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Information card for entry 2008474
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| Coordinates | 2008474.cif |
|---|---|
| Original IUCr paper | HTML |
| Chemical name | cis-chlorohydridotetrakis(triethylphosphine)iridium(III) bis(catecholato)borate |
|---|---|
| Formula | C36 H69 B Cl Ir O4 P4 |
| Calculated formula | C36 H69 B Cl Ir O4 P4 |
| Title of publication | Salts of the bis(catecholato)borate anion with rhodium‒ and iridium‒phosphine complex cations |
| Authors of publication | Clegg, William; Elsegood, Mark R.J.; Scott, Andrew J.; Marder, Todd B.; Dai, Chaoyang; Norman, Nicholas C.; Pickett, Nigel L.; Robins, Edward G. |
| Journal of publication | Acta Crystallographica Section C |
| Year of publication | 1999 |
| Journal volume | 55 |
| Journal issue | 5 |
| Pages of publication | 733 - 739 |
| a | 14.276 ± 0.003 Å |
| b | 15.29 ± 0.003 Å |
| c | 19.807 ± 0.004 Å |
| α | 90° |
| β | 102.36 ± 0.02° |
| γ | 90° |
| Cell volume | 4223.3 ± 1.5 Å3 |
| Cell temperature | 298 ± 2 K |
| Ambient diffraction temperature | 298 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.05 |
| Residual factor for significantly intense reflections | 0.0289 |
| Weighted residual factors for all reflections included in the refinement | 0.0796 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.02 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
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