#------------------------------------------------------------------------------ #$Date: 2016-04-02 18:32:15 +0100 (Sat, 02 Apr 2016) $ #$Revision: 180745 $ #$URL: svn://www.crystallography.net/cod/hkl/2/00/66/2006612.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2006612_Fobs loop_ _publ_author_name 'Bolte, M.' 'Scholtyssik, M.' _publ_section_title ; Dimedone at 133K ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first IUC9700013 _journal_volume 53 _journal_year 1997 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.340 _cell_angle_gamma 90.000 _cell_length_a 9.9740 _cell_length_b 6.7520 _cell_length_c 12.4097 _exptl_crystal_F_000 304.00 _reflns_d_resolution_high 0.7984 _cod_data_source_file qa0018sup2.hkl _cod_data_source_block ms2 #BEGIN Tags that were not found in dictionaries: _shelx_title ' ms2 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 85.21 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2314.84 2068.33 33.58 o 4 0 0 64.11 50.56 1.05 o 6 0 0 379.56 376.09 4.87 o 8 0 0 49.85 51.19 1.42 o 10 0 0 17.36 14.94 1.55 o 1 1 0 241.86 221.46 6.71 o 2 1 0 7260.48 6920.98 59.92 o 3 1 0 24.25 35.53 0.60 o 4 1 0 825.31 791.22 6.15 o 5 1 0 3.84 3.30 0.36 o 6 1 0 37.55 34.94 0.74 o 7 1 0 134.05 132.80 1.67 o 8 1 0 124.55 124.57 1.77 o 9 1 0 0.98 0.02 0.68 o 10 1 0 21.23 18.77 1.18 o 11 1 0 6.09 7.61 1.19 o 0 2 0 2113.42 2034.76 23.74 o 1 2 0 7.23 4.24 0.39 o 2 2 0 1853.24 1821.26 13.74 o 3 2 0 1562.95 1600.75 15.10 o 4 2 0 793.29 813.56 6.15 o 5 2 0 1.84 1.16 0.38 o 6 2 0 44.12 47.05 0.97 o 7 2 0 88.86 84.38 1.36 o 8 2 0 0.30 -0.06 0.61 o 9 2 0 80.45 78.66 1.83 o 10 2 0 2.39 2.24 0.90 o 11 2 0 0.72 -0.26 1.37 o 1 3 0 19.36 18.09 0.49 o 2 3 0 876.43 943.17 7.91 o 3 3 0 1641.33 1618.82 12.20 o 4 3 0 3.86 3.87 0.39 o 5 3 0 702.85 681.72 6.62 o 6 3 0 0.98 2.12 0.56 o 7 3 0 6.89 5.97 0.72 o 8 3 0 3.05 2.90 0.71 o 9 3 0 24.45 23.67 1.29 o 10 3 0 0.02 -0.13 0.90 o 0 4 0 210.69 239.83 3.71 o 1 4 0 19.21 23.13 0.61 o 2 4 0 62.55 76.02 1.12 o 3 4 0 150.66 149.77 1.70 o 4 4 0 7.68 8.78 0.54 o 5 4 0 354.24 380.39 4.24 o 6 4 0 0.94 0.81 0.62 o 7 4 0 8.85 11.44 0.94 o 8 4 0 1.35 1.32 0.93 o 9 4 0 5.36 7.53 1.26 o 10 4 0 22.03 25.27 2.64 o 1 5 0 41.18 39.70 0.86 o 2 5 0 55.89 60.04 1.14 o 3 5 0 18.54 19.86 0.76 o 4 5 0 99.89 102.30 1.58 o 5 5 0 70.73 63.11 1.62 o 6 5 0 6.34 3.56 0.82 o 7 5 0 86.70 76.91 1.97 o 8 5 0 0.12 -1.09 1.09 o 9 5 0 4.01 3.59 2.44 o 0 6 0 85.80 80.86 1.82 o 1 6 0 183.78 179.79 2.54 o 2 6 0 1.46 1.02 0.58 o 3 6 0 0.29 0.37 0.57 o 4 6 0 2.30 2.59 0.71 o 5 6 0 59.41 64.84 1.57 o 6 6 0 16.28 16.46 1.07 o 7 6 0 28.57 24.44 1.71 o 8 6 0 21.92 24.55 2.89 o 1 7 0 37.89 38.59 1.31 o 2 7 0 36.70 39.33 1.08 o 3 7 0 143.35 146.44 2.13 o 4 7 0 26.24 25.03 1.07 o 5 7 0 0.44 0.07 0.82 o 6 7 0 11.94 13.73 1.45 o 0 8 0 0.99 0.58 1.02 o 1 8 0 181.99 174.86 4.26 o 2 8 0 2.90 4.24 0.83 o 3 8 0 0.17 0.22 0.71 o -11 0 1 44.52 47.93 3.41 o -9 0 1 17.79 19.44 1.26 o -7 0 1 39.59 35.74 1.15 o -5 0 1 118.16 111.74 1.76 o -3 0 1 3006.85 2793.49 36.06 o -1 0 1 1135.76 1076.31 27.47 o 1 0 1 67.27 67.21 1.77 o 3 0 1 16.37 18.55 0.67 o 5 0 1 1032.07 1038.31 11.23 o 7 0 1 30.36 37.14 1.07 o 9 0 1 7.04 8.27 1.25 o 11 0 1 74.71 74.38 3.73 o -11 1 1 9.40 9.92 1.12 o -10 1 1 136.56 133.38 2.53 o -9 1 1 1.88 1.13 0.61 o -8 1 1 3.24 2.82 0.62 o -7 1 1 99.89 94.85 1.44 o -6 1 1 211.62 210.30 2.58 o -5 1 1 385.83 388.20 3.31 o -4 1 1 72.25 79.87 0.97 o -3 1 1 8.23 12.57 0.44 o -2 1 1 3640.74 3560.60 37.87 o -1 1 1 1057.61 992.80 17.95 o 0 1 1 2395.91 2200.06 30.93 o 1 1 1 6954.78 6388.27 93.89 o 2 1 1 72.71 86.06 1.41 o 3 1 1 694.17 698.37 7.47 o 4 1 1 178.84 201.09 1.97 o 5 1 1 59.17 65.06 0.85 o 6 1 1 27.90 28.60 0.69 o 7 1 1 11.00 13.31 0.58 o 8 1 1 7.69 6.85 0.66 o 9 1 1 7.48 8.08 0.90 o 10 1 1 0.13 0.32 0.83 o 11 1 1 1.06 1.04 1.04 o -11 2 1 0.05 -1.71 1.71 o -10 2 1 1.52 2.24 0.92 o -9 2 1 81.54 74.33 2.12 o -8 2 1 200.40 204.31 2.55 o -7 2 1 230.87 232.32 2.78 o -6 2 1 39.24 39.78 0.90 o -5 2 1 337.11 328.15 2.86 o -4 2 1 657.48 653.66 5.10 o -3 2 1 25.64 23.74 0.47 o -2 2 1 3179.26 3132.93 24.41 o -1 2 1 536.93 516.66 7.54 o 0 2 1 723.68 684.40 5.83 o 1 2 1 3276.37 3237.54 29.74 o 2 2 1 159.12 158.20 1.38 o 3 2 1 2207.93 2316.23 16.12 o 4 2 1 15.95 17.86 0.42 o 5 2 1 3.73 5.90 0.43 o 6 2 1 0.34 -0.01 0.44 o 7 2 1 93.68 92.77 1.35 o 8 2 1 2.91 2.58 0.74 o 9 2 1 5.71 4.87 0.89 o 10 2 1 9.24 11.24 1.09 o 11 2 1 15.65 16.00 1.61 o -11 3 1 36.42 37.96 2.09 o -10 3 1 18.81 17.70 1.19 o -9 3 1 8.03 8.81 0.84 o -8 3 1 103.57 106.45 2.38 o -7 3 1 57.74 58.34 1.25 o -6 3 1 199.68 190.73 2.20 o -5 3 1 120.96 119.05 1.44 o -4 3 1 539.90 526.09 4.39 o -3 3 1 22.92 27.02 0.55 o -2 3 1 162.02 174.62 1.75 o -1 3 1 113.94 120.39 1.30 o 0 3 1 131.33 130.02 1.29 o 1 3 1 202.98 217.91 1.90 o 2 3 1 866.85 838.02 6.22 o 3 3 1 954.46 943.81 6.98 o 4 3 1 0.39 -0.11 0.34 o 5 3 1 15.25 18.12 0.57 o 6 3 1 8.23 7.27 0.59 o 7 3 1 4.34 2.47 0.71 o 8 3 1 48.63 42.99 2.03 o 9 3 1 33.67 31.61 2.08 o 10 3 1 1.14 4.75 1.16 o -10 4 1 2.25 4.42 2.08 o -9 4 1 1.32 0.22 0.84 o -8 4 1 53.46 60.58 1.54 o -7 4 1 76.24 79.54 1.68 o -6 4 1 241.53 231.41 2.82 o -5 4 1 404.40 423.55 4.37 o -4 4 1 7.83 6.56 0.51 o -3 4 1 7.55 7.98 0.51 o -2 4 1 90.42 92.72 1.13 o -1 4 1 132.16 143.71 2.05 o 0 4 1 857.07 833.16 7.53 o 1 4 1 448.99 443.63 3.96 o 2 4 1 116.68 136.63 1.49 o 3 4 1 3.12 4.26 0.51 o 4 4 1 87.70 90.29 1.21 o 5 4 1 114.18 132.66 1.69 o 6 4 1 2.56 1.95 0.59 o 7 4 1 13.51 10.23 1.02 o 8 4 1 12.77 12.37 1.50 o 9 4 1 14.87 16.89 1.51 o -9 5 1 6.04 7.73 2.48 o -8 5 1 1.33 2.46 1.06 o -7 5 1 193.17 184.76 3.36 o -6 5 1 40.56 34.00 1.06 o -5 5 1 0.05 0.22 0.66 o -4 5 1 14.11 15.62 0.73 o -3 5 1 104.81 103.83 1.58 o -2 5 1 628.86 616.05 6.60 o -1 5 1 78.83 76.79 1.20 o 0 5 1 362.85 366.09 3.83 o 1 5 1 5.89 4.42 0.54 o 2 5 1 39.74 41.04 1.03 o 3 5 1 76.88 73.85 1.35 o 4 5 1 42.84 51.23 1.08 o 5 5 1 169.90 161.59 2.61 o 6 5 1 134.08 142.28 2.64 o 7 5 1 68.17 67.95 2.17 o 8 5 1 0.32 -0.67 1.40 o -8 6 1 118.85 135.53 4.33 o -7 6 1 86.82 74.94 6.44 o -6 6 1 4.74 7.04 0.94 o -5 6 1 0.10 -0.40 0.77 o -4 6 1 4.42 5.65 0.75 o -3 6 1 343.68 344.61 4.00 o -2 6 1 0.38 0.95 0.57 o -1 6 1 105.91 104.84 1.63 o 0 6 1 85.03 84.32 1.42 o 1 6 1 62.24 60.49 1.20 o 2 6 1 31.53 36.04 1.17 o 3 6 1 1.26 1.83 0.67 o 4 6 1 85.98 84.97 3.71 o 5 6 1 2.92 2.41 0.94 o 6 6 1 42.73 40.45 1.53 o 7 6 1 28.21 25.04 2.99 o -6 7 1 4.80 4.83 1.07 o -5 7 1 13.07 13.46 1.05 o -4 7 1 13.14 12.46 0.92 o -3 7 1 13.42 12.06 0.82 o -2 7 1 7.51 6.70 0.74 o -1 7 1 88.23 96.05 1.62 o 0 7 1 9.96 11.03 0.84 o 1 7 1 1.34 1.66 0.77 o 2 7 1 35.83 33.00 1.02 o 3 7 1 2.26 0.99 0.64 o 4 7 1 20.11 21.72 1.13 o 5 7 1 0.75 0.69 0.93 o 6 7 1 24.96 28.37 4.31 o -4 8 1 0.09 -1.31 1.76 o -3 8 1 16.58 18.05 1.09 o -2 8 1 5.60 5.27 0.86 o -1 8 1 13.74 14.14 1.07 o 0 8 1 13.80 13.50 0.94 o 1 8 1 2.22 1.81 0.78 o 2 8 1 2.02 2.37 1.07 o 3 8 1 46.27 47.18 1.49 o -12 0 2 99.88 100.82 4.51 o -10 0 2 412.43 414.27 7.15 o -8 0 2 105.03 103.02 3.13 o -6 0 2 15.00 11.58 0.67 o -4 0 2 161.07 172.51 5.06 o -2 0 2 1590.69 1497.59 26.79 o 0 0 2 2351.81 2311.76 41.02 o 2 0 2 30.39 37.17 0.94 o 4 0 2 79.29 91.61 1.39 o 6 0 2 8.95 7.93 0.79 o 8 0 2 194.17 186.67 3.11 o 10 0 2 5.15 5.75 1.43 o -12 1 2 69.28 73.09 4.47 o -11 1 2 11.66 9.51 1.08 o -10 1 2 244.27 250.99 3.35 o -9 1 2 95.78 100.67 1.60 o -8 1 2 283.65 273.87 3.20 o -7 1 2 0.29 0.46 0.51 o -6 1 2 12.84 15.49 0.53 o -5 1 2 86.57 89.79 1.01 o -4 1 2 0.30 0.49 0.34 o -3 1 2 1.08 0.86 0.35 o -2 1 2 840.64 820.65 7.87 o -1 1 2 1270.72 1213.14 12.89 o 0 1 2 250.25 209.70 2.45 o 1 1 2 577.93 579.03 5.71 o 2 1 2 12.27 18.48 0.51 o 3 1 2 26.41 37.09 0.60 o 4 1 2 381.72 378.88 3.10 o 5 1 2 35.03 41.59 0.69 o 6 1 2 1.87 0.07 0.46 o 7 1 2 64.18 65.85 1.11 o 8 1 2 18.34 17.89 0.73 o 9 1 2 0.00 0.00 0.59 o 10 1 2 30.36 29.98 1.23 o -11 2 2 1.34 0.35 1.05 o -10 2 2 3.22 3.72 0.79 o -9 2 2 109.83 113.80 1.90 o -8 2 2 288.54 298.85 3.47 o -7 2 2 8.17 10.89 0.69 o -6 2 2 54.62 55.39 0.97 o -5 2 2 563.48 555.81 4.87 o -4 2 2 4.20 5.75 0.65 o -3 2 2 423.70 380.92 3.23 o -2 2 2 359.95 342.42 3.36 o -1 2 2 607.58 584.56 5.57 o 0 2 2 88.44 89.07 1.05 o 1 2 2 189.39 200.54 2.63 o 2 2 2 105.23 121.83 1.70 o 3 2 2 1.52 2.83 0.33 o 4 2 2 166.89 194.77 1.69 o 5 2 2 33.38 32.84 0.64 o 6 2 2 90.10 96.89 1.28 o 7 2 2 68.98 66.38 1.21 o 8 2 2 51.57 44.10 1.15 o 9 2 2 35.88 31.12 1.32 o 10 2 2 6.83 6.90 1.31 o -11 3 2 1.29 0.30 1.22 o -10 3 2 0.13 0.26 0.82 o -9 3 2 23.93 21.50 0.96 o -8 3 2 12.34 11.97 0.82 o -7 3 2 717.91 694.52 7.90 o -6 3 2 47.10 46.25 1.02 o -5 3 2 9.03 9.16 0.52 o -4 3 2 165.15 156.50 1.64 o -3 3 2 10.27 7.02 0.40 o -2 3 2 65.22 65.33 0.93 o -1 3 2 185.68 174.46 1.67 o 0 3 2 9.56 6.21 0.36 o 1 3 2 381.42 428.60 3.47 o 2 3 2 1071.56 1121.97 8.24 o 3 3 2 603.28 625.71 5.35 o 4 3 2 58.84 64.53 0.91 o 5 3 2 131.02 135.48 1.59 o 6 3 2 28.70 21.07 0.79 o 7 3 2 40.18 36.13 1.12 o 8 3 2 124.44 124.54 2.38 o 9 3 2 18.89 19.91 1.21 o 10 3 2 0.24 -0.33 1.16 o -10 4 2 83.70 92.03 2.94 o -9 4 2 38.12 40.04 1.40 o -8 4 2 3.84 2.81 0.86 o -7 4 2 196.91 185.64 2.90 o -6 4 2 408.19 378.68 4.25 o -5 4 2 779.55 727.56 7.16 o -4 4 2 329.17 324.38 3.21 o -3 4 2 4.36 4.42 0.48 o -2 4 2 0.02 0.51 0.42 o -1 4 2 201.02 206.73 2.05 o 0 4 2 225.15 237.85 2.44 o 1 4 2 0.92 1.70 0.38 o 2 4 2 49.99 54.58 0.80 o 3 4 2 0.02 2.14 0.79 o 4 4 2 142.31 157.98 2.40 o 5 4 2 97.85 99.87 1.52 o 6 4 2 46.53 46.78 1.13 o 7 4 2 15.20 14.01 1.22 o 8 4 2 4.46 4.41 1.11 o -9 5 2 0.01 -0.61 1.45 o -8 5 2 59.37 59.55 1.87 o -7 5 2 27.64 30.47 1.40 o -6 5 2 17.22 13.54 0.85 o -5 5 2 536.78 514.76 6.17 o -4 5 2 24.24 25.77 1.10 o -3 5 2 190.94 182.27 2.34 o -2 5 2 102.36 102.43 1.56 o -1 5 2 62.38 53.27 1.06 o 0 5 2 87.27 84.15 1.26 o 1 5 2 76.69 72.38 1.16 o 2 5 2 231.61 246.89 2.79 o 3 5 2 6.68 8.89 0.66 o 4 5 2 3.48 2.89 0.64 o 5 5 2 44.79 32.07 1.03 o 6 5 2 44.68 50.11 1.52 o 7 5 2 8.16 8.03 1.65 o 8 5 2 3.02 3.30 2.26 o -8 6 2 22.20 21.86 2.12 o -7 6 2 51.50 48.55 1.47 o -6 6 2 9.65 12.33 1.09 o -5 6 2 4.61 3.82 0.74 o -4 6 2 118.69 119.63 2.38 o -3 6 2 65.50 70.28 1.59 o -2 6 2 205.26 207.01 2.64 o -1 6 2 90.08 90.69 1.51 o 0 6 2 2.10 1.88 0.60 o 1 6 2 0.66 1.57 0.56 o 2 6 2 18.87 16.23 0.78 o 3 6 2 37.45 28.12 0.92 o 4 6 2 24.21 25.07 1.10 o 5 6 2 0.09 0.05 0.75 o 6 6 2 4.63 2.38 1.13 o -6 7 2 10.58 10.00 1.11 o -5 7 2 2.13 0.37 0.74 o -4 7 2 24.66 24.56 1.06 o -3 7 2 18.64 19.69 0.89 o -2 7 2 97.61 91.52 1.59 o -1 7 2 5.83 6.29 0.73 o 0 7 2 15.87 17.76 0.93 o 1 7 2 13.31 14.59 0.89 o 2 7 2 17.51 16.81 1.03 o 3 7 2 23.60 24.02 0.95 o 4 7 2 35.05 32.34 1.28 o 5 7 2 10.39 9.89 1.25 o -4 8 2 33.95 37.34 3.01 o -3 8 2 0.15 -0.21 0.75 o -2 8 2 28.12 27.72 1.08 o -1 8 2 33.53 37.34 1.24 o 0 8 2 94.17 96.88 2.24 o 1 8 2 5.81 5.55 0.84 o 2 8 2 0.37 0.97 0.78 o -11 0 3 223.98 242.89 4.74 o -9 0 3 141.38 135.74 4.30 o -7 0 3 0.13 0.51 0.68 o -5 0 3 2459.03 2577.14 30.13 o -3 0 3 2458.78 2378.34 27.78 o -1 0 3 8.57 10.26 0.53 o 1 0 3 174.59 190.10 4.62 o 3 0 3 141.90 153.18 2.41 o 5 0 3 241.70 257.94 4.16 o 7 0 3 26.59 22.78 1.06 o 9 0 3 0.04 -0.37 0.82 o -12 1 3 130.19 136.77 4.03 o -11 1 3 11.41 7.76 0.96 o -10 1 3 41.22 41.99 1.32 o -9 1 3 67.83 68.75 1.43 o -8 1 3 0.98 0.31 0.57 o -7 1 3 511.38 514.66 5.49 o -6 1 3 44.12 51.45 0.87 o -5 1 3 0.06 -0.26 0.33 o -4 1 3 286.18 287.62 2.53 o -3 1 3 1236.90 1159.84 9.73 o -2 1 3 1.98 1.33 0.31 o -1 1 3 543.39 563.33 4.93 o 0 1 3 650.24 613.76 5.42 o 1 1 3 751.33 749.66 6.51 o 2 1 3 288.06 303.43 2.84 o 3 1 3 3.14 4.39 0.38 o 4 1 3 0.80 0.70 0.37 o 5 1 3 136.65 148.87 1.77 o 6 1 3 66.75 69.54 1.12 o 7 1 3 0.10 -0.49 0.49 o 8 1 3 0.13 0.10 0.54 o 9 1 3 203.60 208.39 2.65 o 10 1 3 22.87 19.98 1.11 o -11 2 3 1.34 2.86 0.93 o -10 2 3 3.03 3.96 0.87 o -9 2 3 638.62 624.97 9.38 o -8 2 3 67.49 70.13 1.28 o -7 2 3 209.24 213.40 2.62 o -6 2 3 0.14 1.04 0.44 o -5 2 3 111.81 108.61 1.26 o -4 2 3 15.49 20.85 0.51 o -3 2 3 39.00 33.13 0.58 o -2 2 3 1.33 3.48 0.35 o -1 2 3 0.53 -0.02 0.30 o 0 2 3 0.02 0.85 0.31 o 1 2 3 16.11 10.97 0.39 o 2 2 3 200.77 197.68 2.04 o 3 2 3 333.20 367.36 2.90 o 4 2 3 89.60 84.45 1.05 o 5 2 3 2.33 2.40 0.45 o 6 2 3 93.74 92.88 1.42 o 7 2 3 32.07 31.04 0.84 o 8 2 3 130.56 133.34 2.32 o 9 2 3 0.74 0.66 0.76 o 10 2 3 19.38 16.29 1.57 o -11 3 3 14.36 14.01 1.29 o -10 3 3 45.17 48.53 1.52 o -9 3 3 8.81 9.52 0.98 o -8 3 3 12.39 13.12 0.95 o -7 3 3 727.09 705.25 8.14 o -6 3 3 50.46 46.42 0.90 o -5 3 3 232.38 216.22 2.28 o -4 3 3 19.87 17.28 0.57 o -3 3 3 327.73 331.58 3.15 o -2 3 3 122.01 128.50 1.32 o -1 3 3 0.15 0.20 0.33 o 0 3 3 494.18 496.87 6.22 o 1 3 3 5.99 7.13 0.39 o 2 3 3 178.63 190.46 1.73 o 3 3 3 12.82 11.56 0.43 o 4 3 3 296.16 292.37 2.72 o 5 3 3 0.31 1.03 0.51 o 6 3 3 82.79 75.18 1.30 o 7 3 3 2.08 3.73 0.76 o 8 3 3 50.59 43.65 1.77 o 9 3 3 3.25 3.18 0.93 o -10 4 3 12.15 12.33 1.14 o -9 4 3 1.15 1.38 0.86 o -8 4 3 1.18 1.72 0.82 o -7 4 3 175.85 181.28 3.15 o -6 4 3 10.98 10.73 0.65 o -5 4 3 81.06 86.26 1.32 o -4 4 3 214.43 208.59 2.23 o -3 4 3 16.80 17.74 0.60 o -2 4 3 7.82 8.87 0.52 o -1 4 3 6.29 5.63 0.45 o 0 4 3 8.77 8.14 0.50 o 1 4 3 31.41 34.46 0.65 o 2 4 3 47.24 46.10 0.83 o 3 4 3 18.51 16.86 0.54 o 4 4 3 51.01 39.06 0.76 o 5 4 3 94.14 76.72 1.40 o 6 4 3 304.53 278.86 4.43 o 7 4 3 30.95 25.23 1.20 o 8 4 3 7.72 7.87 1.23 o 9 4 3 8.28 9.73 1.95 o -9 5 3 4.04 5.82 1.03 o -8 5 3 3.40 1.66 0.87 o -7 5 3 1.23 1.73 0.72 o -6 5 3 375.83 361.26 3.88 o -5 5 3 43.08 43.91 1.14 o -4 5 3 102.20 103.47 1.60 o -3 5 3 0.00 0.16 0.54 o -2 5 3 0.60 1.06 0.53 o -1 5 3 17.52 18.23 0.75 o 0 5 3 220.07 217.84 2.49 o 1 5 3 114.69 115.68 1.57 o 2 5 3 10.40 7.41 0.60 o 3 5 3 1.73 1.09 0.53 o 4 5 3 151.31 128.67 2.15 o 5 5 3 21.60 18.57 1.12 o 6 5 3 15.85 17.11 1.33 o 7 5 3 7.51 8.72 1.77 o 8 5 3 22.07 15.86 2.84 o -8 6 3 111.38 99.38 3.56 o -7 6 3 3.97 3.36 0.90 o -6 6 3 18.11 19.90 1.08 o -5 6 3 3.95 5.07 0.77 o -4 6 3 480.28 473.43 8.39 o -3 6 3 44.31 46.21 1.10 o -2 6 3 30.34 30.99 1.20 o -1 6 3 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