data_2005104
_journal_name_full  'Acta Crystallographica'
_journal_year      1996
_journal_volume    'C52'
_journal_page_first     1668
_journal_page_last     1670
_publ_section_title
;
Trimethyl[3-(triphenylstannyl)propyl]ammonium Iodide
;
_chemical_formula_moiety     'C24 H30 N Sn , I'
_chemical_formula_sum     'C24 H30 I N Sn'
_chemical_formula_weight     578.11
_symmetry_cell_setting    'monoclinic'
loop_
_symmetry_equiv_pos_as_xyz
'x,y,z'
'-x,-y,-z'
'1/2+x,1/2-y,z'
'-1/2-x,-1/2+y,-z'
_symmetry_space_group_name_H-M     'P 21/a'
_cell_length_a     18.678(9)
_cell_length_b     7.627(3)
_cell_length_c     19.099(10)
_cell_angle_alpha     90
_cell_angle_beta     116.60(4)
_cell_angle_gamma     90
_cell_volume     2433(2)
_cell_formula_units_Z     4
_exptl_crystal_density_diffrn     1.578
_cell_measurement_temperature     198
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_u_iso_or_equiv
Sn .20840(3) .16258(6) .19310(3) .0408(2)
I .41694(3)
           -0.86743(6) .56221(3) .0550(2)
C1 .2073(5) .0142(10) .2880(5) .056(2)
C2 .2594(5)
           -0.1523(9) .3147(4) .053(2)
C3 .2684(4)
           -0.1995(9) .3950(4) .037(2)
N .3165(3)
          -0.3621(6) .4326(3) .0390(10)
C4 .3225(4)
           -0.3730(10) .5135(4) .049(2)
C5 .3991(4)
           -0.3510(12) .4396(6) .066(3)
C6 .2747(5)
           -0.5219(10) .3886(5) .060(3)
C7 .0809(5) .3843(11) .2119(5) .066(3)
C8 .0290(6) .5216(16) .2003(6) .100(5)
C9 .0121(7) .6336(13) .1401(7) .095(4)
C10 .0482(6) .6144(12) .0931(7) .089(4)
C11 .1021(5) .4796(11) .1068(5) .065(3)
C12 .1195(4) .3624(9) .1661(4) .043(2)
C13 .3922(5) .2160(11) .2868(5) .071(3)
C14 .4643(5) .3044(13) .3142(6) .084(3)
C15 .4687(5) .4671(13) .2896(6) .070(3)
C16 .3993(5) .5446(12) .2367(5) .069(3)
C17 .3270(5) .4571(11) .2092(5) .061(3)
C18 .3222(4) .2910(9) .2343(4) .043(2)
C19 .1135(5) .0118(11) .0250(5) .057(2)
C20 .0998(6) -.0910(13) -.0378(5) .079(3)
C21 .1587(8)
            -0.2016(14) -.0362(6) .088(4)
C22 .2305(7)
            -0.2102(13) .0286(7) .086(4)
C23 .2446(5)
            -0.1058(11) .0921(5) .069(3)
C24 .1868(4) .0066(9) .0928(4) .047(2)
H1A .1535
         -0.0204 .2728 ?
H1B .2245 .0903 .3320 ?
H2A .3105
         -0.1302 .3171 ?
H2B .2341
         -0.2454 .2791 ?
H3A .2935
         -0.1034 .4288 ?
H3B .2162
         -0.2158 .3908 ?
H4A .2713
         -0.3705 .5128 ?
H4B .3518
         -0.2714 .5394 ?
H4C .3506
         -0.4748 .5405 ?
H5A .3945
         -0.3467 .3881 ?
H5B .4284
         -0.4526 .4656 ?
H5C .4264
         -0.2494 .4677 ?
H6A .2670
         -0.5173 .3360 ?
H6B .2242
         -0.5248 .3892 ?
H6C .3042
         -0.6243 .4132 ?
H7 .0903 .3027 .2527 ?
H8 .0051 .5377 .2345 ?
H9
  -0.0253 .7258 .1307 ?
H10 .0366 .6935 .0510 ?
H11 .1277 .4680 .0738 ?
H13 .3912 .1004 .3050 ?
H14 .5118 .2489 .3512 ?
H15 .5185 .5267 .3082 ?
H16 .4008 .6601 .2188 ?
H17 .2798 .5130 .1721 ?
H19 .0726 .0886 .0230 ?
H20 .0495
         -0.0864
                -0.0830 ?
H21 .1492
         -0.2722
                -0.0805 ?
H22 .2707
         -0.2882 .0299 ?
H23 .2954
         -0.1110 .1367 ?