#------------------------------------------------------------------------------
#$Date: 2009-11-14 13:09:05 +0000 (Sat, 14 Nov 2009) $
#$Revision: 846 $
#$URL: svn://www.crystallography.net/cod/cif/2/2005469.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2005469
_journal_name_full               'Acta Crystallographica C'
_journal_volume                  52
_journal_year       1996
_journal_page_first    	2561
_journal_page_last    	2563
_publ_section_title
;
rel-(1R,6S,7S,8R,9S)-9-Methyl-8-phenyl-6-
[(1S, 2R)-(2-phenylcyclohexyl)oxy]-4-aza-3,5-dioxatricyclo[5.2.1.0^4,9^]decane
;
_chemical_formula_moiety    	'C26 H31 N O3'
_chemical_formula_sum    	'C26 H31 N O3'
_chemical_formula_structural    	'C26 H31 N O3'
_chemical_formula_analytical    	'C26 H31 N O3'
_chemical_formula_weight    	405.52
_symmetry_cell_setting    	triclinic
loop_
_symmetry_equiv_pos_as_xyz
    'x, y, z'
    '-x, -y, -z'
_symmetry_space_group_name_H-M    	'P-1'
_cell_length_a    	9.8583(3)
_cell_length_b    	10.76310(10)
_cell_length_c    	11.3841(3)
_cell_angle_alpha    	64.636(2)
_cell_angle_beta    	84.154(2)
_cell_angle_gamma    	83.762(2)
_cell_volume    	1082.96(4)
_cell_formula_units_Z    	2
_exptl_crystal_density_diffrn    	1.244
_cell_measurement_temperature    	198(2)
loop_
_atom_site_label
_atom_site_occupancy
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
    N 1 -0.1928(2) -0.9614(2) -0.18496(14) 0.0389(4)
    O1 1 -0.09332(14) -1.06328(14) -0.11524(12) 0.0505(4)
    O2 1 -0.18825(12) -0.86268(14) -0.12362(11) 0.0392(3)
    O3 1 -0.34653(11) -0.67515(13) -0.23103(11) 0.0350(3)
    C1 1 -0.1260(2) -0.9053(2) -0.3214(2) 0.0334(4)
    C2 1 0.0428(2) -1.0128(2) -0.1654(2) 0.0540(6)
    H2A 1 0.1067(2) -1.0864(2) -0.1739(2) 0.065
    H2B 1 0.0803(2) -0.9810(2) -0.1063(2) 0.065
    C3 1 0.0220(2) -0.8936(2) -0.2978(2) 0.0393(5)
    H3 1 0.0875(2) -0.9047(2) -0.3663(2) 0.047
    C4 1 0.0213(2) -0.7475(2) -0.3035(2) 0.0429(5)
    H4A 1 0.0875(2) -0.6923(2) -0.3731(2) 0.052
    H4B 1 0.0458(2) -0.7524(2) -0.2194(2) 0.052
    C5 1 -0.1262(2) -0.6825(2) -0.3331(2) 0.0338(4)
    H5 1 -0.1291(2) -0.5806(2) -0.3867(2) 0.041
    C6 1 -0.1849(2) -0.7582(2) -0.4017(2) 0.0297(4)
    H6 1 -0.2867(2) -0.7548(2) -0.3861(2) 0.036
    C7 1 -0.2086(2) -0.7209(2) -0.2039(2) 0.0367(5)
    H7 1 -0.1759(2) -0.6691(2) -0.1586(2) 0.044
    C8 1 -0.1478(2) -1.0105(2) -0.3721(2) 0.0483(5)
    H8A 1 -0.1118(11) -0.9785(6) -0.4629(4) 0.058
    H8B 1 -0.2458(2) -1.0222(9) -0.3669(11) 0.058
    H8C 1 -0.0999(10) -1.0989(4) -0.3191(7) 0.058
    C9 1 -0.1498(2) -0.7084(2) -0.5469(2) 0.0330(4)
    C10 1 -0.2441(2) -0.7189(2) -0.6238(2) 0.0469(5)
    H10 1 -0.3298(2) -0.7540(2) -0.5851(2) 0.056
    C11 1 -0.2158(2) -0.6794(3) -0.7557(2) 0.0603(6)
    H11 1 -0.2818(2) -0.6887(3) -0.8062(2) 0.072
    C12 1 -0.0936(3) -0.6268(2) -0.8147(2) 0.0586(6)
    H12 1 -0.0745(3) -0.6001(2) -0.9054(2) 0.070
    C13 1 0.0007(2) -0.6132(2) -0.7413(2) 0.0537(6)
    H13 1 0.0853(2) -0.5760(2) -0.7813(2) 0.064
    C14 1 -0.0272(2) -0.6538(2) -0.6086(2) 0.0434(5)
    H14 1 0.0392(2) -0.6439(2) -0.5588(2) 0.052
    C15 1 -0.4478(2) -0.7309(2) -0.1256(2) 0.0343(4)
    H15 1 -0.4383(2) -0.8338(2) -0.0900(2) 0.041
    C16 1 -0.5853(2) -0.6788(2) -0.1869(2) 0.0332(4)
    H16 1 -0.5898(2) -0.5758(2) -0.2272(2) 0.040
    C17 1 -0.7023(2) -0.7240(2) -0.0812(2) 0.0434(5)
    H17A 1 -0.7902(2) -0.6824(2) -0.1212(2) 0.052
    H17B 1 -0.7046(2) -0.8255(2) -0.0445(2) 0.052
    C18 1 -0.6873(2) -0.6818(2) 0.0287(2) 0.0453(5)
    H18A 1 -0.6957(2) -0.5800(2) -0.0057(2) 0.054
    H18B 1 -0.7616(2) -0.7182(2) 0.0969(2) 0.054
    C19 1 -0.5507(2) -0.7362(2) 0.0877(2) 0.0498(6)
    H19A 1 -0.5460(2) -0.8382(2) 0.1303(2) 0.060
    H19B 1 -0.5413(2) -0.7030(2) 0.1551(2) 0.060
    C20 1 -0.4333(2) -0.6884(2) -0.0168(2) 0.0443(5)
    H20A 1 -0.4326(2) -0.5868(2) -0.0532(2) 0.053
    H20B 1 -0.3452(2) -0.7290(2) 0.0233(2) 0.053
    C21 1 -0.5993(2) -0.7238(2) -0.2942(2) 0.0326(4)
    C22 1 -0.6178(2) -0.6277(2) -0.4212(2) 0.0366(4)
    H22 1 -0.6224(2) -0.5323(2) -0.4409(2) 0.044
    C23 1 -0.6299(2) -0.6678(2) -0.5198(2) 0.0454(5)
    H23 1 -0.6425(2) -0.6000(2) -0.6060(2) 0.054
    C24 1 -0.6237(2) -0.8054(2) -0.4934(2) 0.0487(5)
    H24 1 -0.6315(2) -0.8330(2) -0.5612(2) 0.058
    C25 1 -0.6062(2) -0.9034(2) -0.3676(2) 0.0515(6)
    H25 1 -0.6022(2) -0.9987(2) -0.3485(2) 0.062
    C26 1 -0.5944(2) -0.8622(2) -0.2693(2) 0.0441(5)
    H26 1 -0.5828(2) -0.9302(2) -0.1830(2) 0.053