#------------------------------------------------------------------------------
#$Date: 2008-01-13 22:15:36 +0000 (Sun, 13 Jan 2008) $
#$Revision: 14 $
#$URL: svn://www.crystallography.net/cod/cif/2/2002033.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2002033
_journal_name_full 'Acta Crystallographica, Section C'
_journal_year 1993
_journal_volume C49
_journal_page_first 22
_journal_page_last 26
loop_
_publ_author_name
'Caira, M.R.'
'Nassimbeni, L.R.'
'Stephen, A.M.'
'Schalkwyk, T.G.D.van.'
_chemical_formula_moiety 'C24 H42 N4,Cl6 Sn1'
_chemical_formula_sum 'C24 H42 Cl6 N4 Sn1'
_chemical_formula_weight 718.0
_symmetry_cell_setting monoclinic
_symmetry_space_group_name_H-M 'P 21/n'
_symmetry_space_group_name_Hall ?
_cell_length_a 10.002(2)
_cell_length_b 10.6390(10)
_cell_length_c 15.616(4)
_cell_angle_alpha  90
_cell_angle_beta 102.05(2)
_cell_angle_gamma  90
_cell_volume 1625.1(2)
_cell_formula_units_Z 2
_exptl_crystal_density_diffrn 1.467
_exptl_crystal_density_meas 1.460(10)
_exptl_crystal_F_000 732
_exptl_absorpt_coefficient_mu 1.31
_diffrn_radiation_type Mo
_diffrn_radiation_wavelength 0.71069
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
Sn(1) 0 0 0 .0380(10)
Cl(1) .23270(10)
   .03200(10)
.08130(10)
 .0590(10)
Cl(2) -.08510(10)
.13450(10)
 .10280(10)
  .0680(10)
Cl(3) -.02360(10)
-.18380(10)
  .08830(10)
   .0630(10)
N(1) .5000(3) -.1089(3) .2241(2) .0450(10)
N(2) .4822(4) -.2090(3) .1636(2) .0580(10)
C(3) .5647(6) -.1902(5) .1134(3) .070(2)
C(4) .6432(7) -.0739(6) .1287(5) .103(3)
C(5) .6205(5) -.0261(4) .2158(3) .057(2)
C(6) .5728(10) -.2789(7) .0409(4) .114(4)
C(7) .5826(6) .1119(5) .2088(4) .078(2)
C(8) .7370(6) -.0517(9) .2900(5) .112(4)
C(9) .4142(4) -.0993(4) .2755(3) .450(10)
C(10) .2971(4) -.1852(4) .2724(3) .53(2)
C(11) .2189(6) -.1279(6) .3351(4) .78(2)
C(12) .3162(7) -.0507(7) .3957(4) .89(3)
C(13) .4160(6) -.0016(4) .3438(3) .63(2)
C(14) .2592(9) .0484(8) .4453(5) .117(4)