4) .1533(7) .0682(3)
O(12) .6967(5) -.0299(7) .1825(3)
O(15) .9448(5) .0446(6) .2220(2)
C(1) 1.0329(7) .1380(9) .2577(4)
C(2) 1.0458(6) .2929(9) .2339(3)
C(4) .9631(7) .4920(10)
  .1563(4)
C(5) .8843(6) .496(2) .0902(4)
C(7) .6910(8) .4110(10)
  .0360(4)
C(8) .5847(8) .3080(10)
  .0484(4)
C(10) .5464(7) .0540(10)
   .0982(4)
C(11) .6136(8) -.0860(10)
.1292(4)
C(13) .7827(8) -.1490(10)
.2077(4)
C(14) .8825(8) -.0750(10)
.2562(4)
C(16) 1.1077(7) .0840(10)
.3132(4)
C(17) 1.1968(8) .1880(10)
.3432(4)
C(18) 1.2112(8) .3390(10)
.3205(4)
C(19) 1.1350(7) .3930(10)
.2651(4)