data_2002059
_journal_name_full 'Acta Crystallographica, Section C'
_journal_year 1993
_journal_volume C49
_journal_page_first 84
_journal_page_last 85
loop_
_publ_author_name
'Viossat, B.'
'Nguyen-Huy Dung'
'Robert, F.'
_chemical_formula_moiety ?
_chemical_formula_sum 'C10 H10 Cl2 N2 Pd1'
_chemical_formula_weight 335.51
_symmetry_cell_setting monoclinic
_symmetry_space_group_name_H-M 'C 1 2/c 1'
_symmetry_space_group_name_Hall '-C 2yc'
_cell_length_a 8.7740(10)
_cell_length_b 15.474(2)
_cell_length_c 8.6350(10)
_cell_angle_alpha  90
_cell_angle_beta 90.560(10)
_cell_angle_gamma  90
_cell_volume 1172.3(3)
_cell_formula_units_Z 4
_exptl_crystal_density_diffrn 1.90
_exptl_crystal_density_meas 1.87(3)
_exptl_crystal_F_000 656
_exptl_absorpt_coefficient_mu 1.991
_diffrn_radiation_type Mo
_diffrn_radiation_wavelength 0.7107
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
Pd .0 .12684(4) .2500 .0383
Cl .26140(10)
.1290(2) .2668(2) .0569
N(1) .0 -.0040(4) .2500 .0417
N(2) .0 .2575(4) .2500 .0455
C(1) .0942(6) -.0489(4) .1559(6) .0456
C(2) .0969(6) -.1379(4) .1547(6) .0501
C(3) .0 -.1813(5) .2500 .0485
C(4) .0565(7) .3011(4) .1299(6) .0492
C(5) .0570(7) .3908(4) .1278(7) .0570
C(6) .0 .4352(6) .2500 .0581
H(1) .165(6) -.011(4) .101(7) ?
H(2) .161(6) -.159(4) .065(7) ?
H(3) .0000 -.236(6) .2500 ?
H(4) .105(7) .268(4) .049(7) ?
H(5) .101(6) .414(4) .033(7) ?
H(6) .0000 .502(6) .2500 ?