data_2004745
_journal_name_full  'Acta Crystallographica'
_journal_year      1996
_journal_volume    	C52
_journal_page_first    	913
_journal_page_last    	919
_publ_section_title    	
;
Structures of Five \w-Phthalimidoaliphatic Carboxylic Acids
;
_chemical_formula_sum    	'C13 H13 N1 O4'
_chemical_formula_weight    	247.1
_symmetry_cell_setting    	monoclinic
_symmetry_space_group_name_H-M    	'P 21/n'
_cell_length_a    	6.574(4)
_cell_length_b    	4.899(2)
_cell_length_c    	37.413(13)
_cell_angle_alpha    	90
_cell_angle_beta    	95.18(3)
_cell_angle_gamma    	90
_cell_volume    	1200(1)
_cell_formula_units_Z    	4
_exptl_crystal_density_diffrn    	1.37
_cell_measurement_temperature    	295
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
N(1) .3410(10) .1679(16) .1404(2) .051(4)
O(7) .6175(9) .2728(17) .1095(2) .089(5)
O(8) .1130(9) .1597(15) .1837(2) .071(4)
O(130) -.2698(9) -.3469(16) -.0046(2) .077(4)
O(131) -.4921(9) -.2720(16) .0345(2) .083(5)
C(1) .4080(10) .4553(17) .1884(2) .040(5)
C(2) .4029(12) .6068(19) .2195(2) .054(6)
C(3) .5637(12) .7890(19) .2277(2) .052(5)
C(4) .7141(12) .828(2) .2048(2) .057(5)
C(5) .7183(12) .673(2) .1736(2) .056(6)
C(6) .5618(11) .4928(18) .1659(2) .043(5)
C(7) .5236(12) .301(2) .1350(2) .053(6)
C(8) .2648(12) .2483(19) .1722(2) .052(5)
C(9) .2468(12) -.0358(19) .1160(2) .054(5)
C(10) .0865(12) .0904(19) .0882(2) .050(5)
C(11) -.0342(11) -.1266(18) .0670(2) .047(5)
C(12) -.1921(12) -.0043(19) .0397(2) .052(5)
C(13) -.3267(12) -.217(2) .0218(2) .013(6)
H(2) .2803(12) .5852(19) .2366(2) ?
H(3) .5703(12) .9021(19) .2525(2) ?
H(4) .8304(12) .9809(20) .2112(2) ?
H(5) .8400(12) .6952(21) .1562(2) ?
H(91) .3643(12) -.1321(19) .1020(2) ?
H(92) .1731(12) -.1872(19) .1314(2) ?
H(101) .1636(12) .2162(19) .0699(2) ?
H(102) -.0171(12) .2148(19) .1021(2) ?
H(111) .0694(11) -.2506(18) .0532(2) ?
H(112) -.1107(11) -.2528(18) .0854(2) ?
H(121) -.1149(12) .1023(19) .0196(2) ?
H(122) -.2850(12) .1380(19) .0531(2) ?