#------------------------------------------------------------------------------
#$Date: 2009-11-14 13:09:05 +0000 (Sat, 14 Nov 2009) $
#$Revision: 846 $
#$URL: svn://www.crystallography.net/cod/cif/2/2003610.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2003610
_journal_name_full               'Acta Crystallographica C'
_journal_volume                  51
_journal_year         1995
_journal_page_first    	1124
_journal_page_last    	1125
_publ_section_title
;
Tetramethylammonium Dichlorotriphenylstannate
;
_chemical_formula_moiety    	'C22 H27 Cl2 N1 Sn1'
_chemical_formula_sum    	'C22 H27 Cl2 N1 Sn1'
_chemical_formula_weight    	495.06
loop_
    _symmetry_equiv_pos_as_xyz
    'x,y,z'
    '-x,y,-z'
    '1/2+x,1/2+y,z'
    '1/2-x,1/2+y,-z'
_symmetry_space_group_name_H-M    	'C 2'
_cell_length_a    	14.648(2)
_cell_length_b    	9.8802(5)
_cell_length_c    	10.900(1)
_cell_angle_alpha    	90.
_cell_angle_beta    	134.984(3)
_cell_angle_gamma    	90.
_cell_volume    	1115.7(2)
_cell_formula_units_Z    	2
_exptl_crystal_density_diffrn    	1.474
_exptl_crystal_density_meas    	?
_diffrn_radiation_type    	'MoK\a'
_diffrn_radiation_wavelength    	0.71073
_cell_measurement_reflns_used    	25
_cell_measurement_theta_min    	10
_cell_measurement_theta_max    	12
_exptl_absorpt_coefficient_mu    	1.396
_cell_measurement_temperature    	300
_exptl_crystal_description    	'irregular'
_exptl_crystal_size_max    	0.21
_exptl_crystal_size_mid    	0.14
_exptl_crystal_size_min    	0.14
_exptl_crystal_size_rad    	0.16
_exptl_crystal_colour    	'colorless'
_chemical_compound_source    	?
_diffrn_measurement_device    	'Enraf-Nonius CAD-4'
_diffrn_measurement_method    	'\w/2\q'
_exptl_absorpt_correction_type
;
empirical (Walker & Stuart, 1983)
;
_exptl_absorpt_correction_T_min    	0.9007
_exptl_absorpt_correction_T_max    	1.0892
_diffrn_reflns_number    	1093
_reflns_number_total    	1007
_reflns_number_observed    	1004
_reflns_observed_criterion    	I>3\s(I)
_diffrn_reflns_av_R_equivalents    	0.025
_diffrn_reflns_theta_max    	25
_diffrn_reflns_limit_h_min    	0
_diffrn_reflns_limit_h_max    	17
_diffrn_reflns_limit_k_min    	0
_diffrn_reflns_limit_k_max    	11
_diffrn_reflns_limit_l_min    	-12
_diffrn_reflns_limit_l_max    	9
_diffrn_standards_number    	3
_diffrn_standards_interval_count    	?
_diffrn_standards_interval_time    	60
_diffrn_standards_decay_%    	none
_refine_ls_structure_factor_coef    	F
_refine_ls_R_factor_obs    	0.020
_refine_ls_wR_factor_obs    	0.025
_refine_ls_goodness_of_fit_obs    	0.389
_refine_ls_number_reflns    	1004
_refine_ls_number_parameters    	119
_refine_ls_hydrogen_treatment    	?
_refine_ls_weighting_scheme    	'w = 1/[\s^2^(F) + 0.0004F^2^ + 1]'
_refine_ls_shift/esd_max    	0.01
_refine_diff_density_max    	0.19(2)
_refine_diff_density_min    	0.07(2)
_refine_ls_extinction_method    	'none'
_refine_ls_extinction_coef    	?
_atom_type_scat_source    	'IntTabIV'
loop_
    _atom_site_label
    _atom_site_fract_x
    _atom_site_fract_y
    _atom_site_fract_z
    _atom_site_B_iso_or_equiv
    Sn 0 .25 0 2.445(7)
    Cl .23377(7) .2433(3) .1360(1) 3.81(2)
    N 0 .4305(7) -.500 4.1(2)
    C1 0 .4670(7) 0 2.6(1)
    C2 .0757(4) .5402(6) -.0102(5) 3.3(1)
    C3 .0748(4) .6803(6) -.0122(5) 4.0(1)
    C4 0 .751(2) 0 4.4(2)
    C5 -.0621(3) .1451(5) -.2199(4) 2.6(1)
    C6 -.1776(4) .1804(6) -.3865(5) 3.2(1)
    C7 -.2176(4) .1150(7) -.5311(5) 4.1(1)
    C8 -.1463(4) .0117(7) -.5128(5) 4.7(1)
    C9 -.0320(4) -.0242(6) -.3485(5) 4.4(1)
    C10 .0093(4) .0428(6) -.2051(5) 3.7(1)
    C11 .0915(7) .344(1) -.3486(9) 9.9(3)
    C12 .0621(6) .5147(9) -.5325(8) 9.3(2)
    H1 .128 .492 -.017 ?
    H2 .127 .726 -.022 ?
    H3 0 .847 0 ?
    H4 -.229 .250 -.401 ?
    H5 -.295 .142 -.645 ?
    H6 -.175 -.035 -.611 ?
    H7 .019 -.094 -.334 ?
    H8 .089 .017 -.092 ?
    H9 .045 .293 -.333 ?
    H10 .132 .283 -.366 ?
    H11 .155 .397 -.248 ?
    H12 -.001 .569 -.632 ?
    H13 .125 .571 -.435 ?
    H14 .102 .457 -.553 ?