#------------------------------------------------------------------------------
#$Date: 2011-09-16 16:46:08 +0100 (Fri, 16 Sep 2011) $
#$Revision: 26025 $
#$URL: svn://www.crystallography.net/cod/hkl/2/2006592.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2006592_Fobs
loop_
_publ_author_name
'Spengler, R.'
'Zouari, F.'
'Ben Salah, A.'
'Burzlaff, H.'
_publ_section_title
;
 Bis(piperidinium) Tetrachloromercurate
;
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1407
_journal_page_last               1409
_journal_volume                  53
_journal_year                    1997
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_exptl_crystal_F_000             984
_[local]_cod_data_source_file    jz1222sup2.hkl
_[local]_cod_data_source_block   hgpip1
#BEGIN Tags that were not found in dictionaries:
_crystan_f_calc_maximum          32000.
#END Tags that were not found in dictionaries
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_calc
_refln_F_meas
_refln_F_sigma
1 1 1 21316.46 21874.00 204.00
2 1 0 20322.46 21110.00 201.00
0 2 0 18024.01 18700.00 207.00
-2 1 1 5479.93 5704.00 89.00
1 2 0 11161.82 11493.00 203.00
0 2 1 21635.75 22335.00 398.00
-1 2 1 22355.19 21117.00 244.00
2 1 1 987.67 1207.00 71.00
0 0 2 28744.98 30748.00 368.00
-3 0 1 29671.73 30057.00 274.00
1 2 1 7500.56 7792.00 161.00
2 2 0 11128.71 11435.00 123.00
3 1 0 6903.95 7076.00 102.00
-1 1 2 1949.24 1887.00 93.00
0 1 2 11003.20 11857.00 156.00
-2 2 1 3489.77 3449.00 63.00
-3 1 1 11955.19 11919.00 125.00
-2 0 2 2146.56 2175.00 57.00
-2 1 2 19201.36 18620.00 238.00
3 0 1 29674.68 31428.00 334.00
1 1 2 13101.17 14058.00 251.00
2 2 1 13897.87 14786.00 264.00
1 3 0 11874.12 12238.00 191.00
3 1 1 11338.16 12151.00 130.00
3 2 0 23069.42 23720.00 228.00
-1 2 2 16366.72 15351.00 155.00
0 2 2 8216.73 8673.00 133.00
-3 2 1 7274.00 7136.00 94.00
0 3 1 7659.81 7809.00 90.00
2 0 2 23427.96 24576.00 425.00
-1 3 1 13617.81 13629.00 141.00
4 0 0 28316.45 29787.00 279.00
-3 1 2 11076.17 10948.00 128.00
-2 2 2 10266.55 9821.00 112.00
1 3 1 16048.12 17203.00 301.00
2 3 0 11522.99 12001.00 142.00
2 1 2 5605.32 6001.00 128.00
4 1 0 8711.48 8950.00 140.00
1 2 2 1860.77 1969.00 65.00
-4 1 1 3549.08 3584.00 113.00
-2 3 1 17827.17 17467.00 206.00
3 2 1 4601.44 4579.00 182.00
-1 0 3 26261.62 27688.00 514.00
2 3 1 12604.09 13033.00 286.00
-3 2 2 11477.35 10993.00 124.00
-4 0 2 24803.69 25275.00 243.00
2 2 2 5046.93 5067.00 126.00
4 2 0 13780.75 14258.00 153.00
-4 2 1 9928.93 10028.00 147.00
-1 1 3 10947.71 11547.00 133.00
4 1 1 6519.04 6768.00 92.00
3 3 0 6490.37 6653.00 93.00
-4 1 2 4824.15 4754.00 77.00
-1 3 2 8097.74 7742.00 101.00
0 3 2 4000.77 4179.00 72.00
-3 3 1 9261.05 9245.00 144.00
0 1 3 12870.07 13827.00 216.00
0 4 0 26603.59 27808.00 625.00
-2 1 3 10704.44 10614.00 120.00
3 1 2 7639.64 7985.00 104.00
1 0 3 15960.57 17013.00 420.00
-2 3 2 2897.50 2753.00 82.00
1 4 0 11134.05 11353.00 249.00
-5 0 1 12132.75 12835.00 147.00
1 3 2 19373.69 20722.00 425.00
-3 0 3 10637.89 10857.00 192.00
1 1 3 17458.33 18469.00 415.00
0 4 1 22967.94 23911.00 357.00
-5 1 1 17604.84 17957.00 196.00
-1 4 1 5651.76 5637.00 167.00
3 3 1 6152.63 6123.00 131.00
5 1 0 13712.92 14368.00 166.00
-1 2 3 7732.68 7609.00 230.00
4 2 1 6600.91 6658.00 95.00
-3 1 3 8372.94 8375.00 105.00
-4 2 2 10938.61 10494.00 134.00
0 2 3 8379.74 8512.00 126.00
1 4 1 4572.46 4535.00 182.00
2 4 0 621.45 1116.00 295.00
-2 2 3 9373.22 9164.00 111.00
3 2 2 16414.49 17499.00 310.00
-3 3 2 7907.71 7360.00 183.00
-2 4 1 5753.71 5601.00 86.00
2 3 2 7477.68 7823.00 271.00
4 3 0 2989.03 2971.00 115.00
-4 3 1 13599.33 13962.00 297.00
1 2 3 6977.89 6998.00 242.00
4 0 2 2556.76 2745.00 80.00
-5 1 2 12585.64 12795.00 195.00
5 0 1 20364.15 21068.00 230.00
2 1 3 3796.67 3929.00 118.00
-5 2 1 9805.47 9889.00 118.00
5 2 0 5971.26 5929.00 196.00
2 4 1 18236.01 18916.00 533.00
-3 2 3 16176.22 15642.00 163.00
4 1 2 15352.07 16097.00 223.00
5 1 1 11802.50 12292.00 138.00
-4 1 3 4997.11 4925.00 112.00
3 4 0 20473.30 21004.00 320.00
-1 4 2 21919.96 21071.00 400.00
0 4 2 3448.03 3692.00 85.00
-3 4 1 2183.61 2197.00 88.00
-1 3 3 5291.11 4940.00 82.00
4 3 1 16112.12 16817.00 293.00
-4 3 2 332.23 756.00 238.00
0 3 3 12317.78 12903.00 250.00
-2 4 2 6814.18 6627.00 107.00
-5 2 2 5257.68 5086.00 86.00
2 2 3 12639.03 13336.00 256.00
1 4 2 2021.21 2252.00 86.00
-2 3 3 16225.28 15033.00 242.00
3 3 2 8498.20 8766.00 112.00
3 0 3 13336.89 13569.00 160.00
4 2 2 1825.07 1987.00 159.00
6 0 0 30751.44 32000.00 351.00
5 2 1 11295.46 11643.00 176.00
-4 2 3 10398.75 10002.00 120.00
-6 1 1 5301.66 5351.00 89.00
3 4 1 373.10 707.00 220.00
3 1 3 12943.84 13440.00 151.00
1 3 3 7341.64 7582.00 279.00
-2 0 4 18228.07 19103.00 382.00
6 1 0 2462.99 2561.00 159.00
1 5 0 18046.44 18531.00 285.00
-5 3 1 6338.14 6307.00 95.00
-5 0 3 16824.09 17211.00 276.00
0 0 4 3904.32 4130.00 87.00
5 3 0 12680.44 12825.00 146.00
-1 1 4 1384.33 1505.00 131.00
-3 3 3 2320.02 2240.00 84.00
-3 4 2 12046.13 11347.00 134.00
-6 0 2 12489.79 12359.00 271.00
-2 1 4 15632.53 16055.00 314.00
0 5 1 10001.44 10380.00 198.00
-5 1 3 21598.03 21453.00 268.00
-1 5 1 4466.09 4562.00 127.00
4 4 0 8623.82 8663.00 220.00
-4 4 1 18995.36 18864.00 233.00
0 1 4 26572.80 28026.00 631.00
-6 1 2 14002.77 14165.00 161.00
1 5 1 8038.36 8299.00 316.00
2 5 0 4670.37 4708.00 84.00
-6 2 1 12200.77 12352.00 143.00
3 2 3 6502.94 6253.00 238.00
-3 1 4 7548.96 7438.00 216.00
5 1 2 6215.44 6407.00 100.00
-2 5 1 16891.12 16962.00 178.00
6 2 0 12555.09 12736.00 144.00
-5 3 2 14867.71 14511.00 200.00
2 3 3 1981.19 2011.00 90.00
-1 2 4 12714.95 13085.00 171.00
1 1 4 4644.04 4835.00 88.00
4 3 2 6465.04 6681.00 118.00
-2 2 4 8394.63 8203.00 204.00
6 1 1 2222.66 2255.00 85.00
5 3 1 7765.71 7945.00 158.00
-5 2 3 6940.63 6873.00 133.00
-4 3 3 5231.35 5129.00 101.00
0 2 4 7550.03 7684.00 179.00
-1 4 3 5366.59 4996.00 90.00
2 5 1 11574.63 11847.00 294.00
4 4 1 9408.92 9808.00 215.00
-4 4 2 3468.82 3342.00 88.00
-6 2 2 9522.12 9455.00 127.00
0 4 3 12046.11 12159.00 223.00
-4 0 4 17093.27 17702.00 549.00
-2 4 3 11177.89 10346.00 224.00
3 4 2 17572.93 18110.00 338.00
3 5 0 2731.28 2808.00 124.00
4 1 3 8281.26 8322.00 249.00
-1 5 2 4050.63 3922.00 82.00
-3 2 4 1347.58 1482.00 107.00
0 5 2 8107.86 8271.00 208.00
5 2 2 11202.78 11579.00 229.00
-3 5 1 2364.09 2411.00 91.00
-4 1 4 5941.86 5894.00 101.00
2 0 4 25530.78 26079.00 419.00
1 2 4 11504.81 12006.00 468.00
-7 0 1 12516.39 12833.00 169.00
1 4 3 3730.54 3758.00 102.00
6 2 1 14376.01 14868.00 165.00
-2 5 2 9758.93 9535.00 123.00
-5 4 1 9270.33 9116.00 134.00
-6 3 1 4531.21 4454.00 90.00
2 1 4 2978.68 3124.00 83.00
1 5 2 22190.22 23037.00 428.00
5 4 0 7512.08 7647.00 171.00
-6 1 3 7089.24 6974.00 103.00
-3 4 3 2521.00 2377.00 86.00
3 3 3 4964.57 5088.00 140.00
-7 1 1 9364.80 9677.00 198.00
6 3 0 1707.70 1677.00 111.00
-1 3 4 1351.49 1436.00 129.00
4 2 3 4054.67 4144.00 89.00
7 1 0 3292.50 3304.00 123.00
-2 3 4 5503.40 5260.00 91.00
-4 2 4 9414.63 9134.00 119.00
-5 3 3 8913.44 8496.00 115.00
0 3 4 13982.24 14587.00 278.00
-3 5 2 13197.69 12616.00 149.00
-6 3 2 5894.08 5684.00 132.00
-7 1 2 374.70 847.00 217.00
-5 4 2 4721.93 4630.00 92.00
2 4 3 19853.98 20419.00 587.00
2 5 2 10564.28 10847.00 166.00
6 0 2 25253.21 26135.00 337.00
2 2 4 15644.62 15875.00 585.00
4 5 0 10142.32 10396.00 207.00
0 6 0 8944.89 9208.00 265.00
-4 5 1 10086.84 9882.00 127.00
-6 2 3 4739.02 4597.00 89.00
-5 1 4 4148.07 4144.00 90.00
-7 2 1 9309.29 9440.00 122.00
-3 3 4 15718.80 14767.00 200.00
5 3 2 5392.87 5429.00 261.00
4 4 2 2117.87 2201.00 104.00
1 6 0 5610.23 5812.00 211.00
5 4 1 4713.60 4599.00 94.00
-4 4 3 20218.08 18956.00 273.00
6 1 2 13300.72 13733.00 222.00
1 3 4 14016.17 14545.00 282.00
7 2 0 8474.26 8502.00 138.00
0 6 1 13892.12 14521.00 228.00
6 3 1 2918.12 2869.00 165.00
5 0 3 21253.73 21768.00 322.00
-1 6 1 7374.77 7472.00 198.00
3 1 4 10052.70 9885.00 373.00
7 0 1 3574.60 3652.00 94.00
-7 2 2 10839.63 10688.00 133.00
5 1 3 9227.53 9097.00 285.00
1 6 1 5427.84 5597.00 164.00
2 6 0 5274.26 5199.00 183.00
7 1 1 23589.82 23949.00 299.00
-1 5 3 4660.60 4366.00 94.00
4 5 1 18694.24 19289.00 212.00
-5 2 4 11212.63 10832.00 222.00
-4 5 2 4276.78 4201.00 112.00
4 3 3 12240.89 12467.00 289.00
-1 0 5 17053.82 17634.00 662.00
-2 6 1 3302.97 3425.00 89.00
0 5 3 19881.35 20441.00 394.00
-4 3 4 3601.46 3411.00 93.00
6 2 2 10865.78 11122.00 152.00
-6 4 1 17752.18 17792.00 217.00
-7 0 3 22410.46 22422.00 443.00
-2 5 3 15520.01 14456.00 285.00
3 5 2 9736.44 9974.00 200.00
3 4 3 1257.43 1496.00 123.00
-1 1 5 10655.05 10983.00 201.00
-2 1 5 2180.66 2204.00 107.00
6 4 0 6062.67 5991.00 141.00
-7 1 3 2085.66 2085.00 131.00
2 3 4 3530.18 3559.00 221.00
3 2 4 2844.96 2906.00 131.00
-3 0 5 11591.74 12066.00 235.00
-1 4 4 18848.17 17047.00 182.00
2 6 1 10574.59 10766.00 380.00
-6 3 3 10977.64 10411.00 133.00
-6 0 4 453.19 655.00 312.00
-7 3 1 3231.77 3414.00 146.00
1 5 3 7712.89 7878.00 337.00
5 2 3 9721.01 9889.00 375.00
0 1 5 8147.47 8281.00 198.00
-5 5 1 8383.89 8330.00 119.00
-5 4 3 3570.34 3387.00 94.00
-3 1 5 11980.74 12039.00 310.00
7 2 1 4326.97 4393.00 156.00
0 4 4 2733.45 2843.00 74.00
5 5 0 18341.51 18311.00 211.00
3 6 0 14646.70 14952.00 345.00
-6 1 4 20763.63 20647.00 214.00
-3 5 3 11521.68 10573.00 156.00
-1 6 2 13197.80 13266.00 248.00
-6 4 2 1999.96 1842.00 181.00
0 6 2 11157.47 11423.00 250.00
7 3 0 13428.86 13633.00 158.00
-3 6 1 15728.10 15680.00 260.00
4 0 4 11160.60 11330.00 387.00
-8 1 1 8956.60 8877.00 122.00
1 0 5 26215.05 27166.00 597.00
-1 2 5 10567.34 10629.00 242.00
-3 4 4 1971.58 1795.00 108.00
-2 2 5 10944.18 11213.00 171.00
-7 3 2 8589.51 8499.00 147.00
5 4 2 13866.78 14144.00 452.00
-2 6 2 6885.07 6734.00 204.00
8 0 0 4112.31 4059.00 117.00
-7 2 3 18492.06 18383.00 196.00
1 6 2 851.11 1208.00 163.00
-8 0 2 3773.20 3837.00 185.00
-5 3 4 8669.90 8480.00 169.00
1 4 4 10873.61 11188.00 408.00
4 1 4 18215.70 18490.00 642.00
1 1 5 8685.51 8962.00 303.00
6 4 1 17720.96 17585.00 498.00
0 2 5 852.23 962.00 162.00
-5 5 2 15124.04 14490.00 184.00
2 5 3 2309.90 2377.00 100.00
-4 1 5 5772.58 5713.00 98.00
8 1 0 14951.43 15088.00 171.00
6 3 2 7191.50 7452.00 374.00
-3 2 5 2791.24 2689.00 103.00
3 6 1 17319.54 17747.00 444.00
-8 1 2 12594.09 12805.00 188.00
-6 2 4 3897.25 3770.00 93.00
4 5 2 9542.37 9824.00 248.00
5 5 1 4536.22 4467.00 99.00
-4 5 3 6205.89 5826.00 102.00
3 3 4 10267.04 10479.00 352.00
-3 6 2 9992.37 9796.00 129.00
4 4 3 5401.48 5554.00 175.00
7 1 2 6490.22 6210.00 108.00
5 3 3 7023.23 7138.00 316.00
-4 4 4 1122.51 997.00 297.00
2 6 2 13912.72 14127.00 372.00
7 3 1 15731.62 15699.00 318.00
4 6 0 3907.00 4035.00 95.00
-4 6 1 7332.89 7390.00 113.00
4 2 4 1738.27 1945.00 130.00
1 2 5 14269.94 14737.00 527.00
6 1 3 6594.63 6420.00 159.00
-4 2 5 8661.62 8352.00 132.00
8 2 0 9090.06 9286.00 128.00
2 4 4 5668.54 5636.00 136.00
-5 0 5 15651.76 15644.00 213.00
-8 2 2 2071.59 2170.00 112.00
-6 4 3 5426.77 5115.00 100.00
2 1 5 1867.74 1710.00 119.00
-1 3 5 9587.07 9818.00 324.00
-2 3 5 9247.16 9090.00 124.00
-6 5 1 9032.02 8913.00 127.00
-5 1 5 892.11 1198.00 426.00
3 5 3 7485.01 7646.00 340.00
-7 1 4 4697.61 4582.00 96.00
7 4 0 11383.31 11312.00 230.00
7 2 2 887.25 957.00 244.00
8 1 1 6019.46 5902.00 111.00
0 3 5 11466.24 11838.00 330.00
1 7 0 3100.26 3052.00 150.00
-3 3 5 3621.36 3609.00 91.00
-8 1 3 4131.64 4146.00 173.00
-1 5 4 3886.91 3705.00 94.00
-1 6 3 15020.16 14596.00 323.00
4 6 1 5111.76 5071.00 189.00
-6 3 4 10952.81 10736.00 137.00
-4 6 2 13051.66 12661.00 190.00
6 2 3 7586.88 7720.00 219.00
-7 4 2 16914.93 16659.00 186.00
-2 5 4 2034.32 2065.00 121.00
0 7 1 1578.88 1594.00 103.00
0 6 3 8672.27 8766.00 234.00
-5 5 3 1188.53 1241.00 282.00
-1 7 1 4597.75 4521.00 147.00
-2 6 3 5970.51 5629.00 114.00
0 5 4 1134.79 1375.00 113.00
3 6 2 11331.12 11744.00 407.00
-5 4 4 12653.47 11661.00 282.00
-8 3 1 13470.75 13568.00 162.00
2 2 5 7833.18 7869.00 136.00
-6 5 2 2625.55 2635.00 117.00
1 7 1 9899.87 9984.00 332.00
2 7 0 10001.41 9891.00 289.00
6 4 2 4326.86 4353.00 115.00
-5 2 5 7984.92 7690.00 115.00
5 1 4 1945.54 2103.00 234.00
4 3 4 9559.44 9679.00 360.00
1 3 5 2609.51 2792.00 196.00
-3 5 4 14104.41 12747.00 154.00
1 6 3 4331.31 4497.00 138.00
-7 2 4 8449.80 8297.00 215.00
5 5 2 9434.86 9545.00 333.00
-2 7 1 1879.47 1899.00 129.00
8 2 1 6570.19 6671.00 291.00
-4 3 5 6153.85 5580.00 148.00
3 0 5 2856.18 2794.00 237.00
-5 6 1 7291.79 7030.00 211.00
8 3 0 5505.15 5506.00 172.00
3 4 4 3676.53 3897.00 99.00
-8 2 3 5492.58 5447.00 102.00
-8 3 2 1670.25 1652.00 154.00
5 6 0 4503.89 4437.00 117.00
-3 6 3 791.33 1306.00 254.00
1 5 4 9581.38 9684.00 198.00
-9 0 1 9022.94 9264.00 126.00
6 5 1 1312.65 1591.00 143.00
5 4 3 3079.08 3261.00 141.00
3 1 5 12418.96 12470.00 605.00
7 4 1 1597.45 1632.00 143.00
2 7 1 2690.67 2738.00 105.00
-6 1 5 4195.41 4007.00 97.00
-9 1 1 1505.39 1500.00 139.00
7 3 2 12232.31 12444.00 375.00
5 2 4 10863.06 10864.00 321.00
3 7 0 4712.24 4774.00 96.00
4 5 3 15023.17 15324.00 632.00
6 3 3 10175.91 10344.00 351.00
-1 4 5 3354.56 3379.00 100.00
-1 7 2 2328.97 2411.00 106.00
-2 4 5 13812.30 12985.00 214.00
0 7 2 8629.59 8666.00 259.00
-3 7 1 3114.64 3275.00 100.00
-5 6 2 2190.13 2124.00 116.00
2 6 3 10267.44 10780.00 472.00
-9 1 2 6688.20 6624.00 110.00
-7 4 3 6327.22 5968.00 107.00
2 3 5 5986.60 6039.00 299.00
9 1 0 4241.65 4442.00 102.00
7 0 3 1874.13 1972.00 131.00
-2 0 6 16640.58 16999.00 354.00
4 6 2 1086.06 1370.00 167.00
8 0 2 13516.73 13571.00 325.00
-2 7 2 15632.90 15328.00 293.00
0 4 5 2395.75 2573.00 129.00
5 6 1 6494.87 6564.00 258.00
3 2 5 1405.80 1392.00 161.00
-4 6 3 8572.25 8170.00 154.00
2 5 4 1316.71 1215.00 186.00
-3 4 5 7535.62 7274.00 144.00
-5 3 5 2972.21 2865.00 113.00
1 7 2 6231.35 6383.00 276.00
-6 5 3 11988.17 11451.00 146.00
-6 4 4 989.16 793.00 305.00
-8 0 4 14572.50 14653.00 288.00
-7 5 1 3664.83 3668.00 108.00
7 1 3 11922.60 11867.00 323.00
-6 2 5 913.16 894.00 235.00
-9 2 1 4856.56 4843.00 102.00
-7 3 4 2308.58 2363.00 130.00
-2 1 6 3204.23 3504.00 149.00
8 3 1 6580.11 6445.00 210.00
8 1 2 4910.91 4862.00 217.00
-1 1 6 5440.86 5554.00 101.00
3 7 1 1482.13 1703.00 173.00
-8 3 3 12226.49 11936.00 149.00
-8 1 4 9410.43 9131.00 129.00
-8 4 1 1415.44 1401.00 181.00
7 5 0 10271.92 10209.00 244.00
0 0 6 10451.23 10927.00 272.00
-3 1 6 3419.92 3494.00 108.00
-9 2 2 5147.03 4898.00 102.00
4 4 4 1309.65 1205.00 201.00
-3 7 2 955.14 849.00 329.00
1 4 5 7374.66 7734.00 341.00
9 2 0 8589.49 8661.00 126.00
-9 0 3 1866.09 1949.00 150.00
-7 5 2 2987.10 2853.00 114.00
0 1 6 13094.16 13429.00 324.00
-4 4 5 11353.18 10646.00 140.00
2 7 2 9980.45 10114.00 281.00
8 4 0 78.78 819.00 307.00
-6 6 1 11594.24 11537.00 148.00
4 7 0 11294.82 11356.00 186.00
-4 7 1 4325.02 4330.00 152.00
-8 4 2 2224.07 2232.00 135.00
5 3 4 1412.22 1713.00 191.00
-4 0 6 1152.57 1376.00 160.00
6 0 4 8065.59 8043.00 413.00
-5 5 4 6549.05 6132.00 181.00
3 6 3 7330.26 7522.00 331.00
-7 0 5 9108.03 8866.00 254.00
-9 1 3 9687.35 9726.00 172.00
7 2 3 1780.65 1878.00 143.00
4 1 5 4436.73 4518.00 186.00
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