#------------------------------------------------------------------------------
#$Date: 2010-01-30 13:59:17 +0000 (Sat, 30 Jan 2010) $
#$Revision: 966 $
#$URL: svn://www.crystallography.net/cod/cif/2/2003499.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2003499
_journal_name_full               'Acta Crystallographica C'
_journal_volume                  51
_journal_year         1995
_journal_page_first    	878
_journal_page_last    	880
_publ_section_title
;
Chlorure de cis-Chloro(dim\'ethylsulfoxyde)(metformine)platine(II)
;
_chemical_formula_sum    	'C6 H17 Cl2 N5 O Pt S'
_chemical_formula_weight    	473.30
_space_group_IT_number           15
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_[local]_cod_cif_authors_sg_H-M  'C 2/c'
loop_
    _symmetry_equiv_pos_as_xyz
    'x,y,z'
    'x,-y,1/2+z'
    '-x,-y,-z'
    '-x,y,1/2-z'
    '1/2+x,1/2+y,z'
    '1/2+x,1/2-y,1/2+z'
    '1/2-x,1/2-y,-z'
    '1/2-x,1/2+y,1/2-z'
_cell_length_a    	18.169(3)
_cell_length_b    	10.932(3)
_cell_length_c    	16.120(3)
_cell_angle_alpha    	90
_cell_angle_beta    	117.17(2)
_cell_angle_gamma    	90
_cell_volume    	2842(8)
_cell_formula_units_Z    	8
_exptl_crystal_density_diffrn    	2.21
_exptl_crystal_density_meas    	2.20
_diffrn_radiation_type    	'MoK\a'
_diffrn_radiation_wavelength    	0.7107
_cell_measurement_reflns_used    	25
_cell_measurement_theta_min    	8.79
_cell_measurement_theta_max    	13.38
_exptl_absorpt_coefficient_mu    	10.47
_cell_measurement_temperature    	293
_exptl_crystal_description    	"parall\'el\'epip\`ede"
_exptl_crystal_size_max    	0.25
_exptl_crystal_size_mid    	0.12
_exptl_crystal_size_min    	0.10
_exptl_crystal_size_rad    	?
_exptl_crystal_colour    	'jaune p\^ale'
_chemical_compound_source    	"\'evaporation d'une solution m\'ethanolique"
_diffrn_measurement_device    	'Enraf-Nonius CAD-4'
_diffrn_measurement_method    	'\w-2\q'
_exptl_absorpt_correction_type    	'empirical'
_exptl_absorpt_correction_T_min    	0.668
_exptl_absorpt_correction_T_max    	1.330
_diffrn_reflns_number    	2877
_reflns_number_total    	2877
_reflns_number_observed    	1816
_reflns_observed_criterion    	'I >= 3\s(I)'
_diffrn_reflns_av_R_equivalents    	?
_diffrn_reflns_theta_max    	26
_diffrn_reflns_limit_h_min    	-22
_diffrn_reflns_limit_h_max    	19
_diffrn_reflns_limit_k_min    	0
_diffrn_reflns_limit_k_max    	13
_diffrn_reflns_limit_l_min    	0
_diffrn_reflns_limit_l_max    	19
_diffrn_standards_number    	3
_diffrn_standards_interval_count    	?
_diffrn_standards_interval_time    	120
_diffrn_standards_decay_%    	'non significatives'
_refine_ls_structure_factor_coef    	F
_refine_ls_R_factor_obs    	0.032
_refine_ls_wR_factor_obs    	0.038
_refine_ls_goodness_of_fit_obs    	1.20
_refine_ls_number_reflns    	1816
_refine_ls_number_parameters    	145
_refine_ls_hydrogen_treatment    	?
_refine_ls_weighting_scheme    	'1/\s^2^(F~o~)'
_refine_ls_shift/esd_max    	0.01
_refine_diff_density_max    	0.9(2)
_refine_diff_density_min    	-0.9(2)
_refine_ls_extinction_method    	'none'
_refine_ls_extinction_coef    	?
_atom_type_scat_source    	'IntTabIV'
loop_
    _atom_site_label
    _atom_site_fract_x
    _atom_site_fract_y
    _atom_site_fract_z
    _atom_site_u_iso_or_equiv
    Pt 1.00855(2) .16633(4) .60610(2) .04113(8)
    Cl(1) 1.0719(2) .3542(2) .6232(2) .0573(8)
    Cl(2) .8116(1) .6548(3) .7144(2) .0563(6)
    S .8829(1) .2463(2) .5514(2) .0490(6)
    O .8181(4) .1531(7) .5176(6) .071(3)
    N(1) 1.2132(5) -.0715(8) .7385(6) .052(3)
    N(2) 1.1188(4) .0829(7) .6607(5) .044(2)
    N(3) 1.0743(4) -.1175(7) .6754(5) .044(2)
    N(4) .9554(4) .0048(8) .5890(5) .052(2)
    N(5) .9428(4) -.2033(7) .6069(5) .049(2)
    C(1) 1.1349(5) -.0284(9) .6900(6) .045(3)
    C(2) .9899(5) -.1012(9) .6212(6) .046(3)
    C(3) .8749(6) .331(1) .6409(6) .072(3)
    C(4) .8594(6) .361(1) .4635(7) .065(3)
    C(51) .8529(6) -.192(1) .5493(8) .058(4)
    C(52) .9746(6) -.329(1) .6245(7) .056(3)
_cod_database_code 2003499