#------------------------------------------------------------------------------
#$Date: 2008-11-20 19:58:43 +0000 (Thu, 20 Nov 2008) $
#$Revision: 481 $
#$URL: svn://www.crystallography.net/cod/cif/2/2008938.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2008938
_journal_name_full 'Acta Crystallographica Section C'
_journal_year  1999
_journal_volume 55
_journal_page_first  1412
_journal_page_last  1413
_publ_section_title
;
[4-(4-Methylphenyl)-3,5-bis(2-pyridyl)-4H-1,2,4-triazole]-
bis(triphenylphosphine)silver(I) perchlorate
;
loop_
_publ_author_name
  'Shao, Si-Chang'
  'Zhu, Dun-Ru'
  'Zhu, Xu-Hui'
  'You, Xiao-Zeng'
  'Shanmuga Sundara Raj, S.'
  'Fun, Hoong-Kun'
_chemical_formula_sum  'C55 H45 Ag Cl N5 O4 P2'
_chemical_formula_iupac  '[Ag (C19 H15 N5) (C18 H15 P)2] Cl O4'
_chemical_formula_weight  1045.22
_symmetry_cell_setting  Monoclinic
_symmetry_space_group_name_H-M  'P 21/c'
loop_
_symmetry_equiv_pos_as_xyz
  'x, y, z'
  '-x, y+1/2, -z+1/2'
  '-x, -y, -z'
  'x, -y-1/2, z-1/2'
_cell_length_a  16.7610(2)
_cell_length_b  14.2287(2)
_cell_length_c  21.1305(2)
_cell_angle_alpha  90.00
_cell_angle_beta  97.6910(10)
_cell_angle_gamma  90.00
_cell_volume  4994.02(10)
_cell_formula_units_Z  4
_cell_measurement_temperature  293(2)
_exptl_crystal_density_diffrn  1.390
_diffrn_ambient_temperature  293(2)
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
_atom_site_type_symbol
  Ag1 0.267650(12) 0.533352(14) 0.097921(9) 0.04248(7) Uani d . 1 . . Ag
  P1 0.29601(4) 0.61667(5) 0.00264(3) 0.03844(15) Uani d . 1 . . P
  P2 0.31387(4) 0.59032(5) 0.20838(3) 0.04235(16) Uani d . 1 . . P
  Cl1 0.10082(5) 0.28039(5) 0.43382(3) 0.05518(18) Uani d . 1 . . Cl
  O1 0.09108(16) 0.25323(18) 0.36810(10) 0.0785(7) Uani d . 1 A . O
  O2A 0.1853(5) 0.2788(9) 0.4607(6) 0.131(5) Uani d P 0.60 A 1 O
  O3A 0.0653(5) 0.2190(5) 0.4737(4) 0.095(3) Uani d P 0.60 A 1 O
  O4A 0.0713(6) 0.3706(6) 0.4420(5) 0.103(4) Uani d P 0.60 A 1 O
  O2B 0.0277(8) 0.2513(14) 0.4560(7) 0.167(8) Uani d P 0.40 A 2 O
  O3B 0.1157(11) 0.3765(10) 0.4374(8) 0.130(7) Uani d P 0.40 A 2 O
  O4B 0.1633(10) 0.2358(12) 0.4634(7) 0.148(8) Uani d P 0.40 A 2 O
  N1 0.24848(12) 0.37268(15) 0.09490(10) 0.0404(5) Uani d . 1 . . N
  N2 0.30349(12) 0.30054(15) 0.09555(10) 0.0434(5) Uani d . 1 . . N
  N3 0.18873(11) 0.24286(14) 0.11933(9) 0.0364(4) Uani d . 1 . . N
  N4 0.12291(13) 0.48939(15) 0.10928(11) 0.0451(5) Uani d . 1 . . N
  N5 0.28260(19) 0.0643(2) 0.14826(17) 0.0845(10) Uani d . 1 . . N
  C1 0.40833(17) 0.6546(2) 0.22759(14) 0.0558(8) Uani d . 1 . . C
  C2 0.4791(2) 0.6130(4) 0.2135(2) 0.0929(13) Uani d . 1 . . C
  H2C 0.4774 0.5543 0.1940 0.111 Uiso calc R 1 . . H
  C3 0.5526(3) 0.6596(5) 0.2286(3) 0.123(2) Uani d . 1 . . C
  H3B 0.6001 0.6312 0.2202 0.147 Uiso calc R 1 . . H
  C4 0.5548(4) 0.7464(6) 0.2556(3) 0.137(3) Uani d . 1 . . C
  H4B 0.6038 0.7775 0.2647 0.164 Uiso calc R 1 . . H
  C5 0.4863(4) 0.7887(5) 0.2696(3) 0.135(2) Uani d . 1 . . C
  H5B 0.4888 0.8478 0.2886 0.162 Uiso calc R 1 . . H
  C6 0.4126(2) 0.7429(3) 0.25546(19) 0.0897(12) Uani d . 1 . . C
  H6A 0.3658 0.7718 0.2648 0.108 Uiso calc R 1 . . H
  C7 0.23555(16) 0.67170(19) 0.22602(13) 0.0458(6) Uani d . 1 . . C
  C8 0.2012(2) 0.7312(2) 0.17815(15) 0.0654(9) Uani d . 1 . . C
  H8A 0.2213 0.7329 0.1393 0.079 Uiso calc R 1 . . H
  C9 0.1361(3) 0.7889(3) 0.1879(2) 0.0899(13) Uani d . 1 . . C
  H9A 0.1129 0.8286 0.1556 0.108 Uiso calc R 1 . . H
  C10 0.1069(3) 0.7862(3) 0.2459(3) 0.0976(14) Uani d . 1 . . C
  H10A 0.0637 0.8242 0.2527 0.117 Uiso calc R 1 . . H
  C11 0.1405(2) 0.7289(3) 0.2928(2) 0.0849(11) Uani d . 1 . . C
  H11A 0.1201 0.7278 0.3316 0.102 Uiso calc R 1 . . H
  C12 0.20506(18) 0.6715(2) 0.28427(15) 0.0592(8) Uani d . 1 . . C
  H12A 0.2280 0.6330 0.3173 0.071 Uiso calc R 1 . . H
  C13 0.31832(16) 0.5035(2) 0.27287(13) 0.0454(6) Uani d . 1 . . C
  C14 0.3776(2) 0.5014(3) 0.32474(16) 0.0719(10) Uani d . 1 . . C
  H14A 0.4204 0.5434 0.3273 0.086 Uiso calc R 1 . . H
  C15 0.3732(2) 0.4362(3) 0.37327(18) 0.0854(12) Uani d . 1 . . C
  H15A 0.4135 0.4348 0.4081 0.102 Uiso calc R 1 . . H
  C16 0.3108(2) 0.3745(3) 0.37047(16) 0.0690(9) Uani d . 1 . . C
  H16A 0.3083 0.3316 0.4034 0.083 Uiso calc R 1 . . H
  C17 0.2522(2) 0.3755(2) 0.31960(15) 0.0630(8) Uani d . 1 . . C
  H17A 0.2091 0.3340 0.3180 0.076 Uiso calc R 1 . . H
  C18 0.25618(18) 0.4385(2) 0.26982(14) 0.0536(7) Uani d . 1 . . C
  H18A 0.2170 0.4371 0.2343 0.064 Uiso calc R 1 . . H
  C19 0.27046(16) 0.55785(19) -0.07378(12) 0.0430(6) Uani d . 1 . . C
  C20 0.2710(2) 0.6055(3) -0.13117(14) 0.0742(10) Uani d . 1 . . C
  H20A 0.2819 0.6696 -0.1308 0.089 Uiso calc R 1 . . H
  C21 0.2556(3) 0.5589(3) -0.18825(17) 0.0890(13) Uani d . 1 . . C
  H21A 0.2561 0.5917 -0.2262 0.107 Uiso calc R 1 . . H
  C22 0.2397(2) 0.4656(3) -0.19010(17) 0.0758(11) Uani d . 1 . . C
  H22A 0.2311 0.4343 -0.2291 0.091 Uiso calc R 1 . . H
  C23 0.2364(2) 0.4178(3) -0.13484(18) 0.0717(10) Uani d . 1 . . C
  H23A 0.2242 0.3540 -0.1362 0.086 Uiso calc R 1 . . H
  C24 0.25121(18) 0.4636(2) -0.07606(15) 0.0532(7) Uani d . 1 . . C
  H24A 0.2481 0.4307 -0.0385 0.064 Uiso calc R 1 . . H
  C25 0.40359(16) 0.64120(19) 0.00563(12) 0.0440(6) Uani d . 1 . . C
  C26 0.4409(2) 0.6906(3) 0.05676(16) 0.0796(12) Uani d . 1 . . C
  H26A 0.4108 0.7125 0.0876 0.096 Uiso calc R 1 . . H
  C27 0.5233(2) 0.7085(4) 0.06320(18) 0.0957(14) Uani d . 1 . . C
  H27A 0.5480 0.7416 0.0984 0.115 Uiso calc R 1 . . H
  C28 0.5679(2) 0.6773(3) 0.0177(2) 0.0784(11) Uani d . 1 . . C
  H28A 0.6230 0.6892 0.0217 0.094 Uiso calc R 1 . . H
  C29 0.5314(2) 0.6293(3) -0.0331(2) 0.0935(13) Uani d . 1 . . C
  H29A 0.5613 0.6089 -0.0645 0.112 Uiso calc R 1 . . H
  C30 0.4498(2) 0.6098(3) -0.03917(18) 0.0752(10) Uani d . 1 . . C
  H30A 0.4260 0.5751 -0.0739 0.090 Uiso calc R 1 . . H
  C31 0.24781(16) 0.73159(19) -0.00942(12) 0.0443(6) Uani d . 1 . . C
  C32 0.16820(18) 0.7395(2) 0.00141(14) 0.0584(8) Uani d . 1 . . C
  H32A 0.1420 0.6873 0.0154 0.070 Uiso calc R 1 . . H
  C33 0.1270(2) 0.8242(3) -0.00839(17) 0.0815(12) Uani d . 1 . . C
  H33A 0.0734 0.8282 -0.0017 0.098 Uiso calc R 1 . . H
  C34 0.1655(3) 0.9017(3) -0.02793(19) 0.0906(13) Uani d . 1 . . C
  H34A 0.1382 0.9586 -0.0339 0.109 Uiso calc R 1 . . H
  C35 0.2443(3) 0.8956(3) -0.0388(2) 0.0871(12) Uani d . 1 . . C
  H35A 0.2701 0.9484 -0.0522 0.105 Uiso calc R 1 . . H
  C36 0.2857(2) 0.8111(2) -0.02973(16) 0.0668(9) Uani d . 1 . . C
  H36A 0.3390 0.8075 -0.0373 0.080 Uiso calc R 1 . . H
  C37 0.18014(14) 0.33728(17) 0.10844(11) 0.0355(5) Uani d . 1 . . C
  C38 0.26693(14) 0.22337(19) 0.10965(12) 0.0404(6) Uani d . 1 . . C
  C39 0.30696(16) 0.13070(19) 0.11250(13) 0.0449(6) Uani d . 1 . . C
  C40 0.3217(3) -0.0183(3) 0.1496(3) 0.1089(17) Uani d . 1 . . C
  H40A 0.3043 -0.0662 0.1743 0.131 Uiso calc R 1 . . H
  C41 0.3840(3) -0.0367(3) 0.1178(2) 0.0854(12) Uani d . 1 . . C
  H41A 0.4091 -0.0951 0.1209 0.103 Uiso calc R 1 . . H
  C42 0.4094(3) 0.0325(3) 0.0810(2) 0.0985(15) Uani d . 1 . . C
  H42A 0.4525 0.0224 0.0583 0.118 Uiso calc R 1 . . H
  C43 0.3705(2) 0.1176(3) 0.07783(19) 0.0842(12) Uani d . 1 . . C
  H43A 0.3866 0.1658 0.0527 0.101 Uiso calc R 1 . . H
  C44 0.13068(14) 0.17876(17) 0.14142(12) 0.0369(5) Uani d . 1 . . C
  C45 0.11096(16) 0.1902(2) 0.20206(12) 0.0462(6) Uani d . 1 . . C
  H45A 0.1349 0.2375 0.2284 0.055 Uiso calc R 1 . . H
  C46 0.05484(16) 0.1302(2) 0.22347(13) 0.0519(7) Uani d . 1 . . C
  H46A 0.0407 0.1384 0.2642 0.062 Uiso calc R 1 . . H
  C47 0.01983(16) 0.0588(2) 0.18536(15) 0.0495(7) Uani d . 1 . . C
  C48 0.04181(18) 0.04839(19) 0.12454(15) 0.0521(7) Uani d . 1 . . C
  H48A 0.0188 0.0005 0.0983 0.063 Uiso calc R 1 . . H
  C49 0.09713(16) 0.10772(19) 0.10232(13) 0.0460(6) Uani d . 1 . . C
  H49A 0.1115 0.0998 0.0616 0.055 Uiso calc R 1 . . H
  C50 -0.0424(2) -0.0059(3) 0.20807(18) 0.0737(10) Uani d . 1 . . C
  H50A -0.0598 -0.0509 0.1753 0.111 Uiso calc R 1 . . H
  H50B -0.0876 0.0305 0.2173 0.111 Uiso calc R 1 . . H
  H50C -0.0190 -0.0382 0.2460 0.111 Uiso calc R 1 . . H
  C51 0.10697(14) 0.39642(18) 0.10767(11) 0.0373(5) Uani d . 1 . . C
  C52 0.02967(15) 0.3612(2) 0.10339(14) 0.0500(7) Uani d . 1 . . C
  H52A 0.0204 0.2968 0.1021 0.060 Uiso calc R 1 . . H
  C53 -0.03398(17) 0.4245(2) 0.10103(16) 0.0608(8) Uani d . 1 . . C
  H53A -0.0866 0.4027 0.0983 0.073 Uiso calc R 1 . . H
  C54 -0.01855(18) 0.5187(2) 0.10272(16) 0.0586(8) Uani d . 1 . . C
  H54A -0.0603 0.5620 0.1012 0.070 Uiso calc R 1 . . H
  C55 0.06024(17) 0.5481(2) 0.10666(15) 0.0541(7) Uani d . 1 . . C
  H55A 0.0704 0.6123 0.1075 0.065 Uiso calc R 1 . . H
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
  Ag1 0.04577(12) 0.03624(11) 0.04690(12) -0.00449(9) 0.01158(9) 0.00442(8)
  P1 0.0407(3) 0.0355(4) 0.0397(3) -0.0049(3) 0.0075(3) 0.0034(3)
  P2 0.0414(4) 0.0424(4) 0.0429(4) -0.0004(3) 0.0045(3) 0.0027(3)
  Cl1 0.0720(5) 0.0440(4) 0.0519(4) 0.0012(3) 0.0169(4) -0.0011(3)
  O1 0.1048(19) 0.0794(18) 0.0518(13) 0.0004(14) 0.0118(12) -0.0138(11)
  O2A 0.061(3) 0.234(15) 0.097(5) -0.019(6) 0.009(3) -0.004(7)
  O3A 0.133(8) 0.077(4) 0.081(4) -0.030(4) 0.035(5) 0.017(3)
  O4A 0.178(9) 0.052(5) 0.078(4) 0.050(6) 0.012(5) 0.003(3)
  O2B 0.100(9) 0.29(2) 0.128(12) -0.066(10) 0.077(9) -0.080(12)
  O3B 0.26(2) 0.045(6) 0.088(6) -0.043(10) 0.045(11) -0.022(4)
  O4B 0.212(19) 0.146(12) 0.069(6) 0.126(13) -0.047(10) -0.012(7)
  N1 0.0353(11) 0.0355(12) 0.0520(13) 0.0007(9) 0.0120(10) 0.0006(9)
  N2 0.0356(11) 0.0382(13) 0.0585(13) 0.0036(9) 0.0135(10) 0.0049(10)
  N3 0.0339(10) 0.0327(11) 0.0436(11) 0.0003(8) 0.0088(9) 0.0032(9)
  N4 0.0411(12) 0.0327(12) 0.0629(14) -0.0006(9) 0.0120(11) 0.0007(10)
  N5 0.087(2) 0.0582(18) 0.118(3) 0.0275(16) 0.051(2) 0.0344(18)
  C1 0.0470(16) 0.067(2) 0.0526(17) -0.0077(15) 0.0022(13) 0.0149(15)
  C2 0.055(2) 0.113(4) 0.112(3) 0.001(2) 0.015(2) 0.024(3)
  C3 0.047(2) 0.189(7) 0.129(4) -0.013(3) 0.002(3) 0.056(4)
  C4 0.090(4) 0.204(8) 0.106(4) -0.079(5) -0.024(3) 0.053(4)
  C5 0.125(5) 0.144(6) 0.130(4) -0.079(4) -0.007(4) -0.017(4)
  C6 0.078(3) 0.086(3) 0.102(3) -0.031(2) 0.000(2) -0.013(2)
  C7 0.0452(14) 0.0382(15) 0.0515(16) -0.0012(12) -0.0030(12) -0.0050(12)
  C8 0.078(2) 0.052(2) 0.0615(19) 0.0175(17) -0.0092(17) -0.0049(15)
  C9 0.093(3) 0.063(3) 0.103(3) 0.025(2) -0.024(3) -0.006(2)
  C10 0.077(3) 0.081(3) 0.137(4) 0.031(2) 0.021(3) -0.018(3)
  C11 0.090(3) 0.070(3) 0.102(3) 0.013(2) 0.038(2) -0.014(2)
  C12 0.0623(19) 0.0510(19) 0.066(2) 0.0022(15) 0.0143(16) -0.0061(15)
  C13 0.0419(15) 0.0496(16) 0.0456(15) 0.0053(12) 0.0095(12) 0.0069(12)
  C14 0.0531(19) 0.084(3) 0.073(2) -0.0126(17) -0.0096(17) 0.0284(19)
  C15 0.067(2) 0.107(3) 0.074(2) -0.009(2) -0.0173(19) 0.041(2)
  C16 0.065(2) 0.075(2) 0.067(2) 0.0058(18) 0.0095(18) 0.0307(18)
  C17 0.066(2) 0.056(2) 0.070(2) -0.0049(16) 0.0165(17) 0.0093(16)
  C18 0.0552(17) 0.0551(18) 0.0499(16) -0.0026(14) 0.0043(14) 0.0061(13)
  C19 0.0409(14) 0.0420(16) 0.0453(15) 0.0004(11) 0.0036(12) 0.0003(11)
  C20 0.120(3) 0.053(2) 0.0474(18) -0.006(2) 0.0006(19) 0.0053(15)
  C21 0.137(4) 0.079(3) 0.0464(19) 0.000(3) -0.003(2) -0.0032(18)
  C22 0.073(2) 0.097(3) 0.056(2) -0.011(2) 0.0034(17) -0.028(2)
  C23 0.072(2) 0.059(2) 0.088(3) -0.0228(17) 0.0262(19) -0.0285(19)
  C24 0.0516(16) 0.0492(18) 0.0612(17) -0.0097(14) 0.0160(14) -0.0041(14)
  C25 0.0433(14) 0.0422(15) 0.0470(15) -0.0059(12) 0.0077(12) 0.0087(12)
  C26 0.060(2) 0.122(3) 0.059(2) -0.036(2) 0.0145(16) -0.016(2)
  C27 0.071(2) 0.146(4) 0.068(2) -0.052(3) 0.001(2) -0.005(2)
  C28 0.0422(17) 0.094(3) 0.097(3) -0.0158(18) 0.0023(19) 0.025(2)
  C29 0.053(2) 0.108(4) 0.127(4) -0.011(2) 0.041(2) -0.020(3)
  C30 0.0544(19) 0.087(3) 0.088(3) -0.0132(18) 0.0241(18) -0.024(2)
  C31 0.0522(16) 0.0403(15) 0.0398(14) -0.0002(12) 0.0045(12) 0.0004(11)
  C32 0.0563(18) 0.063(2) 0.0562(18) 0.0099(15) 0.0101(14) 0.0066(15)
  C33 0.075(2) 0.095(3) 0.073(2) 0.038(2) 0.0078(19) 0.000(2)
  C34 0.125(4) 0.056(2) 0.085(3) 0.038(2) -0.004(3) -0.002(2)
  C35 0.114(3) 0.043(2) 0.100(3) 0.003(2) 0.002(3) 0.0109(19)
  C36 0.073(2) 0.0442(19) 0.085(2) -0.0003(15) 0.0163(18) 0.0103(16)
  C37 0.0347(12) 0.0297(13) 0.0423(13) -0.0016(10) 0.0058(10) -0.0001(10)
  C38 0.0354(13) 0.0390(14) 0.0475(15) 0.0013(11) 0.0075(11) 0.0022(11)
  C39 0.0421(14) 0.0403(15) 0.0519(15) 0.0058(12) 0.0051(12) 0.0034(12)
  C40 0.117(4) 0.063(3) 0.159(4) 0.038(2) 0.065(3) 0.051(3)
  C41 0.088(3) 0.052(2) 0.115(3) 0.032(2) 0.012(2) 0.004(2)
  C42 0.106(3) 0.087(3) 0.112(3) 0.053(3) 0.052(3) 0.019(3)
  C43 0.097(3) 0.061(2) 0.105(3) 0.032(2) 0.050(2) 0.023(2)
  C44 0.0337(12) 0.0308(13) 0.0467(14) -0.0004(10) 0.0074(11) 0.0060(10)
  C45 0.0467(15) 0.0478(17) 0.0438(15) -0.0093(12) 0.0051(12) -0.0048(12)
  C46 0.0488(16) 0.0600(19) 0.0489(16) -0.0058(14) 0.0142(13) 0.0049(14)
  C47 0.0383(14) 0.0448(16) 0.0660(19) -0.0021(11) 0.0086(13) 0.0136(13)
  C48 0.0534(17) 0.0383(16) 0.0638(19) -0.0102(12) 0.0045(14) -0.0026(13)
  C49 0.0518(16) 0.0414(16) 0.0458(15) -0.0056(12) 0.0098(12) -0.0032(12)
  C50 0.064(2) 0.060(2) 0.103(3) -0.0128(17) 0.029(2) 0.0150(19)
  C51 0.0349(12) 0.0362(14) 0.0416(13) 0.0020(10) 0.0077(10) 0.0003(10)
  C52 0.0345(13) 0.0391(15) 0.0762(19) -0.0021(11) 0.0059(13) -0.0022(13)
  C53 0.0317(14) 0.058(2) 0.092(2) -0.0009(13) 0.0054(15) 0.0012(17)
  C54 0.0414(15) 0.054(2) 0.082(2) 0.0128(13) 0.0120(15) 0.0025(16)
  C55 0.0460(16) 0.0371(16) 0.081(2) 0.0051(12) 0.0155(15) 0.0028(14)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
  Ag1 N1 . 2.308(2) ?
  Ag1 P1 . 2.4380(10)
  ?
  Ag1 P2 . 2.4940(10)
  ?
  Ag1 N4 . 2.548(2) ?
  P1 C19 . 1.818(3) y
  P1 C31 . 1.826(3) y
  P1 C25 . 1.829(3) y
  P2 C7 . 1.826(3) y
  P2 C1 . 1.826(3) y
  P2 C13 . 1.834(3) y
  Cl1 O4B . 1.310(11) ?
  Cl1 O3B . 1.391(14) ?
  Cl1 O4A . 1.395(8) ?
  Cl1 O3A . 1.401(6) ?
  Cl1 O1 . 1.430(2) ?
  Cl1 O2B . 1.430(13) ?
  Cl1 O2A . 1.453(9) ?
  N1 C37 . 1.317(3) ?
  N1 N2 . 1.379(3) ?
  N2 C38 . 1.311(3) ?
  N3 C37 . 1.367(3) ?
  N3 C38 . 1.382(3) ?
  N3 C44 . 1.455(3) ?
  N4 C55 . 1.337(3) ?
  N4 C51 . 1.349(3) ?
  N5 C39 . 1.309(4) ?
  N5 C40 . 1.343(4) ?
  C1 C6 . 1.385(5) ?
  C1 C2 . 1.393(5) ?
  C2 C3 . 1.399(6) ?
  C3 C4 . 1.359(9) ?
  C4 C5 . 1.363(9) ?
  C5 C6 . 1.394(6) ?
  C7 C8 . 1.384(4) ?
  C7 C12 . 1.395(4) ?
  C8 C9 . 1.402(5) ?
  C9 C10 . 1.381(6) ?
  C10 C11 . 1.346(6) ?
  C11 C12 . 1.386(5) ?
  C13 C14 . 1.378(4) ?
  C13 C18 . 1.388(4) ?
  C14 C15 . 1.392(5) ?
  C15 C16 . 1.362(5) ?
  C16 C17 . 1.355(4) ?
  C17 C18 . 1.390(4) ?
  C19 C24 . 1.378(4) ?
  C19 C20 . 1.391(4) ?
  C20 C21 . 1.371(5) ?
  C21 C22 . 1.353(5) ?
  C22 C23 . 1.359(5) ?
  C23 C24 . 1.395(5) ?
  C25 C26 . 1.368(4) ?
  C25 C30 . 1.376(4) ?
  C26 C27 . 1.393(5) ?
  C27 C28 . 1.369(5) ?
  C28 C29 . 1.349(5) ?
  C29 C30 . 1.383(5) ?
  C31 C32 . 1.388(4) ?
  C31 C36 . 1.393(4) ?
  C32 C33 . 1.391(5) ?
  C33 C34 . 1.369(6) ?
  C34 C35 . 1.373(6) ?
  C35 C36 . 1.389(5) ?
  C37 C51 . 1.486(3) ?
  C38 C39 . 1.477(4) ?
  C39 C43 . 1.383(4) ?
  C40 C41 . 1.340(6) ?
  C41 C42 . 1.358(6) ?
  C42 C43 . 1.373(5) ?
  C44 C45 . 1.375(3) ?
  C44 C49 . 1.377(4) ?
  C45 C46 . 1.390(4) ?
  C46 C47 . 1.378(4) ?
  C47 C48 . 1.391(4) ?
  C47 C50 . 1.516(4) ?
  C48 C49 . 1.382(4) ?
  C51 C52 . 1.381(3) ?
  C52 C53 . 1.391(4) ?
  C53 C54 . 1.365(4) ?
  C54 C55 . 1.377(4) ?