#------------------------------------------------------------------------------
#$Date: 2011-09-10 04:16:28 +0100 (Sat, 10 Sep 2011) $
#$Revision: 25271 $
#$URL: svn://www.crystallography.net/cod/cif/2/2006268.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2006268
loop_
_publ_author_name
'Suh, I.-H.'
'Choi, S.'
'Lewis, D. E.'
'Jensen, W. P.'
_publ_section_title
;
 Two Related Benzylcamphor Dimers
;
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              963
_journal_page_last               967
_journal_volume                  53
_journal_year                    1997
_chemical_formula_moiety         'C34 H42 O2'
_chemical_formula_sum            'C34 H42 O2'
_chemical_formula_weight         482.70
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           4
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_cell_angle_alpha                90.0
_cell_angle_beta                 101.012(17)
_cell_angle_gamma                90.0
_cell_formula_units_Z            2
_cell_length_a                   13.453(3)
_cell_length_b                   10.1847(16)
_cell_length_c                   10.2639(18)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293
_cell_measurement_theta_max      29.50
_cell_measurement_theta_min      25.00
_cell_volume                     1380.4(5)
_computing_data_reduction
'NRCVAX DATRD2 (Gabe, Le Page, Charland, Lee & White, 1989)'
_computing_molecular_graphics    NRCVAX
_computing_publication_material  'NRCVAX TABLES Jan 94 Version'
_computing_structure_refinement  'NRCVAX LSTSQ'
_computing_structure_solution    'NRCVAX SOLVER'
_diffrn_ambient_temperature      293
_diffrn_measurement_device       'Nonius CAD-4    '
_diffrn_measurement_method       \w
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'xray tube'
_diffrn_radiation_type           'Copper K\a'
_diffrn_radiation_wavelength     1.54056
_diffrn_reflns_av_R_equivalents  0.000
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       11
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            2040
_diffrn_reflns_theta_max         59.88
_diffrn_reflns_theta_min         0.00
_diffrn_standards_decay_%        2.2
_diffrn_standards_interval_time  180
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    0.50
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  1.0000
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.161
_exptl_crystal_description       prism
_exptl_crystal_F_000             525.34
_exptl_crystal_size_max          0.26
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.20
_refine_diff_density_max         0.24
_refine_diff_density_min         -0.30
_refine_ls_extinction_coef       '1.32(7) x 10^-6^'
_refine_ls_extinction_method     'Larson (1970)'
_refine_ls_goodness_of_fit_obs   7.32
_refine_ls_hydrogen_treatment    'H-atom parameters not refined'
_refine_ls_matrix_type           atomblock
_refine_ls_number_parameters     325
_refine_ls_number_reflns         1808
_refine_ls_R_factor_all          0.080
_refine_ls_R_factor_obs          0.080
_refine_ls_shift/esd_max         0.125
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      1/\s^2^(F)
_refine_ls_wR_factor_all         0.067
_refine_ls_wR_factor_obs         0.067
_reflns_number_observed          1808
_reflns_number_total             2040
_reflns_observed_criterion       'Inet > 3.0\s(Inet)'
_[local]_cod_data_source_file    bk1252.cif
_[local]_cod_data_source_block   2
_[local]_cod_cif_authors_sg_H-M  'P 21'
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_cell_volume        1380.4(4)
_cod_database_code               2006268
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
-x,1/2+y,-z
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
_atom_site_aniso_type_symbol
O1 0.050(5) 0.081(6) 0.043(4) -0.022(5) 0.001(3) -0.006(5) O
O2 0.088(6) 0.082(7) 0.033(4) -0.034(6) 0.010(4) -0.013(5) O
C1 0.066(7) 0.041(6) 0.029(5) -0.007(6) -0.001(5) 0.002(6) C
C2 0.041(6) 0.042(7) 0.030(5) -0.004(5) 0.001(4) -0.002(5) C
C3 0.050(7) 0.050(7) 0.025(5) -0.002(6) -0.006(5) 0.003(5) C
C4 0.043(7) 0.054(8) 0.022(5) -0.020(6) -0.002(5) -0.003(5) C
C5 0.061(7) 0.034(6) 0.031(5) -0.004(6) 0.003(5) -0.007(5) C
C6 0.064(8) 0.052(8) 0.038(6) 0.016(7) -0.013(5) 0.003(6) C
C7 0.086(9) 0.033(6) 0.031(6) 0.002(6) -0.007(5) 0.002(5) C
C8 0.064(7) 0.051(7) 0.016(4) -0.022(7) -0.003(4) -0.003(5) C
C9 0.053(6) 0.041(6) 0.028(5) 0.000(6) -0.007(4) -0.007(5) C
C10 0.058(7) 0.057(8) 0.035(6) 0.005(6) -0.017(5) -0.008(6) C
C11 0.072(8) 0.065(8) 0.038(6) -0.025(7) -0.023(5) -0.003(6) C
C12 0.078(8) 0.082(9) 0.022(5) 0.003(8) 0.015(5) -0.007(7) C
C13 0.054(6) 0.043(7) 0.029(5) -0.007(6) -0.008(5) -0.005(5) C
C14 0.027(5) 0.050(7) 0.034(6) -0.005(6) -0.007(4) 0.003(5) C
C15 0.036(6) 0.047(7) 0.047(6) -0.009(5) 0.005(5) -0.011(6) C
C16 0.044(6) 0.097(11) 0.034(6) 0.001(7) -0.012(5) -0.012(7) C
C17 0.058(8) 0.118(13) 0.081(9) -0.014(9) -0.021(7) -0.041(9) C
C18 0.071(8) 0.061(9) 0.054(7) -0.019(7) 0.020(6) 0.002(7) C
C19 0.106(10) 0.036(7) 0.053(7) -0.013(7) 0.009(7) -0.018(6) C
C20 0.22(2) 0.052(10) 0.074(10) 0.036(12) -0.026(11) -0.006(8) C
C21 0.150(14) 0.064(10) 0.071(9) -0.031(10) -0.005(9) -0.021(8) C
C22 0.098(10) 0.083(11) 0.038(6) -0.014(8) 0.009(6) -0.025(7) C
C23 0.049(7) 0.050(7) 0.026(5) 0.013(6) -0.011(5) -0.001(5) C
C24 0.061(8) 0.053(8) 0.044(6) -0.001(7) -0.013(6) 0.003(6) C
C25 0.113(11) 0.058(9) 0.025(6) 0.034(9) -0.019(6) 0.005(6) C
C26 0.092(10) 0.097(12) 0.037(7) 0.047(10) -0.020(7) -0.012(8) C
C27 0.063(8) 0.128(14) 0.049(7) 0.044(9) -0.013(6) -0.023(9) C
C28 0.069(8) 0.082(10) 0.039(6) 0.026(8) -0.002(6) -0.009(7) C
C29 0.055(7) 0.051(7) 0.023(5) -0.006(6) -0.011(5) 0.000(5) C
C30 0.051(6) 0.058(8) 0.029(5) 0.005(6) -0.015(5) 0.002(6) C
C31 0.133(11) 0.039(7) 0.036(6) 0.024(10) -0.007(7) 0.001(6) C
C32 0.093(10) 0.077(10) 0.037(7) 0.041(10) -0.020(7) -0.012(8) C
C33 0.073(9) 0.110(12) 0.038(7) 0.018(10) 0.003(6) -0.030(8) C
C34 0.044(6) 0.083(9) 0.030(6) 0.006(7) 0.004(5) -0.008(6) C
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_thermal_displace_type
_atom_site_type_symbol
O1 0.1687(5) 0.75770 0.2636(6) 0.059(5) Uij O
O2 0.3309(6) 0.6787(9) -0.2628(6) 0.068(5) Uij O
C1 0.1915(8) 0.6782(14) -0.0440(8) 0.046(6) Uij C
C2 0.2938(7) 0.7434(13) 0.0314(8) 0.038(6) Uij C
C3 0.2749(7) 0.8583(13) 0.1195(9) 0.043(6) Uij C
C4 0.2274(8) 0.8419(14) 0.2441(9) 0.041(6) Uij C
C5 0.2683(7) 0.9554(13) 0.3336(8) 0.043(6) Uij C
C6 0.2263(8) 1.0809(15) 0.2544(10) 0.055(7) Uij C
C7 0.2984(8) 1.0914(13) 0.1507(9) 0.053(7) Uij C
C8 0.3543(7) 0.9644(15) 0.1657(8) 0.045(6) Uij C
C9 0.3796(7) 0.9495(14) 0.3233(8) 0.043(6) Uij C
C10 0.4345(8) 0.8227(14) 0.3745(9) 0.053(7) Uij C
C11 0.4440(8) 1.0636(15) 0.3906(9) 0.063(7) Uij C
C12 0.2428(8) 0.9473(16) 0.4748(8) 0.060(8) Uij C
C13 0.2141(7) 0.5721(14) -0.1423(9) 0.044(6) Uij C
C14 0.2615(7) 0.6048(14) -0.2592(9) 0.039(6) Uij C
C15 0.2097(7) 0.5186(13) -0.3736(9) 0.044(6) Uij C
C16 0.1071(8) 0.5916(15) -0.4130(9) 0.061(8) Uij C
C17 0.0474(8) 0.5549(18) -0.3055(12) 0.090(9) Uij C
C18 0.1284(9) 0.4770(16) -0.2044(11) 0.061(8) Uij C
C19 0.1825(10) 0.4011(14) -0.3029(11) 0.066(8) Uij C
C20 0.2719(14) 0.3223(17) -0.2348(14) 0.124(14) Uij C
C21 0.1022(11) 0.3066(16) -0.3936(12) 0.098(11) Uij C
C22 0.2658(9) 0.5031(15) -0.4870(9) 0.074(8) Uij C
C23 0.1188(7) 0.7847(14) -0.1037(9) 0.044(6) Uij C
C24 0.1411(8) 0.8741(14) -0.1985(10) 0.056(7) Uij C
C25 0.0754(10) 0.9715(16) -0.2506(9) 0.070(8) Uij C
C26 -0.0192(10) 0.9760(18) -0.2140(10) 0.080(10) Uij C
C27 -0.0425(9) 0.8883(19) -0.1214(11) 0.083(10) Uij C
C28 0.0240(9) 0.7928(15) -0.0652(9) 0.065(8) Uij C
C29 0.3672(8) 0.6376(14) 0.0968(9) 0.045(6) Uij C
C30 0.3382(8) 0.5414(15) 0.1806(9) 0.049(6) Uij C
C31 0.4098(11) 0.4487(16) 0.2378(10) 0.073(9) Uij C
C32 0.5031(10) 0.4442(18) 0.2137(10) 0.073(9) Uij C
C33 0.5359(9) 0.5412(19) 0.1335(10) 0.075(9) Uij C
C34 0.4635(8) 0.6355(15) 0.0741(9) 0.053(7) Uij C
H1 0.161 0.632 0.033 0.06(2) Uiso H
H2 0.329 0.787 -0.046 0.05(5) Uiso H
H3 0.217 0.915 0.054 0.05(5) Uiso H
H6A 0.233 1.168 0.316 0.06(4) Uiso H
H6B 0.149 1.072 0.203 0.06(2) Uiso H
H7A 0.348 1.176 0.176 0.06(3) Uiso H
H7B 0.255 1.110 0.052 0.06(5) Uiso H
H8 0.420 0.963 0.121 0.06(2) Uiso H
H10A 0.505 0.813 0.338 0.06(3) Uiso H
H10B 0.447 0.831 0.481 0.06(4) Uiso H
H10C 0.390 0.738 0.338 0.06(6) Uiso H
H11A 0.502 1.094 0.337 0.07(5) Uiso H
H11B 0.471 1.050 0.497 0.07(12) Uiso H
H11C 0.389 1.144 0.365 0.07(5) Uiso H
H12A 0.266 0.850 0.504 0.07(4) Uiso H
H12B 0.164 0.957 0.481 0.07(3) Uiso H
H12C 0.279 1.019 0.550 0.07(5) Uiso H
H13 0.266 0.507 -0.081 0.05(3) Uiso H
H16A 0.123 0.695 -0.421 0.07(3) Uiso H
H16B 0.069 0.567 -0.515 0.1(2) Uiso H
H17A 0.023 0.651 -0.263 0.1(6) Uiso H
H17B -0.019 0.506 -0.350 0.10(5) Uiso H
H18 0.091 0.417 -0.141 0.07(7) Uiso H
H20A 0.334 0.382 -0.187 0.12(3) Uiso H
H20B 0.301 0.267 -0.313 0.1(2) Uiso H
H20C 0.249 0.251 -0.169 0.12(7) Uiso H
H21A 0.136 0.232 -0.448 0.10(18) Uiso H
H21B 0.047 0.361 -0.466 0.10(11) Uiso H
H21C 0.058 0.258 -0.332 0.10(6) Uiso H
H22A 0.273 0.607 -0.508 0.08(5) Uiso H
H22B 0.230 0.445 -0.571 0.08(4) Uiso H
H22C 0.341 0.463 -0.455 0.08(5) Uiso H
H24 0.212 0.866 -0.230 0.06(3) Uiso H
H25 0.091 1.044 -0.322 0.08(4) Uiso H
H26 -0.073 1.052 -0.254 0.09(3) Uiso H
H27 -0.116 0.889 -0.097 0.09(4) Uiso H
H28 0.005 0.722 0.003 0.07(4) Uiso H
H30 0.262 0.544 0.203 0.06(3) Uiso H
H31 0.388 0.380 0.307 0.08(3) Uiso H
H32 0.553 0.367 0.256 0.08(3) Uiso H
H33 0.612 0.537 0.113 0.08(3) Uiso H
H34 0.487 0.713 0.014 0.06(4) Uiso H
loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O 0.047 0.032 'International Tables Vol. IV Table 2.2B'
C 0.017 0.009 'International Tables Vol. IV Table 2.2B'
H 0.000 0.000 'International Tables Vol. IV Table 2.2B'
loop_
_diffrn_standard_refln_index_h
_diffrn_standard_refln_index_k
_diffrn_standard_refln_index_l
1,4,4 2,2,3 3,-5,3
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_publ_flag
C2 C1 C13 110.5(8) y
C2 C1 C23 109.3(10) y
C13 C1 C23 115.5(8) n
C1 C2 C3 112.4(8) y
C1 C2 C29 110.2(10) n
C3 C2 C29 116.5(7) n
C2 C3 C4 123.3(11) y
C2 C3 C8 122.5(9) y
C4 C3 C8 101.2(8) y
O1 C4 C3 127.0(10) y
O1 C4 C5 127.9(9) y
C3 C4 C5 105.1(9) y
C4 C5 C6 104.8(8) y
C4 C5 C9 100.1(9) y
C4 C5 C12 113.9(10) n
C6 C5 C9 105.1(9) y
C6 C5 C12 114.0(10) n
C9 C5 C12 117.2(7) n
C5 C6 C7 101.5(9) y
C6 C7 C8 103.6(9) y
C3 C8 C7 105.8(8) y
C3 C8 C9 104.3(9) y
C7 C8 C9 101.1(9) y
C5 C9 C8 92.6(7) y
C5 C9 C10 115.3(10) n
C5 C9 C11 114.7(10) n
C8 C9 C10 115.1(10) n
C8 C9 C11 112.2(10) n
C10 C9 C11 106.9(8) n
C1 C13 C14 122.2(11) y
C1 C13 C18 118.9(9) y
C14 C13 C18 101.9(8) y
O2 C14 C13 127.8(10) y
O2 C14 C15 125.4(9) y
C13 C14 C15 106.7(9) y
C14 C15 C16 100.2(9) y
C14 C15 C19 102.0(8) y
C14 C15 C22 115.5(9) n
C16 C15 C19 103.0(9) y
C16 C15 C22 113.5(9) n
C19 C15 C22 119.9(11) n
C15 C16 C17 104.9(10) y
C16 C17 C18 101.9(9) y
C13 C18 C17 109.0(12) y
C13 C18 C19 100.1(9) y
C17 C18 C19 99.9(9) y
C15 C19 C18 96.1(10) y
C15 C19 C20 114.1(12) n
C15 C19 C21 113.7(9) n
C18 C19 C20 113.2(10) n
C18 C19 C21 109.1(10) n
C20 C19 C21 109.9(12) n
C1 C23 C24 122.6(10) n
C1 C23 C28 118.7(11) n
C24 C23 C28 118.7(11) n
C23 C24 C25 122.2(11) n
C24 C25 C26 118.2(13) n
C25 C26 C27 120.2(12) n
C26 C27 C28 122.1(11) n
C23 C28 C27 118.5(12) n
C2 C29 C30 121.9(9) n
C2 C29 C34 119.5(11) n
C30 C29 C34 118.6(11) n
C29 C30 C31 118.6(11) n
C30 C31 C32 123.2(14) n
C31 C32 C33 119.8(13) n
C32 C33 C34 117.3(11) n
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_publ_flag
O1 C4 1.208(12) y
O2 C14 1.206(14) y
C1 C2 1.590(14) y
C1 C13 1.547(17) y
C1 C23 1.510(17) n
C2 C3 1.530(17) y
C2 C29 1.528(17) n
C3 C4 1.543(14) y
C3 C8 1.531(17) y
C4 C5 1.514(16) y
C5 C6 1.561(18) y
C5 C9 1.522(13) y
C5 C12 1.554(12) n
C6 C7 1.575(16) y
C7 C8 1.489(19) y
C8 C9 1.596(12) y
C9 C10 1.531(18) n
C9 C11 1.533(17) n
C13 C14 1.500(14) y
C13 C18 1.547(17) y
C14 C15 1.524(15) y
C15 C16 1.552(16) y
C15 C19 1.480(18) y
C15 C22 1.512(14) n
C16 C17 1.530(18) y
C17 C18 1.570(19) y
C18 C19 1.559(18) y
C19 C20 1.50(2) n
C19 C21 1.605(18) n
C23 C24 1.407(18) n
C23 C28 1.408(16) n
C24 C25 1.368(19) n
C25 C26 1.39(2) n
C26 C27 1.38(2) n
C27 C28 1.37(2) n
C29 C30 1.407(18) n
C29 C34 1.359(15) n
C30 C31 1.395(18) n
C31 C32 1.33(2) n
C32 C33 1.41(3) n
C33 C34 1.42(2) no
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
C13 C1 C2 C3 174.(2)
C13 C1 C2 C29 -53.9(13)
C23 C1 C2 C3 46.2(12)
C23 C1 C2 C29 178.(2)
C2 C1 C13 C14 -63.8(14)
C2 C1 C13 C18 168.(2)
C23 C1 C13 C14 60.9(14)
C23 C1 C13 C18 -67.8(15)
C2 C1 C23 C24 60.5(14)
C2 C1 C23 C28 -121.(2)
C13 C1 C23 C24 -64.7(15)
C13 C1 C23 C28 114.(2)
C1 C2 C3 C4 66.6(14)
C1 C2 C3 C8 -159.(2)
C29 C2 C3 C4 -62.0(14)
C29 C2 C3 C8 72.1(15)
C1 C2 C29 C30 -51.9(13)
C1 C2 C29 C34 128.(2)
C3 C2 C29 C30 77.7(16)
C3 C2 C29 C34 -102.3(19)
C2 C3 C4 O1 -28.5(10)
C2 C3 C4 C5 153.(2)
C8 C3 C4 O1 -170.(2)
C8 C3 C4 C5 11.0(10)
C2 C3 C8 C7 137.(2)
C2 C3 C8 C9 -116.6(19)
C4 C3 C8 C7 -80.6(16)
C4 C3 C8 C9 25.6(10)
O1 C4 C5 C6 -115.(2)
O1 C4 C5 C9 136.(2)
O1 C4 C5 C12 9.9(9)
C3 C4 C5 C6 63.2(14)
C3 C4 C5 C9 -45.4(12)
C3 C4 C5 C12 -172.(2)
C4 C5 C6 C7 -77.2(16)
C9 C5 C6 C7 27.9(11)
C12 C5 C6 C7 158.(2)
C4 C5 C9 C8 57.2(13)
C4 C5 C9 C10 -62.2(14)
C4 C5 C9 C11 173.(2)
C6 C5 C9 C8 -51.3(13)
C6 C5 C9 C10 -171.(2)
C6 C5 C9 C11 64.5(15)
C12 C5 C9 C8 -179.(2)
C12 C5 C9 C10 61.6(14)
C12 C5 C9 C11 -63.2(14)
C5 C6 C7 C8 10.4(10)
C6 C7 C8 C3 65.6(15)
C6 C7 C8 C9 -43.0(12)
C3 C8 C9 C5 -51.7(13)
C3 C8 C9 C10 67.8(15)
C3 C8 C9 C11 -170.(2)
C7 C8 C9 C5 58.0(14)
C7 C8 C9 C10 178.(2)
C7 C8 C9 C11 -60.1(14)
C1 C13 C14 O2 42.5(12)
C1 C13 C14 C15 -141.(2)
C18 C13 C14 O2 178.(2)
C18 C13 C14 C15 -5.8(10)
C1 C13 C18 C17 70.5(16)
C1 C13 C18 C19 175.(2)
C14 C13 C18 C17 -67.1(16)
C14 C13 C18 C19 37.2(12)
O2 C14 C15 C16 -108.(2)
O2 C14 C15 C19 146.(2)
O2 C14 C15 C22 14.6(11)
C13 C14 C15 C16 76.0(16)
C13 C14 C15 C19 -29.8(12)
C13 C14 C15 C22 -162.(2)
C14 C15 C16 C17 -75.7(17)
C19 C15 C16 C17 29.2(13)
C22 C15 C16 C17 161.(2)
C14 C15 C19 C18 51.4(14)
C14 C15 C19 C20 -67.4(17)
C14 C15 C19 C21 166.(2)
C16 C15 C19 C18 -52.2(14)
C16 C15 C19 C20 -171.(2)
C16 C15 C19 C21 61.9(15)
C22 C15 C19 C18 -180.(2)
C22 C15 C19 C20 61.7(17)
C22 C15 C19 C21 -65.4(16)
C15 C16 C17 C18 6.8(10)
C16 C17 C18 C13 66.1(16)
C16 C17 C18 C19 -38.3(13)
C13 C18 C19 C15 -55.3(14)
C13 C18 C19 C20 64.2(17)
C13 C18 C19 C21 -173.(2)
C17 C18 C19 C15 56.2(15)
C17 C18 C19 C20 176.(3)
C17 C18 C19 C21 -61.6(16)
C1 C23 C24 C25 -179.(3)
C28 C23 C24 C25 2.6(13)
C1 C23 C28 C27 -179.(3)
C24 C23 C28 C27 -0.4(13)
C23 C24 C25 C26 -4.2(13)
C24 C25 C26 C27 3.8(13)
C25 C26 C27 C28 -1.8(13)
C26 C27 C28 C23 0.1(13)
C2 C29 C30 C31 -179.(2)
C34 C29 C30 C31 0.7(12)
C2 C29 C34 C33 179.(2)
C30 C29 C34 C33 -1.1(13)
C29 C30 C31 C32 -2.3(13)
C30 C31 C32 C33 4.2(13)
C31 C32 C33 C34 -4.4(13)
C32 C33 C34 C29 2.9(13)