#------------------------------------------------------------------------------
#$Date: 2016-04-02 18:34:11 +0100 (Sat, 02 Apr 2016) $
#$Revision: 180768 $
#$URL: svn://www.crystallography.net/cod/hkl/2/00/89/2008918.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2008918_Fobs
loop_
_publ_author_name
'Thu\'ery, P.'
'Nierlich, M.'
'Charbonnel, M.-C.'
'Dognon, J.-P.'
_publ_section_title
;
 Bis[2-(2-ethoxyethyl)-<i>N</i>,<i>N</i>,<i>N</i>',<i>N</i>'-tetraethylmalondiamide-<i>O</i>^1^,<i>O</i>^3^]tris(nitrato-<i>O</i>,<i>O</i>')lanthanum(III)
;
_journal_issue                   9
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1434
_journal_page_last               1436
_journal_volume                  55
_journal_year                    1999
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_exptl_crystal_F_000             1864.00
_cod_data_source_file            gs1046sup2.hkl
_cod_data_source_block           1
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     P2(1)/n
_shelx_refln_list_code           4
_shelx_f_calc_maximum            368.50
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 30191.10 26814.81 766.90 x
4 0 0 113.86 53.74 16.17 x
6 0 0 8562.67 7962.17 187.81 o
8 0 0 8526.84 8856.62 209.98 o
2 1 0 60.15 94.43 7.04 x
3 1 0 4590.86 4346.80 72.52 o
4 1 0 3391.70 3083.76 52.95 o
5 1 0 8839.22 8397.27 168.77 o
6 1 0 9874.90 10086.27 176.60 o
7 1 0 3023.86 2967.68 52.95 o
8 1 0 8103.22 8345.36 139.29 o
9 1 0 7837.83 8203.72 241.81 o
1 2 0 8957.06 1468.06 171.12 x
2 2 0 20030.80 18315.81 391.27 x
3 2 0 61349.91 57567.40 942.19 o
4 2 0 6281.30 6065.01 100.17 o
5 2 0 6358.90 5942.41 99.38 o
6 2 0 1551.85 1445.89 29.22 o
7 2 0 1612.29 1436.76 30.78 o
8 2 0 757.62 783.59 31.30 o
9 2 0 10041.10 10487.19 376.41 o
1 3 0 61888.24 27748.91 1094.79 x
2 3 0 4577.53 4138.64 88.69 x
3 3 0 40317.86 37670.32 660.73 o
4 3 0 3082.41 3043.59 56.87 o
5 3 0 35232.30 34760.29 576.22 o
6 3 0 1863.56 2014.54 37.30 o
7 3 0 848.52 689.69 23.74 o
8 3 0 5164.99 5116.30 137.99 o
9 3 0 4849.63 4911.80 232.94 o
0 4 0 135792.27 -6.52 7.83 x
1 4 0 238.24 198.77 7.04 x
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5 4 0 62.73 47.74 15.39 o
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7 4 0 333.79 350.06 21.91 o
8 4 0 38.33 143.73 33.39 o
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2 5 0 251.04 313.54 11.22 x
3 5 0 5680.69 5466.88 111.90 o
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9 5 0 0.19 -31.56 56.60 o
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1 7 0 69376.79 63386.43 1208.26 x
2 7 0 2603.49 2526.59 45.39 o
3 7 0 42335.18 40454.63 719.16 o
4 7 0 251.88 205.03 15.91 o
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6 7 0 543.85 469.79 25.04 o
7 7 0 7245.17 7797.84 303.37 o
8 7 0 41.51 26.87 30.52 o
0 8 0 55428.03 49774.52 1211.12 o
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2 8 0 7389.64 7088.85 133.82 o
3 8 0 627.07 562.13 19.30 o
4 8 0 1900.88 1623.27 31.82 o
5 8 0 4712.58 4855.71 88.17 o
6 8 0 588.34 730.64 22.95 o
7 8 0 2934.24 3074.37 67.82 o
12 8 0 31.72 113.47 80.86 o
1 9 0 11841.84 10806.21 193.03 o
2 9 0 3513.72 3697.28 65.21 o
3 9 0 7365.55 6846.52 117.64 o
4 9 0 18594.46 17707.25 314.32 o
5 9 0 14717.63 15629.06 397.80 o
6 9 0 3944.22 3956.30 132.25 o
7 9 0 4268.71 4385.66 105.12 o
12 9 0 1097.89 945.32 90.78 o
0 10 0 32393.96 30752.85 749.42 o
1 10 0 2008.35 1762.30 32.61 o
2 10 0 20772.04 19130.70 365.71 o
3 10 0 130.02 122.60 15.13 o
4 10 0 65826.63 66341.07 1086.70 o
5 10 0 4920.31 5299.16 125.47 o
6 10 0 11005.64 10809.60 347.71 o
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9 10 0 1199.81 1077.31 77.47 o
12 10 0 336.63 346.15 64.95 o
1 11 0 23162.21 21620.77 386.06 o
2 11 0 3.27 -15.91 16.69 o
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4 11 0 304.55 194.59 17.22 o
5 11 0 5044.80 4802.50 82.69 o
6 11 0 4220.76 4387.23 75.65 o
7 11 0 28.14 70.43 38.61 o
8 11 0 2070.08 2045.58 63.91 o
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10 11 0 3974.36 4094.82 114.25 o
11 11 0 1778.99 1750.30 100.69 o
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1 12 0 1020.71 1018.10 22.95 o
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8 12 0 1180.05 1116.96 34.43 o
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10 12 0 59.98 -40.95 56.34 o
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2 13 0 0.33 -48.26 17.74 o
3 13 0 13214.54 12593.81 240.76 o
4 13 0 110.25 93.12 18.26 o
5 13 0 7793.70 7762.36 130.95 o
6 13 0 3107.34 3162.28 58.69 o
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8 13 0 2628.14 2584.24 55.04 o
9 13 0 3951.57 4022.82 81.91 o
10 13 0 393.55 349.28 41.48 o
11 13 0 336.05 422.58 54.00 o
12 13 0 372.66 225.37 57.39 o
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1 14 0 2279.66 2462.42 45.65 o
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3 14 0 4401.65 4669.47 86.08 o
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5 14 0 828.89 1052.27 33.39 o
6 14 0 8721.09 9384.32 158.86 o
7 14 0 10.01 -39.13 27.13 o
8 14 0 346.70 353.71 31.82 o
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12 14 0 153.42 134.86 59.21 o
1 15 0 403.64 485.18 20.61 o
2 15 0 157.31 142.42 19.04 o
3 15 0 6.21 -10.96 23.74 o
4 15 0 242.63 196.42 23.48 o
5 15 0 1309.38 1248.43 39.91 o
6 15 0 6024.61 6427.33 111.38 o
7 15 0 5.68 -95.21 32.08 o
8 15 0 8827.02 9246.59 191.20 o
9 15 0 8.07 33.65 39.65 o
10 15 0 5358.89 5405.32 112.17 o
11 15 0 99.01 173.20 48.78 o
12 15 0 1554.93 1440.93 68.60 o
0 16 0 33143.91 33281.27 790.37 o
1 16 0 516.44 452.57 23.22 o
2 16 0 4664.76 4531.48 79.56 o
3 16 0 8.61 39.65 22.69 o
4 16 0 9202.94 9472.49 159.90 o
5 16 0 3789.66 3984.74 75.65 o
6 16 0 5248.89 5099.87 92.86 o
7 16 0 5308.70 5375.33 105.64 o
8 16 0 896.78 812.02 40.43 o
9 16 0 1223.79 1118.00 45.65 o
10 16 0 873.44 806.29 47.74 o
11 16 0 272.98 238.68 50.34 o
1 17 0 13694.11 13456.70 239.20 o
2 17 0 6.29 9.91 26.08 o
3 17 0 4178.80 4114.90 73.82 o
4 17 0 0.95 -30.78 25.30 o
5 17 0 15481.74 16488.30 301.80 o
6 17 0 6.53 -15.39 32.61 o
7 17 0 5919.50 6224.13 116.34 o
8 17 0 254.46 302.32 30.52 o
9 17 0 1918.78 2014.02 51.65 o
10 17 0 112.55 77.99 42.26 o
11 17 0 7.07 109.04 52.43 o
12 17 0 52.48 1138.61 498.48 o
0 18 0 25070.06 25720.02 665.43 o
1 18 0 100.48 159.12 27.39 o
2 18 0 14.23 46.95 24.52 o
3 18 0 574.58 674.04 25.30 o
4 18 0 4303.35 4380.19 80.34 o
5 18 0 1674.42 1697.87 41.48 o
6 18 0 2255.96 2180.96 49.04 o
7 18 0 4566.33 4536.17 87.65 o
8 18 0 274.83 322.15 37.82 o
9 18 0 2126.93 2185.40 57.65 o
10 18 0 192.39 195.38 41.21 o
11 18 0 1299.77 1333.72 59.47 o
1 19 0 341.50 400.66 27.39 o
2 19 0 1601.59 1461.54 36.78 o
3 19 0 674.57 586.91 29.74 o
4 19 0 498.63 454.92 30.78 o
5 19 0 9317.41 9821.77 183.12 o
6 19 0 2600.24 2639.28 62.60 o
7 19 0 1625.48 1609.44 48.00 o
8 19 0 6717.53 6989.20 144.77 o
9 19 0 82.99 27.39 41.48 o
10 19 0 3687.52 3381.65 80.08 o
11 19 0 140.36 67.56 65.47 o
0 20 0 10694.00 10111.05 266.07 o
1 20 0 35.80 25.30 36.52 o
2 20 0 11169.52 11921.08 211.81 o
3 20 0 1677.65 1672.57 41.48 o
4 20 0 19334.22 20211.66 379.80 o
5 20 0 1.83 -46.43 28.95 o
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9 20 0 455.16 521.18 45.39 o
10 20 0 1751.55 1759.95 61.56 o
11 20 0 35.94 77.99 57.91 o
1 21 0 9733.19 9951.41 178.42 o
2 21 0 250.48 264.24 26.35 o
3 21 0 8012.20 8029.47 143.99 o
4 21 0 931.26 757.77 39.13 o
5 21 0 3525.24 3560.07 71.21 o
6 21 0 2881.08 3017.25 61.56 o
7 21 0 1978.99 2060.45 50.87 o
8 21 0 275.90 319.54 46.95 o
9 21 0 2698.05 2733.18 69.91 o
10 21 0 2282.05 2138.18 63.13 o
11 21 0 379.65 219.64 57.65 o
0 22 0 771.63 856.11 46.17 o
1 22 0 728.38 645.60 37.56 o
2 22 0 1.16 88.43 32.35 o
3 22 0 4842.85 4910.23 98.34 o
4 22 0 4963.66 4972.31 100.95 o
5 22 0 879.83 805.76 40.43 o
6 22 0 694.05 666.99 44.34 o
7 22 0 1184.39 1134.70 46.43 o
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10 22 0 27.17 -135.12 58.17 o
11 22 0 3087.86 2358.86 107.99 o
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7 23 0 1974.05 2005.93 55.04 o
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3 24 0 48.76 -12.26 33.65 o
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1 25 0 505.87 407.45 33.13 o
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3 29 0 1763.08 1738.82 58.43 o
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1 30 0 25.57 -10.69 46.43 o
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1 1 1 20758.39 10387.81 539.96 x
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