data_2005053
_journal_name_full  'Acta Crystallographica'
_journal_year       1996
_journal_volume    'C52'
_journal_page_first     1471
_journal_page_last     1473
_publ_section_title
;
Piperazinium L-Tartrate
;
_chemical_formula_moiety     'C4 H12 N2 , C4 H4 O6'
_chemical_formula_sum     'C8 H16 N2 O6'
_chemical_formula_weight     236.23
_symmetry_cell_setting    'monoclinic'
loop_
_symmetry_equiv_pos_as_xyz
'x,y,z'
'-x,y+1/2,-z'
_symmetry_space_group_name_H-M     'P 21'
_cell_length_a     6.4262(10)
_cell_length_b     9.1322(10)
_cell_length_c     9.3627(10)
_cell_angle_alpha     90
_cell_angle_beta     108.850(10)
_cell_angle_gamma     90
_cell_volume     519.98(11)
_cell_formula_units_Z     2
_exptl_crystal_density_diffrn     1.509
_cell_measurement_temperature     293(2)
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
C(1) -0.5779(3)  .4773(2) -0.6549(2)  .0290(10)
C(2) -0.5047(3)  .5182(2) -0.7866(2)  .0290(10)
N(3) -0.3463(2)  .40810(10)
                          -0.80540(10)
                                      .0240(10)
C(4) -0.4425(3)  .2579(2) -0.8263(2)  .0260(10)
C(5) -0.5191(3)  .2163(2) -0.6958(2)  .0290(10)
N(6) -0.6749(2)  .3277(2) -0.67480(10)
                                      .0280(10)
C(1')  .1048(2)  .3610(2) -0.4015(2)  .0270(10)
O(11')  -.0590(2)  .3588(2) -0.51620(10)
                                        .0500(10)
O(12')  .2969(2)  .3290(2) -0.39460(10)
                                       .0380(10)
C(2')  .0716(2)  .4078(2) -0.2529(2)  .0240(10)
O(21')  .2753(2)  .42540(10)
                           -0.13770(10)
                                       .0310(10)
C(3')  -.0698(2)  .2957(2) -0.2043(2)  .0220(10)
O(31')  .0288(2)  .15560(10)
                           -0.18690(10)
                                       .0300(10)
C(4') -0.1082(2)  .3450(2)  -.05790(10)
                                       .0220(10)
O(41') -0.2368(2)  .45010(10)
                             -.06650(10)
                                        .0310(10)
O(42')  -.0096(2)  .27440(10)
                             .05890(10)
                                       .0310(10)
H(1A) -0.6757  .5486 -0.6383  .0350(10)
H(1B) -0.4381  .4765 -0.5618  .0350(10)
H(2B) -0.6344  .5286 -0.8788  .0340(10)
H(2A) -0.4317  .6135 -0.7826  .0340(10)
H(3B) -0.2286  .4135 -0.7206  .0290(10)
H(3A) -0.3108  .4349 -0.9018  .0290(10)
H(4B) -0.5806  .2578 -0.9184  .0320(10)
H(4A) -0.3297  .1827 -0.8419  .0320(10)
H(5B) -0.3884  .2088 -0.6027  .0340(10)
H(5A) -0.5932  .1233 -0.7190  .0340(10)
H(6B) -0.8010  .3295 -0.7600  .0340(10)
H(6A) -0.7118  .3106 -0.5993  .0340(10)
H(2') -0.0095  .5092 -0.2791  .0290(10)
H(21')  .3846  .4043 -0.1585  .0370(10)
H(3') -0.2221  .2858 -0.2799  .0260(10)
H(31')  .0656  .1400 -0.1003  .0360(10)