#------------------------------------------------------------------------------
#$Date: 2008-01-13 22:15:36 +0000 (Sun, 13 Jan 2008) $
#$Revision: 14 $
#$URL: svn://www.crystallography.net/cod/cif/2/2003252.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2003252
_journal_name_full     'Acta Crystallographica'
_journal_year          1995
_journal_volume    	C51
_journal_page_first    	348
_journal_page_last    	350
_publ_section_title    	
;
Eu~2~(PO~3~H)~3~
;
_chemical_formula_moiety    	'Eu2 (P1 O3 H1 )3'
_chemical_formula_sum    	'H3 Eu2 O9 P3'
_chemical_formula_weight    	543,8
loop_
    _symmetry_equiv_pos_as_xyz
    'x,y,z'
    '-x,-y,-z'
    'x,-y,z'
    '-x,+y,-z'
    '1/2-x,1/2-y,-z'
    '1/2-x,1/2+y,-z'
    '1/2+x,1/2+y,z'
    '1/2+x,1/2-y,z'
_symmetry_space_group_name_H-M    	'C 1 2/m 1'
_cell_length_a    	14.822(3)
_cell_length_b    	7.055(1)
_cell_length_c    	10.205(2)
_cell_angle_alpha    90
_cell_angle_beta    	123.79(1)
_cell_angle_gamma    90
_cell_volume    	886.9(3)
_cell_formula_units_Z    	4
_exptl_crystal_density_diffrn    	4.074
_exptl_crystal_density_meas    	4.06(1)
_diffrn_radiation_type    	'MoK\a'
_diffrn_radiation_wavelength    	0.71073
_cell_measurement_reflns_used    	20
_cell_measurement_theta_min    	5
_cell_measurement_theta_max    	12.5
_exptl_absorpt_coefficient_mu    	14.67
_cell_measurement_temperature    	293
_exptl_crystal_description    	'parallelepiped'
_exptl_crystal_size_max    	0.12
_exptl_crystal_size_mid    	0.10
_exptl_crystal_size_min    	0.04
_exptl_crystal_size_rad    	?
_exptl_crystal_colour    	'jaune'
_chemical_compound_source    	?
_diffrn_measurement_device    	'Siemens P3'
_diffrn_measurement_method    	'\w-2\q'
_exptl_absorpt_correction_type    	'empirique (Walker & Stuart, 1983)'
_exptl_absorpt_correction_T_min    	0.59
_exptl_absorpt_correction_T_max    	0.83
_diffrn_reflns_number    	2180
_reflns_number_total    	1099
_reflns_number_observed    	945
_reflns_observed_criterion    	F>=5\s(F)
_diffrn_reflns_av_R_equivalents    	0.033
_diffrn_reflns_theta_max    	27.5
_diffrn_reflns_limit_h_min    	-19
_diffrn_reflns_limit_h_max    	19
_diffrn_reflns_limit_k_min    	-1
_diffrn_reflns_limit_k_max    	9
_diffrn_reflns_limit_l_min    	-1
_diffrn_reflns_limit_l_max    	13
_diffrn_standards_number    	3
_diffrn_standards_interval_count    	50
_diffrn_standards_interval_time    	?
_diffrn_standards_decay_%    	<3
_refine_ls_structure_factor_coef    	Fsqd
_refine_ls_R_factor_obs    	0.026
_refine_ls_wR_factor_obs    	0.032
_refine_ls_goodness_of_fit_obs    	3.34
_refine_ls_number_reflns    	945
_refine_ls_number_parameters    	86
_refine_ls_hydrogen_treatment    	'noref'
_refine_ls_weighting_scheme    	'1/[\s^2^(F)+0.000030F^2^]'
_refine_ls_shift/esd_max    	0.002
_refine_diff_density_max    	1.32
_refine_diff_density_min    	-2.00
_refine_ls_extinction_method    	aucun
_refine_ls_extinction_coef    	?
_atom_type_scat_source    	'IntTabIV'
loop_
    _atom_site_label
    _atom_site_fract_x
    _atom_site_fract_y
    _atom_site_fract_z
    _atom_site_U_iso_or_equiv
    Eu(1) .16220(4) .0 .09290(5) .0080(2)
    Eu(2) .27840(4) .5 .31220(5) .0090(2)
    P(1) .3847(2) .0 .0500(3) .009(1)
    P(2) .3335(2) .0 .4566(3) .0009(1)
    P(3) .0025(3) .0546(6) .2755(4) .010(2)
    O(11) .3517(4) .1722(7) .9391(6) .017(2)
    O(12) .3338(6) .0 .1427(8) .017(3)
    O(21) .2775(5) .1708(7) .3486(6) .018(3)
    O(22) .3319(6) .0 .6022(8) .014(3)
    O(31) .0275(6) .0 .1517(8) .016(3)
    O(32) .8819(6) .0 .1967(8) .018(3)
    O(33) .0753(8) .9611(17) .4332(11) .023(7)
    H(1) .4940 .0 .1341 .020
    H(2) .4377 .0 .5005 .020
    H(3) .0105 .2453 .2789 .020