data_2005481
_journal_name_full  'Acta Crystallographica'
_journal_year       1996
_journal_volume    	C52
_journal_page_first    	2436
_journal_page_last    	2439
_publ_section_title    	
;
Aquabis(p-nitrosalicylato-O,O')lead(II)
;
_chemical_formula_iupac    	'[Pb (C7 H4 N O5)2 (H2 O)]'
_chemical_formula_moiety    	'C14 H8 N2 O10 Pb , H2 O'
_chemical_formula_sum    	'C14 H10 N2 O11 Pb'
_chemical_formula_weight    	589.433
_symmetry_cell_setting    	triclinic
loop_
_symmetry_equiv_pos_as_xyz
    'x,y,z'
    '-x,-y,-z'
_symmetry_space_group_name_H-M    	'P -1'
_cell_length_a    	4.8797(11)
_cell_length_b    	12.1550(10)
_cell_length_c    	14.7338(16)
_cell_angle_alpha    	68.364(10)
_cell_angle_beta    	86.482(12)
_cell_angle_gamma    	78.770(11)
_cell_volume    	796.68(19)
_cell_formula_units_Z    	2
_exptl_crystal_density_diffrn    	2.457
_cell_measurement_temperature    	295
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_B_iso_or_equiv
    Pb 0.35950(6) 0.37081(2) 0.32420(2) 2.204(4)
    O1 -0.0242(9) 0.5389(4) 0.3134(3) 2.61(9)
    O2 0.2808(9) 0.5216(4) 0.4229(3) 2.9(1)
    O3 -0.6471(12) 1.0940(5) 0.3274(4) 5.0(2)
    O4 -0.3232(12) 1.0801(4) 0.4265(4) 4.2(1)
    O5 0.2351(10) 0.6750(4) 0.5077(3) 3.3(1)
    O6 0.2464(10) 0.3930(4) 0.1594(3) 3.1(1)
    O7 -0.0837(10) 0.3143(4) 0.2579(3) 3.1(1)
    O8 -0.3967(17) 0.0829(6) -0.0777(5) 11.2(2)
    O9 -0.1169(13) 0.1690(5) -0.1737(4) 6.2(1)
    O10 0.2542(9) 0.4056(4) -0.0190(3) 3.2(1)
    O11 0.5198(9) 0.5505(4) 0.2170(3) 2.6(1)
    N1 -0.4430(10) 1.0381(5) 0.3791(4) 3.0(1)
    N2 -0.2222(13) 0.1432(5) -0.0970(4) 3.4(1)
    C1 -0.0838(12) 0.6914(5) 0.3817(4) 2.0(1)
    C2 0.0150(13) 0.7376(5) 0.4452(4) 2.2(1)
    C3 -0.1037(14) 0.8509(5) 0.4460(4) 2.4(1)
    C4 -0.3260(13) 0.9152(5) 0.3836(4) 2.3(1)
    C5 -0.4377(14) 0.8732(6) 0.3210(5) 2.8(1)
    C6 -0.3103(14) 0.7603(6) 0.3217(5) 2.7(1)
    C7 0.0674(13) 0.5763(5) 0.3733(4) 2.1(1)
    C8 -0.0238(13) 0.2860(5) 0.1061(4) 2.3(1)
    C9 0.0793(13) 0.3239(5) 0.0119(4) 2.4(1)
    C10 0.0125(14) 0.2768(6) -0.0546(4) 2.6(1)
    C11 -0.1525(15) 0.1915(6) -0.0242(5) 3.0(1)
    C12 -0.2603(15) 0.1489(6) 0.0688(5) 3.2(2)
    C13 -0.1935(15) 0.2006(6) 0.1322(5) 3.0(2)
    C14 0.0447(14) 0.3342(6) 0.1795(4) 2.6(1)
    H3 -0.028 0.886 0.493 3.3
    H5 -0.611 0.924 0.276 3.7
    H5' 0.273 0.613 0.495 4.3
    H6 -0.389 0.726 0.275 3.6
    H10 0.088 0.305 -0.126 3.5
    H10' 0.303 0.420 0.031 4.1
    H12 -0.383 0.082 0.090 4.1
    H13 -0.276 0.174 0.203 4.0
    H111 0.661 0.552 0.243 3.4
    H112 0.541 0.561 0.155 3.4