#------------------------------------------------------------------------------
#$Date: 2008-11-20 19:58:43 +0000 (Thu, 20 Nov 2008) $
#$Revision: 481 $
#$URL: svn://www.crystallography.net/cod/cif/2/2002034.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2002034
_journal_name_full 'Acta Crystallographica Section C'
_journal_year 1993
_journal_volume 49
_journal_page_first 22
_journal_page_last 26
loop_
_publ_author_name
'Caira, M.R.'
'Nassimbeni, L.R.'
'Stephen, A.M.'
'Schalkwyk, T.G.D.van.'
_chemical_formula_moiety 'C24 H42 N4,Cl6 Sn1'
_chemical_formula_sum 'C24 H42 Cl6 N4 Sn1'
_chemical_formula_weight 718.0
_symmetry_cell_setting monoclinic
_symmetry_space_group_name_H-M 'P 21'
_symmetry_space_group_name_Hall ?
_cell_length_a 9.998(2)
_cell_length_b 10.6490(10)
_cell_length_c 15.637(4)
_cell_angle_alpha  90
_cell_angle_beta 102.03(2)
_cell_angle_gamma  90
_cell_volume 1628.3(3)
_cell_formula_units_Z 2
_exptl_crystal_density_diffrn 1.465
_exptl_crystal_density_meas 1.480(10)
_exptl_crystal_F_000 732
_exptl_absorpt_coefficient_mu 1.30
_diffrn_radiation_type Mo
_diffrn_radiation_wavelength 0.71069
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
Sn(1) .2439 0 .24820(10)
   .0360(10)
Cl(1) .4777(2) .0300(5) .3283(2) .060(2)
Cl(2) .1608(3) .1355(5) .3503(3) .0650(10)
Cl(3) .2223(3) -.1835(6) .3355(2) .0670(10)
Cl(4) .0122(2) -.0326(5) .1669(2) .0560(10)
Cl(5) .3305(3) -.1327(6) .1438(3) .072(2)
Cl(6) .2687(3) .1838(5) .1594(2) .0600(10)
N(1) .7443(8) -.1046(10) .4727(6) .047(4)
N(2) .7218(9) -.2029(10) .4112(5) .051(4)
N(15) -.2524(8) .1115(9) .0231(5) .040(4)
N(16) -.2394(9) .2136(10) .0820(6) .059(4)
C(3) .8020(18) -.1829(16) .3594(11) .099(8)
C(4) .8915(19) -.0728(16) .3754(11) .119(9)
C(5) .8633(9) -.0214(13) .4605(7) .056(5)
C(6) .794(3)   -.266(2)   .2812(12) .179(15)
C(7) .8240(14) .1163(14) .4498(11) .084(7)
C(8) .9775(13) -.036(3)   .5384(13) .164(13)
C(9) .6621(9) -.0959(11) .5266(7) .050(4)
C(10) .5475(9) -.1856(12) .5268(7) .051(4)
C(11) .4796(10) -.1377(13) .5995(8) .062(4)
C(12) .551(3)   -.023(3)   .637(2)   .245(18)
C(13) .6721(11) .0017(16) .5985(7) .069(5)
C(14A) .358(2)   -.055(3)   .5691(19) .088(11)
C(14B) .518(3)   .063(3)   .7056(17) .114(16)
C(17) -.3239(11) .1932(11) .1317(7) .053(4)
C(18) -.4022(14) .0785(16) .1131(10) .095(8)
C(19) -.3762(9) .0294(11) .0275(8) .058(5)
C(20) -.3396(15) .2823(15) .2015(9) .077(6)
C(21) -.3402(13) -.1080(12) .0325(10) .069(5)
C(22) -.4920(12) .0610(15) -.0468(9) .088(6)
C(23) -.1653(8) .1018(10) -.0254(5) .037(4)
C(24) -.0460(9) .1859(12) -.0184(7) .054(4)
C(25) .0424(10) .1249(13) -.0781(8) .061(5)
C(26) -.0622(11) .0582(12) -.1447(6) .056(4)
C(27) -.1596(9) .0021(14) -.0908(7) .061(4)
C(28) -.0013(13) -.0449(11) -.1902(8) .064(5)