Crystallography Open Database

Information card for entry 2008236

2008235 << 2008236 >> 2008237

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Coordinates	2008236.cif
Original IUCr paper	HTML

Structure parameters

Chemical name	1-chloro-1-hydrido-2,6-di(2-hydroxyethoxy)-1,3,5-tris(triphenylphosphine)- iso-closo-1-ruthenadecaborane‒trichloromethane (1:1.2)
Formula	C59.2 H62.2 B9 Cl4.6 O4 P3 Ru
Calculated formula	C59.2 H62.2 B9 Cl4.6 O4 P3 Ru
Title of publication	A degraded glycol-substituted <i>iso</i>-<i>closo</i> ten-vertex ruthenaborane: [(PPh~3~)HClRuB~9~H~5~(OCH~2~CH~2~OH)~2~(PPh~3~)~2~]^.^1.2CHCl~3~
Authors of publication	Hai-Jun Yao; Chun-Hua Hu; Jian-Min Dou; Jie Sun; Jing-De Wei; Ruo-Shui Jin; Zu-En Huang; Pei-Ju Zheng
Journal of publication	Acta Crystallographica Section C
Year of publication	1999
Journal volume	55
Journal issue	3
Pages of publication	337 - 339
a	15.018 ± 0.005 Å
b	18.383 ± 0.004 Å
c	14.671 ± 0.007 Å
α	98.91 ± 0.03°
β	117.43 ± 0.03°
γ	97.21 ± 0.02°
Cell volume	3461 ± 2 Å³
Cell temperature	294 ± 2 K
Ambient diffraction temperature	294 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.17
Residual factor for significantly intense reflections	0.07
Weighted residual factors for all reflections included in the refinement	0.242
Goodness-of-fit parameter for all reflections included in the refinement	1.052
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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