#------------------------------------------------------------------------------ #$Date: 2016-04-02 18:31:43 +0100 (Sat, 02 Apr 2016) $ #$Revision: 180731 $ #$URL: svn://www.crystallography.net/cod/hkl/2/00/51/2005121.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2005121_Fobs loop_ _publ_author_name 'Roszak, A. W.' 'Clement, O.' 'Buncel, E.' _publ_section_title ; 2,2':6',2''-Terpyridine(1-methylimidazole-N^3^)platinum(II) Perchlorate Acetonitrile Solvate ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1645 _journal_page_last 1648 _journal_volume 52 _journal_year 1996 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _exptl_crystal_F_000 1456.00 _cod_data_source_file fg1115sup2.hkl _cod_data_source_block bun2 #BEGIN Tags that were not found in dictionaries: _shelx_title 'BUN2: [Pt(tpy)(MeIm)](ClO4)2.CH3CN, P2(1)/c, Z=4, 14Aug95' _shelx_refln_list_code 4 _shelx_f_calc_maximum 699.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 11759.03 11654.95 452.98 o 2 0 0 90824.98 82123.24 2962.77 o 3 0 0 6332.11 5385.95 282.74 o 4 0 0 7868.93 8067.97 308.62 o 5 0 0 25300.26 25013.29 831.29 o 6 0 0 19317.39 18611.88 526.65 o 7 0 0 23356.74 20566.15 633.17 o 8 0 0 9105.23 8338.76 191.15 o 9 0 0 14366.36 14506.22 246.90 o 10 0 0 4.24 25.88 25.88 o 11 0 0 10320.12 10343.81 198.12 o 12 0 0 1391.12 1523.20 83.63 o 13 0 0 6195.23 6152.52 140.37 o 14 0 0 360.53 318.58 85.62 o 15 0 0 2517.83 2448.07 105.53 o 16 0 0 1467.34 1564.02 100.55 o 17 0 0 447.98 323.56 159.29 o 18 0 0 1071.34 1057.28 109.51 o 19 0 0 49.15 53.76 59.73 o 1 1 0 76662.30 76741.28 1840.78 o 2 1 0 29878.75 33333.14 815.36 o 3 1 0 134653.41 136475.52 3248.49 o 4 1 0 34396.00 33387.89 827.31 o 5 1 0 13152.83 12162.68 320.57 o 6 1 0 15223.61 17863.22 462.93 o 7 1 0 5761.13 6411.37 173.23 o 8 1 0 25551.04 25934.18 642.13 o 9 1 0 409.18 160.28 140.37 o 10 1 0 16932.74 16944.33 409.17 o 11 1 0 6.40 2.99 62.72 o 12 1 0 5636.19 5730.41 190.15 o 13 1 0 936.79 1042.34 115.48 o 14 1 0 3454.46 4053.90 172.23 o 15 1 0 2179.27 2599.39 153.32 o 16 1 0 710.43 452.98 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281.74 244.91 o 4 12 0 526.07 726.75 139.38 o 5 12 0 796.54 867.13 146.35 o 6 12 0 189.98 48.78 73.67 o 7 12 0 748.09 919.89 152.32 o 8 12 0 52.76 143.36 168.25 o 9 12 0 444.33 586.38 158.29 o 10 12 0 0.20 75.66 104.53 o 1 13 0 1004.69 1281.28 153.32 o 2 13 0 75.50 70.68 99.56 o 3 13 0 817.07 1036.37 155.31 o 4 13 0 397.24 328.53 287.72 o 5 13 0 295.74 204.09 161.28 o 6 13 0 520.92 907.95 158.29 o 7 13 0 96.14 47.79 71.68 o 8 13 0 714.89 1144.89 166.26 o 0 14 0 1308.21 1366.90 171.24 o 1 14 0 10.02 118.47 154.31 o 2 14 0 843.79 1389.79 168.25 o 3 14 0 73.03 249.88 264.82 o 4 14 0 629.45 353.42 314.60 o 5 14 0 331.60 194.13 220.02 o -19 1 1 26.49 42.81 72.68 o -18 1 1 26.08 194.13 140.37 o -17 1 1 111.00 244.91 232.96 o -16 1 1 12.88 78.65 108.52 o -15 1 1 292.24 379.31 105.53 o -14 1 1 87.30 215.04 192.14 o -13 1 1 1037.30 866.13 103.54 o -12 1 1 152.52 71.68 87.61 o -11 1 1 566.38 485.83 79.64 o -10 1 1 4.66 3.98 96.57 o -9 1 1 226.16 275.77 60.73 o -8 1 1 969.41 846.22 61.72 o -7 1 1 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