Crystallography Open Database

Information card for entry 2003469

2003468 << 2003469 >> 2003470

Preview

Coordinates	2003469.cif
Original IUCr paper	HTML

Structure parameters

Chemical name	1,1-Dimethyl-5-trimethylsilyl-1,3,3a,4,6,7,8,9-octahydro1-silanaphtho- [1,2 c] furan
Formula	C17 H30 O Si2
Calculated formula	C17 H30 O Si2
SMILES	[Si]1(OC[C@@H]2C1=C1CCCCC1=C([C@@H]2C)[Si](C)(C)C)(C)C.[Si]1(OC[C@H]2C1=C1CCCCC1=C([C@H]2C)[Si](C)(C)C)(C)C
Title of publication	<i>rac</i>-1,1,4-Trimethyl-5-trimethylsilyl-1,3,3a,4,6,7,8,9-octahydro-1-silanaphtho[1,2-<i>c</i>]furan at 153 K
Authors of publication	Pohl, E.; Herbst-Irmer, R.; Groth, U.; Eckenberg, P.
Journal of publication	Acta Crystallographica Section C
Year of publication	1995
Journal volume	51
Journal issue	5
Pages of publication	891 - 892
a	17.721 ± 0.002 Å
b	19.714 ± 0.002 Å
c	10.49 ± 0.001 Å
α	90°
β	90°
γ	90°
Cell volume	3664.7 ± 0.7 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	4
Space group number	56
Hermann-Mauguin space group symbol	P c c n
Hall space group symbol	-P 2ab 2ac
Residual factor for all reflections	0.0464
Residual factor for significantly intense reflections	0.0361
Weighted residual factors for all reflections	0.0927
Weighted residual factors for significantly intense reflections	0.0842
Goodness-of-fit parameter for all reflections	1.068
Goodness-of-fit parameter for significantly intense reflections	1.063
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

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