data_2005146
_journal_name_full  'Acta Crystallographica'
_journal_year      1996
_journal_volume    'C52'
_journal_page_first     1661
_journal_page_last     1663
_publ_section_title
;
(5-Benzyldibenzo[b,d]phosphole 5-oxide)trimethylindium
;
_chemical_formula_iupac     '[In (C H3)3 (C19 H15 O P)]'
_chemical_formula_sum     'C22 H24 In O P'
_chemical_formula_weight     450.22
_symmetry_cell_setting    'triclinic'
loop_
_symmetry_equiv_pos_as_xyz
'x,y,z'
'-x,-y,-z'
_symmetry_space_group_name_H-M     'P -1'
_cell_length_a     9.089(2)
_cell_length_b     9.418(3)
_cell_length_c     12.575(8)
_cell_angle_alpha     89.45(4)
_cell_angle_beta     105.25(3)
_cell_angle_gamma     91.85(2)
_cell_volume     1038.0(8)
_cell_formula_units_Z     2
_exptl_crystal_density_diffrn     1.44
_cell_measurement_temperature     296
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_B_iso_or_equiv
In 1.01482(3)  .15638(3)  .13305(2) 3.99(2)
P  .84010(10)
             .40130(10)
                       .26165(7) 3.07(3)
O  .9748(3)  .3312(3)  .2433(2) 4.20(10)
C(1)  .8767(4)  .5646(4)  .3375(3) 3.30(10)
C(2)  .9508(5)  .6873(4)  .3163(3) 4.3(2)
C(3)  .9565(6)  .8041(5)  .3826(4) 5.3(2)
C(4)  .8918(6)  .7971(5)  .4698(4) 5.5(2)
C(5)  .8158(6)  .6743(5)  .4911(3) 4.7(2)
C(6)  .8082(4)  .5559(4)  .4256(3) 3.30(10)
C(7)  .7367(4)  .4159(4)  .4355(3) 3.60(10)
C(8)  .6629(5)  .3751(5)  .5158(3) 5.1(2)
C(9)  .6065(6)  .2379(6)  .5157(4) 6.1(2)
C(10)  .6204(6)  .1411(5)  .4380(4) 5.9(2)
C(11)  .6915(5)  .1806(5)  .3571(4) 4.8(2)
C(12)  .7468(4)  .3183(4)  .3569(3) 3.40(10)
C(13)  .6972(4)  .4348(4)  .1331(3) 3.70(10)
C(14)  .5699(4)  .5207(4)  .1488(3) 3.40(10)
C(15)  .4430(5)  .4572(5)  .1731(3) 4.5(2)
C(16)  .3291(5)  .5392(7)  .1914(4) 5.9(2)
C(17)  .3390(6)  .6834(7)  .1854(5) 6.4(2)
C(18)  .4625(6)  .7473(5)  .1607(5) 6.0(2)
C(19)  .5766(5)  .6656(4)  .1410(3) 4.4(2)
C(20)  .7997(6)  .0373(5)  .1023(4) 5.8(2)
C(21) 1.2176(6)  .0777(6)  .2467(5) 6.3(2)
C(22) 1.0507(6)  .2870(6)  -.0004(4) 5.7(2)
H(1)  .9974  .6913  .2570 5.1
H(2) 1.0053  .8899  .3678 6.3
H(3)  .8993  .8774  .5162 6.6
H(4)  .7692  .6717  .5505 5.6
H(5)  .6518  .4411  .5696 6.1
H(6)  .5569  .2093  .5705 7.4
H(7)  .5810  .0467  .4399 7.1
H(8)  .7019  .1145  .3031 5.8
H(9)  .7451  .4845  .0845 4.4
H(10)  .6563  .3463  .1013 4.4
H(11)  .4343  .3566  .1771 5.3
H(12)  .2428  .4946  .2085 7.1
H(13)  .2602  .7393  .1983 7.7
H(14)  .4704  .8480  .1571 7.2
H(15)  .6609  .7110  .1218 5.3
H(16)  .7188  .0969  .0671 7.0
H(17)  .8017 -0.0415  .0561 7.0
H(18)  .7842  .0041  .1703 7.0
H(19) 1.1941  .0477  .3129 7.5
H(20) 1.2534 -0.0004  .2145 7.5
H(21) 1.2943  .1511  .2628 7.5
H(22) 1.1355  .3504  .0267 6.8
H(23) 1.0704  .2282 -0.0557 6.8
H(24)  .9622  .3398 -0.0308 6.8