#------------------------------------------------------------------------------
#$Date: 2009-11-14 13:09:05 +0000 (Sat, 14 Nov 2009) $
#$Revision: 846 $
#$URL: svn://www.crystallography.net/cod/cif/2/2005536.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2005536
_journal_name_full               'Acta Crystallographica C'
_journal_volume                  52
_journal_year       1996
_journal_page_first    	2536
_journal_page_last    	2538
_publ_section_title
;
 Chiral Hydroxylamines. II. (1R,2R)-N-Benzyl-N-[(3-tert-butoxycarbonyl-2,2-
dimethyloxazol-4-yl)(furan-2-yl)methyl]hydroxylamine
;
_chemical_formula_sum    	'C22 H30 N2 O5'
_chemical_formula_weight    	402.48
_symmetry_cell_setting    	orthorhombic
loop_
_symmetry_equiv_pos_as_xyz
    'x, y, z'
    '-x+1/2, -y, z+1/2'
    '-x, y+1/2, -z+1/2'
    'x+1/2, -y+1/2, -z'
_symmetry_space_group_name_H-M    	'P 21 21 21'
_cell_length_a    	12.3140(10)
_cell_length_b    	12.4250(10)
_cell_length_c    	14.855(5)
_cell_angle_alpha    	90.00
_cell_angle_beta    	90.00
_cell_angle_gamma    	90.00
_cell_volume    	2272.8(8)
_cell_formula_units_Z    	4
_exptl_crystal_density_diffrn    	1.176
_cell_measurement_temperature    	293(2)
loop_
_atom_site_label
_atom_site_occupancy
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
    O1 1 0.5478(2) 0.1710(2) 0.8350(2) 0.0817(7)
    C1 1 0.5119(2) 0.2392(2) 0.7693(2) 0.0558(7)
    C2 1 0.5968(3) 0.2740(4) 0.7225(2) 0.0924(12)
    H2 1 0.5957(3) 0.3227(4) 0.6750(2) 0.095(2)
    C3 1 0.6913(3) 0.2213(4) 0.7601(2) 0.0841(10)
    H3 1 0.7626(3) 0.2285(4) 0.7404(2) 0.095(2)
    C4 1 0.6577(3) 0.1625(3) 0.8261(3) 0.0850(10)
    H4 1 0.7022(3) 0.1204(3) 0.8624(3) 0.095(2)
    C16 1 0.3495(2) 0.1039(2) 0.6689(2) 0.0613(7)
    H16A 1 0.3395(2) 0.0656(2) 0.7252(2) 0.095(2)
    H16B 1 0.4228(2) 0.0900(2) 0.6480(2) 0.095(2)
    C17 1 0.2701(2) 0.0612(2) 0.6007(2) 0.0552(7)
    C18 1 0.1887(2) 0.1237(2) 0.5656(2) 0.0669(8)
    H18 1 0.1832(2) 0.1955(2) 0.5826(2) 0.095(2)
    C19 1 0.1141(3) 0.0811(3) 0.5050(2) 0.0815(9)
    H19 1 0.0599(3) 0.1245(3) 0.4810(2) 0.095(2)
    C20 1 0.1209(3) -0.0252(3) 0.4806(2) 0.0905(11)
    H20 1 0.0707(3) -0.0541(3) 0.4406(2) 0.095(2)
    C21 1 0.2012(3) -0.0886(3) 0.5152(3) 0.0918(11)
    H21 1 0.2058(3) -0.1605(3) 0.4983(3) 0.095(2)
    C22 1 0.2756(3) -0.0466(2) 0.5749(2) 0.0734(9)
    H22 1 0.3298(3) -0.0905(2) 0.5983(2) 0.095(2)
    O4 1 0.30016(15) 0.3757(2) 0.92914(11) 0.0639(5)
    C7 1 0.3921(2) 0.4101(3) 0.8787(2) 0.0640(7)
    H7A 1 0.4577(2) 0.3744(3) 0.8990(2) 0.095(2)
    H7B 1 0.4019(2) 0.4873(3) 0.8831(2) 0.095(2)
    C6 1 0.3634(2) 0.3769(2) 0.7830(2) 0.0527(6)
    H6 1 0.3998(2) 0.4233(2) 0.7391(2) 0.095(2)
    N2 1 0.2461(2) 0.3970(2) 0.78406(13) 0.0511(5)
    C8 1 0.2049(2) 0.4033(2) 0.8790(2) 0.0561(7)
    C9 1 0.1213(2) 0.3179(3) 0.8993(2) 0.0715(8)
    H9A 1 0.0557(2) 0.3333(3) 0.8669(2) 0.095(2)
    H9B 1 0.1064(2) 0.3172(3) 0.9628(2) 0.095(2)
    H9C 1 0.1486(2) 0.2488(3) 0.8812(2) 0.095(2)
    C10 1 0.1682(3) 0.5158(3) 0.9039(2) 0.0763(9)
    H10A 1 0.1043(3) 0.5339(3) 0.8701(2) 0.095(2)
    H10B 1 0.2249(3) 0.5662(3) 0.8903(2) 0.095(2)
    H10C 1 0.1521(3) 0.5186(3) 0.9671(2) 0.095(2)
    C11 1 0.1896(2) 0.4182(2) 0.7082(2) 0.0514(6)
    O3 1 0.2289(2) 0.4235(2) 0.63310(11) 0.0577(5)
    O2 1 0.08402(14) 0.4342(2) 0.72687(12) 0.0659(5)
    C12 1 0.0040(2) 0.4602(3) 0.6563(2) 0.0699(8)
    C13 1 0.0355(3) 0.5660(3) 0.6125(2) 0.0954(12)
    H13A 1 0.0400(3) 0.6212(3) 0.6576(2) 0.095(2)
    H13B 1 -0.0182(3) 0.5855(3) 0.5686(2) 0.095(2)
    H13C 1 0.1048(3) 0.5583(3) 0.5835(2) 0.095(2)
    C14 1 -0.0994(3) 0.4740(4) 0.7101(3) 0.1051(14)
    H14A 1 -0.0907(3) 0.5323(4) 0.7519(3) 0.095(2)
    H14B 1 -0.1146(3) 0.4089(4) 0.7425(3) 0.095(2)
    H14C 1 -0.1585(3) 0.4896(4) 0.6700(3) 0.095(2)
    C15 1 -0.0045(3) 0.3703(4) 0.5898(3) 0.118(2)
    H15A 1 0.0625(3) 0.3642(4) 0.5572(3) 0.095(2)
    H15B 1 -0.0626(3) 0.3849(4) 0.5485(3) 0.095(2)
    H15C 1 -0.0188(3) 0.3042(4) 0.6210(3) 0.095(2)
    O5 1 0.3875(2) 0.2722(2) 0.60851(11) 0.0607(5)
    N1 1 0.3369(2) 0.2192(2) 0.68500(13) 0.0516(5)
    C5 1 0.3912(2) 0.2576(2) 0.7663(2) 0.0507(6)
    H5 1 0.3602(2) 0.2171(2) 0.8167(2) 0.095(2)
    H(O) 1 0.3282(31) 0.3261(30) 0.6064(25) 0.096(12)