#------------------------------------------------------------------------------ #$Date: 2016-04-02 18:33:34 +0100 (Sat, 02 Apr 2016) $ #$Revision: 180763 $ #$URL: svn://www.crystallography.net/cod/hkl/2/00/84/2008414.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008414_Fobs loop_ _publ_author_name 'Guzman-Jimenez, I. Y.' 'Whitmire, K. H.' _publ_section_title ; trans-Dichlorobis(methyldiphenylphosphine-P)palladium(II) ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first IUC9900028 _journal_volume 55 _journal_year 1999 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.381 _cell_angle_gamma 90.000 _cell_length_a 9.3640 _cell_length_b 15.4010 _cell_length_c 9.8710 _exptl_crystal_F_000 584.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file qb0079sup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 158.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 22148.40 34589.14 373.49 o 4 0 0 14.39 -3.13 8.32 o 6 0 0 1219.87 1298.81 31.95 o 8 0 0 482.24 516.92 26.35 o 1 1 0 9645.83 15164.02 166.41 o 2 1 0 7616.93 7908.77 86.95 o 3 1 0 346.70 352.90 12.02 o 4 1 0 154.17 168.30 10.87 o 5 1 0 3221.69 3352.41 51.96 o 6 1 0 205.64 218.94 16.96 o 7 1 0 1030.89 1067.68 32.28 o 8 1 0 89.65 129.93 12.68 o 9 1 0 619.50 561.14 31.78 o 0 2 0 19637.84 18727.88 191.27 o 1 2 0 4237.90 4359.33 48.83 o 2 2 0 252.04 327.54 11.61 o 3 2 0 7757.74 8157.43 93.62 o 4 2 0 236.90 207.08 11.61 o 5 2 0 21.22 35.16 3.87 o 6 2 0 2068.09 2125.90 42.40 o 7 2 0 68.90 92.88 9.30 o 8 2 0 273.98 288.02 21.74 o 9 2 0 1.13 11.20 18.53 o 1 3 0 2197.28 2120.79 27.67 o 2 3 0 6333.36 6331.00 72.70 o 3 3 0 1717.06 1698.97 28.41 o 4 3 0 123.21 124.17 11.69 o 5 3 0 7469.65 7424.87 95.02 o 6 3 0 284.39 336.60 20.09 o 7 3 0 1127.00 1187.98 33.43 o 8 3 0 26.54 1.56 17.13 o 9 3 0 94.67 102.84 10.29 o 0 4 0 4011.01 3935.53 47.34 o 1 4 0 454.93 462.25 11.61 o 2 4 0 5990.38 5850.31 69.00 o 3 4 0 7.03 2.06 7.90 o 4 4 0 11583.33 11484.07 132.56 o 5 4 0 1796.91 1863.32 37.05 o 6 4 0 4355.62 4287.12 67.35 o 7 4 0 9.98 16.06 5.76 o 8 4 0 128.99 118.73 11.28 o 9 4 0 39.57 44.87 6.83 o 1 5 0 484.01 444.13 12.43 o 2 5 0 21.91 26.18 2.72 o 3 5 0 3256.37 3128.45 45.29 o 4 5 0 845.98 891.31 23.55 o 5 5 0 7023.27 7112.56 93.37 o 6 5 0 137.23 159.49 11.94 o 7 5 0 962.45 1004.78 33.10 o 8 5 0 80.99 61.51 6.42 o 0 6 0 2777.00 2590.12 37.55 o 1 6 0 27.28 31.29 2.96 o 2 6 0 5511.22 5496.17 68.67 o 3 6 0 598.82 584.36 17.87 o 4 6 0 3462.23 3486.37 53.44 o 5 6 0 118.37 122.27 11.28 o 6 6 0 532.85 557.18 24.37 o 7 6 0 1532.38 1473.12 40.59 o 8 6 0 22.64 -0.58 13.67 o 1 7 0 1877.63 1731.99 30.22 o 2 7 0 96.44 107.04 7.66 o 3 7 0 2053.59 1863.15 34.25 o 4 7 0 303.92 278.39 16.96 o 5 7 0 1659.90 1701.77 37.63 o 6 7 0 489.95 476.90 24.70 o 7 7 0 1469.79 1452.78 41.99 o 8 7 0 131.84 137.18 12.52 o 0 8 0 4152.24 3817.29 54.67 o 1 8 0 0.00 -7.08 8.32 o 2 8 0 4898.90 4777.52 65.13 o 3 8 0 1126.27 1152.49 27.50 o 4 8 0 1248.88 1217.13 30.38 o 5 8 0 186.28 156.61 12.43 o 6 8 0 448.28 475.18 24.29 o 7 8 0 740.21 782.63 31.62 o 8 8 0 563.60 496.75 29.72 o 1 9 0 3701.93 3518.98 53.44 o 2 9 0 63.09 52.04 5.19 o 3 9 0 1567.72 1488.84 32.85 o 4 9 0 765.61 779.09 25.20 o 5 9 0 37.91 28.98 5.10 o 6 9 0 69.77 71.55 6.67 o 7 9 0 380.56 392.51 26.60 o 8 9 0 12.53 22.73 7.16 o 0 10 0 2337.10 2107.21 39.93 o 1 10 0 235.19 201.98 15.56 o 2 10 0 3599.51 3444.38 55.00 o 3 10 0 40.03 41.00 4.94 o 4 10 0 590.98 579.66 24.29 o 5 10 0 1.18 4.86 13.83 o 6 10 0 214.09 216.88 21.08 o 7 10 0 42.26 45.12 7.00 o 8 10 0 549.69 552.98 31.95 o 1 11 0 2135.87 2049.24 41.33 o 2 11 0 1246.33 1223.06 32.19 o 3 11 0 3365.94 3277.73 56.90 o 4 11 0 0.15 -6.59 14.41 o 5 11 0 242.59 256.81 19.93 o 6 11 0 8.54 -2.31 11.61 o 7 11 0 616.45 606.42 31.37 o 8 11 0 2.35 -17.04 23.38 o 0 12 0 234.04 190.53 16.39 o 1 12 0 84.87 63.32 6.26 o 2 12 0 2158.79 1948.37 43.23 o 3 12 0 20.90 20.50 5.68 o 4 12 0 834.84 859.61 29.64 o 5 12 0 1.99 7.08 15.64 o 6 12 0 219.74 210.21 15.73 o 7 12 0 28.07 12.43 21.66 o 1 13 0 2.80 -3.62 9.47 o 2 13 0 172.34 137.67 13.50 o 3 13 0 1303.90 1249.40 36.31 o 4 13 0 9.50 -17.62 17.62 o 5 13 0 317.69 336.85 24.04 o 6 13 0 45.40 62.49 6.75 o 7 13 0 387.00 405.19 28.82 o 0 14 0 78.49 77.56 7.66 o 1 14 0 4.07 -15.48 15.48 o 2 14 0 1501.20 1430.38 39.44 o 3 14 0 38.57 32.28 6.50 o 4 14 0 941.54 1000.58 35.49 o 5 14 0 0.14 9.80 17.54 o 6 14 0 183.13 210.95 15.97 o 7 14 0 1.64 -11.53 22.40 o 1 15 0 540.80 587.48 26.43 o 2 15 0 98.50 82.50 8.07 o 3 15 0 1609.81 1682.75 45.70 o 4 15 0 18.22 11.45 6.83 o 5 15 0 301.27 287.53 26.68 o 6 15 0 13.21 -16.39 20.75 o 7 15 0 176.59 165.17 15.73 o 0 16 0 116.07 105.56 8.81 o 1 16 0 4.04 -17.04 18.61 o 2 16 0 721.77 700.78 31.12 o 3 16 0 0.48 -17.04 19.93 o 4 16 0 497.94 508.69 30.55 o 5 16 0 17.46 28.24 6.92 o 6 16 0 109.01 124.74 12.19 o 1 17 0 194.02 212.93 15.48 o 2 17 0 180.42 172.66 16.71 o 3 17 0 464.84 451.38 30.55 o 4 17 0 6.72 10.05 12.19 o 5 17 0 72.90 69.16 7.82 o 0 18 0 253.05 284.15 25.85 o 1 18 0 27.28 14.49 15.07 o 2 18 0 349.75 317.50 27.58 o 3 18 0 0.48 -21.90 21.90 o 4 18 0 216.50 203.95 15.97 o 1 19 0 300.84 334.29 27.25 o 2 19 0 67.50 76.41 8.07 o 3 19 0 261.52 277.97 20.01 o 0 20 0 277.14 311.82 21.66 o -9 0 1 521.61 498.48 28.57 o -7 0 1 3740.23 3777.69 63.65 o -5 0 1 1219.90 1303.66 27.83 o -3 0 1 844.56 901.36 17.62 o -1 0 1 12107.50 17694.86 190.04 o 1 0 1 223.49 250.31 7.66 o 3 0 1 3689.41 3714.62 50.14 o 5 0 1 1033.78 1021.16 26.92 o 7 0 1 27.73 33.02 5.43 o -9 1 1 0.01 9.88 17.37 o -8 1 1 1087.10 1079.70 35.90 o -7 1 1 134.76 160.40 12.76 o -6 1 1 2940.94 2862.50 48.83 o -5 1 1 1044.19 1103.50 25.11 o -4 1 1 35.80 51.79 4.78 o -3 1 1 1476.08 1590.70 25.11 o -2 1 1 18979.22 28204.37 306.13 o -1 1 1 4.43 -3.95 3.95 o 0 1 1 9648.93 11240.99 2822.27 o 1 1 1 257.38 285.39 8.48 o 2 1 1 3811.12 3982.46 49.81 o 3 1 1 908.54 956.20 21.00 o 4 1 1 6507.61 7036.07 88.02 o 5 1 1 495.97 517.91 19.84 o 6 1 1 518.26 559.65 23.05 o 7 1 1 3.45 3.29 14.00 o 8 1 1 442.18 457.55 27.42 o -9 2 1 423.34 387.90 26.35 o -8 2 1 31.16 5.85 18.44 o -7 2 1 3762.35 3842.73 63.57 o -6 2 1 264.19 273.36 17.37 o -5 2 1 2270.47 2350.27 39.60 o -4 2 1 501.08 544.09 16.06 o -3 2 1 4297.65 4174.64 52.12 o -2 2 1 50.75 56.07 4.36 o -1 2 1 24182.81 21288.60 218.20 o 0 2 1 7591.15 7486.95 225.98 o 1 2 1 2428.96 2661.26 34.25 o 2 2 1 175.89 195.88 10.29 o 3 2 1 7318.01 7796.54 92.30 o 4 2 1 252.45 380.90 15.97 o 5 2 1 3133.75 3228.00 52.70 o 6 2 1 26.58 30.79 4.94 o 7 2 1 257.26 304.08 19.93 o 8 2 1 215.59 209.47 15.97 o -9 3 1 45.64 42.57 6.67 o -8 3 1 469.37 474.10 25.52 o -7 3 1 22.41 42.07 5.68 o -6 3 1 1846.50 1875.59 38.12 o -5 3 1 296.62 309.02 15.31 o -4 3 1 93.11 59.61 5.27 o -3 3 1 881.59 884.89 18.03 o -2 3 1 9541.78 8812.52 96.83 o -1 3 1 10490.65 10653.11 113.38 o 0 3 1 12876.46 12646.46 107.16 o 1 3 1 1534.30 1802.64 26.60 o 2 3 1 6271.03 6558.50 77.32 o 3 3 1 64.65 81.27 7.00 o 4 3 1 4968.17 5073.61 68.92 o 5 3 1 177.04 198.27 15.97 o 6 3 1 723.12 776.86 27.17 o 7 3 1 136.68 128.94 11.20 o 8 3 1 375.33 365.75 25.44 o -9 4 1 109.35 122.11 12.10 o -8 4 1 3.06 -16.96 16.96 o -7 4 1 2209.68 2211.86 45.94 o -6 4 1 1296.92 1259.12 31.78 o -5 4 1 1869.89 1835.74 35.16 o -4 4 1 228.97 258.38 12.76 o -3 4 1 1766.83 1613.67 27.09 o -2 4 1 3671.40 3707.04 46.77 o -1 4 1 4933.02 4688.76 55.41 o 0 4 1 116.43 118.47 22.85 o 1 4 1 4.58 13.17 2.47 o 2 4 1 132.23 141.46 9.88 o 3 4 1 2921.66 2920.22 43.89 o 4 4 1 2.27 -11.45 11.45 o 5 4 1 3542.64 3620.01 58.62 o 6 4 1 552.17 544.17 24.78 o 7 4 1 450.84 420.75 24.95 o 8 4 1 166.60 170.36 13.01 o -9 5 1 256.67 246.36 24.62 o -8 5 1 339.58 320.30 23.38 o -7 5 1 4.97 15.73 16.88 o -6 5 1 2246.67 2250.31 43.80 o -5 5 1 817.79 853.27 24.29 o -4 5 1 6339.33 6062.33 77.56 o -3 5 1 0.34 5.85 2.80 o -2 5 1 10344.11 9895.43 110.83 o -1 5 1 17.03 8.56 2.22 o 0 5 1 2851.92 2642.44 208.56 o 1 5 1 2045.26 2155.04 32.19 o 2 5 1 592.88 610.79 16.47 o 3 5 1 9.47 2.88 9.72 o 4 5 1 3081.71 3122.77 50.14 o 5 5 1 544.76 607.49 23.30 o 6 5 1 2009.12 2056.16 45.29 o 7 5 1 3.39 7.33 17.62 o 8 5 1 497.80 449.32 28.41 o -9 6 1 272.61 264.22 18.44 o -8 6 1 153.75 123.84 11.36 o -7 6 1 1714.33 1760.81 42.07 o -6 6 1 176.67 194.98 18.03 o -5 6 1 4398.84 4335.12 64.31 o -4 6 1 0.32 9.55 9.96 o -3 6 1 6631.12 6478.06 80.20 o -2 6 1 26.30 29.39 2.88 o -1 6 1 4469.59 4254.76 54.92 o 0 6 1 673.82 646.68 65.05 o 1 6 1 1467.72 1512.64 26.92 o 2 6 1 225.79 222.97 12.02 o 3 6 1 2402.64 2521.45 41.91 o 4 6 1 976.25 948.29 26.35 o 5 6 1 2276.14 2436.31 46.93 o 6 6 1 61.27 71.47 6.67 o 7 6 1 337.48 359.00 24.29 o 8 6 1 150.70 133.80 13.34 o -8 7 1 60.40 64.22 6.83 o -7 7 1 8.23 11.03 16.14 o -6 7 1 47.58 57.97 5.60 o -5 7 1 294.68 283.16 17.29 o -4 7 1 2245.13 2206.34 39.03 o -3 7 1 199.92 234.42 13.09 o -2 7 1 3757.16 3723.51 51.96 o -1 7 1 128.59 101.19 9.47 o 0 7 1 2224.09 1993.43 115.36 o 1 7 1 12.58 0.08 8.48 o 2 7 1 1349.17 1235.32 26.43 o 3 7 1 3255.35 3381.64 52.37 o 4 7 1 3242.57 3432.28 55.74 o 5 7 1 146.58 145.41 12.60 o 6 7 1 2617.42 2760.81 54.76 o 7 7 1 87.25 85.96 8.32 o 8 7 1 491.57 543.85 29.64 o -8 8 1 146.73 140.39 12.52 o -7 8 1 218.48 264.97 21.49 o -6 8 1 94.19 92.96 9.22 o -5 8 1 1743.51 1745.49 38.04 o -4 8 1 38.26 32.19 4.03 o -3 8 1 2618.40 2573.98 43.23 o -2 8 1 687.87 724.25 20.34 o -1 8 1 1110.38 1030.63 23.71 o 0 8 1 3877.94 3690.30 314.90 o 1 8 1 4683.50 4567.97 62.58 o 2 8 1 14.05 6.50 10.62 o 3 8 1 1420.62 1356.11 31.45 o 4 8 1 513.23 515.19 22.40 o 5 8 1 585.06 604.20 26.02 o 6 8 1 131.68 150.43 11.86 o 7 8 1 533.94 555.95 29.72 o 8 8 1 7.40 8.73 9.88 o -8 9 1 812.41 772.66 35.98 o -7 9 1 5.01 2.06 16.63 o -6 9 1 293.86 325.90 20.83 o -5 9 1 10.07 18.94 4.94 o -4 9 1 1486.17 1433.92 33.10 o -3 9 1 425.97 439.11 18.53 o -2 9 1 1857.35 1808.15 34.91 o -1 9 1 297.22 270.65 14.66 o 0 9 1 5359.82 4761.00 232.28 o 1 9 1 28.38 -11.77 11.77 o 2 9 1 4235.19 4099.55 61.01 o 3 9 1 2023.55 2167.07 41.66 o 4 9 1 948.64 1005.52 29.64 o 5 9 1 118.33 123.26 12.10 o 6 9 1 471.18 469.49 26.18 o 7 9 1 239.64 265.05 24.87 o 8 9 1 185.87 198.35 17.37 o -8 10 1 17.84 33.35 7.25 o -7 10 1 553.36 564.84 27.67 o -6 10 1 8.17 3.46 7.00 o -5 10 1 1455.81 1408.48 35.65 o -4 10 1 82.80 70.73 6.01 o -3 10 1 961.57 922.11 25.85 o -2 10 1 159.64 127.38 9.80 o -1 10 1 532.94 514.45 19.02 o 0 10 1 250.83 99.75 14.45 o 1 10 1 6816.08 6406.42 86.37 o 2 10 1 250.77 212.52 17.62 o 3 10 1 1001.89 1025.36 29.07 o 4 10 1 87.09 104.73 9.55 o 5 10 1 50.16 54.01 5.76 o 6 10 1 31.66 32.28 6.18 o 7 10 1 525.21 561.30 31.21 o 8 10 1 110.35 108.28 10.79 o -8 11 1 512.97 534.29 32.11 o -7 11 1 13.81 17.46 6.26 o -6 11 1 386.89 407.49 24.04 o -5 11 1 47.30 37.13 5.76 o -4 11 1 1071.45 918.24 29.97 o -3 11 1 152.40 163.19 16.06 o -2 11 1 106.14 103.99 10.05 o -1 11 1 20.06 4.94 11.45 o 0 11 1 2796.25 2611.32 138.37 o 1 11 1 101.78 73.94 7.16 o 2 11 1 3616.91 3476.74 58.54 o 3 11 1 53.01 48.99 5.43 o 4 11 1 106.24 111.98 9.80 o 5 11 1 21.07 16.47 5.60 o 6 11 1 209.18 205.52 16.14 o 7 11 1 0.78 15.89 19.27 o 8 11 1 352.75 352.66 30.38 o -7 12 1 199.56 204.69 16.80 o -6 12 1 402.74 398.02 25.20 o -5 12 1 752.33 728.53 28.98 o -4 12 1 150.26 132.48 10.87 o -3 12 1 698.49 640.02 25.69 o -2 12 1 150.88 133.55 11.45 o -1 12 1 303.47 272.95 19.27 o 0 12 1 14.15 -14.39 14.39 o 1 12 1 3796.60 3355.70 58.95 o 2 12 1 62.28 68.26 6.34 o 3 12 1 732.77 762.45 28.16 o 4 12 1 212.96 219.93 19.18 o 5 12 1 120.85 117.00 11.12 o 6 12 1 4.55 -4.36 13.83 o 7 12 1 523.90 479.05 33.59 o -7 13 1 60.73 57.39 7.08 o -6 13 1 348.41 336.85 24.62 o -5 13 1 201.58 196.54 15.81 o -4 13 1 1968.26 2032.11 47.26 o -3 13 1 82.47 80.20 7.90 o -2 13 1 131.93 129.68 11.61 o -1 13 1 393.74 389.21 22.48 o 0 13 1 1017.17 932.68 21.77 o 1 13 1 22.52 -14.41 16.47 o 2 13 1 2386.22 2307.70 48.42 o 3 13 1 169.41 196.29 18.53 o 4 13 1 267.80 275.09 22.23 o 5 13 1 45.74 45.20 6.59 o 6 13 1 652.49 660.68 34.01 o 7 13 1 20.96 8.32 9.72 o -7 14 1 44.27 27.50 7.25 o -6 14 1 3.16 1.40 13.01 o -5 14 1 1194.93 1187.81 39.28 o -4 14 1 7.74 15.48 18.36 o -3 14 1 2278.31 2272.38 51.05 o -2 14 1 79.92 77.40 7.49 o -1 14 1 344.46 278.47 21.00 o 0 14 1 63.64 6.85 13.70 o 1 14 1 548.34 489.34 25.69 o 2 14 1 2.82 -17.54 17.54 o 3 14 1 126.10 124.41 10.95 o 4 14 1 5.47 -9.80 17.62 o 5 14 1 293.19 264.80 18.03 o 6 14 1 133.10 134.46 12.52 o 7 14 1 565.44 543.85 37.55 o -7 15 1 1.68 8.65 20.50 o -6 15 1 147.41 152.82 13.59 o -5 15 1 31.21 -13.42 21.33 o -4 15 1 1475.62 1551.01 45.45 o -3 15 1 19.44 -20.26 20.26 o -2 15 1 150.50 161.80 13.75 o -1 15 1 40.45 22.89 5.93 o 0 15 1 162.60 139.14 9.11 o 1 15 1 75.92 74.43 6.83 o 2 15 1 833.91 796.62 32.03 o 3 15 1 16.84 16.63 17.29 o 4 15 1 231.84 270.89 21.90 o 5 15 1 6.43 19.43 20.17 o 6 15 1 492.34 503.25 34.01 o 7 15 1 3.52 -0.58 26.02 o -7 16 1 8.49 -11.28 23.55 o -6 16 1 41.26 53.03 7.58 o -5 16 1 503.50 504.82 32.03 o -4 16 1 29.61 -2.06 20.67 o -3 16 1 1232.19 1226.76 42.07 o -2 16 1 282.79 298.48 25.69 o -1 16 1 236.54 230.55 22.48 o 0 16 1 47.45 29.75 10.13 o 1 16 1 250.40 244.55 21.74 o 2 16 1 25.74 -0.41 19.60 o 3 16 1 195.64 233.10 22.81 o 4 16 1 0.02 2.22 18.11 o 5 16 1 341.62 350.35 29.72 o 6 16 1 43.99 22.15 25.03 o -6 17 1 121.03 126.88 11.45 o -5 17 1 51.95 60.35 7.99 o -4 17 1 648.46 690.24 32.52 o -3 17 1 91.28 59.61 8.07 o -2 17 1 371.18 382.05 26.51 o -1 17 1 48.50 31.54 7.00 o 0 17 1 360.97 358.90 19.51 o 1 17 1 32.21 3.46 22.40 o 2 17 1 605.58 628.16 32.28 o 3 17 1 4.94 6.67 18.20 o 4 17 1 185.61 170.28 14.41 o 5 17 1 59.45 60.27 8.40 o -5 18 1 96.32 101.52 9.80 o -4 18 1 3.37 -4.61 21.66 o -3 18 1 161.62 155.54 13.50 o -2 18 1 92.79 87.94 8.81 o -1 18 1 206.17 194.48 16.80 o 0 18 1 10.83 -15.54 15.54 o 1 18 1 573.42 594.81 34.50 o 2 18 1 20.21 -17.21 21.90 o 3 18 1 336.95 327.71 28.90 o 4 18 1 34.24 18.44 21.82 o -3 19 1 33.09 39.60 7.49 o -2 19 1 153.55 166.41 13.59 o -1 19 1 0.39 9.96 20.83 o 0 19 1 304.03 308.93 20.11 o 1 19 1 21.95 23.55 23.71 o 2 19 1 347.28 418.86 30.96 o 3 19 1 29.21 40.02 7.99 o -8 0 2 4538.54 4300.13 72.38 o -6 0 2 2768.05 2715.60 46.36 o -4 0 2 3873.27 3974.06 52.53 o -2 0 2 314.36 269.74 8.40 o 0 0 2 3534.33 3855.55 31.88 o 2 0 2 15407.51 14968.22 162.21 o 4 0 2 5532.88 5811.69 77.73 o 6 0 2 11.17 0.08 14.24 o 8 0 2 410.99 425.03 28.65 o -9 1 2 1066.51 1001.15 36.64 o -8 1 2 57.92 83.41 8.23 o -7 1 2 4075.48 4014.33 64.31 o -6 1 2 136.74 151.75 13.42 o -5 1 2 177.84 159.57 11.12 o -4 1 2 56.31 66.94 6.18 o -3 1 2 3333.63 3136.93 41.09 o -2 1 2 1450.25 1470.65 21.74 o -1 1 2 6727.55 6431.54 70.56 o 0 1 2 4589.96 4701.72 38.13 o 1 1 2 25252.41 22940.15 238.78 o 2 1 2 676.78 798.77 18.69 o 3 1 2 8833.03 9084.98 107.45 o 4 1 2 1108.54 1156.11 27.83 o 5 1 2 98.05 84.97 8.15 o 6 1 2 44.29 61.84 5.68 o 7 1 2 53.04 71.47 6.50 o 8 1 2 39.99 48.58 6.83 o -9 2 2 145.32 147.47 12.35 o -8 2 2 1694.69 1651.21 41.75 o -7 2 2 83.77 112.06 10.79 o -6 2 2 475.46 463.98 19.10 o -5 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