#------------------------------------------------------------------------------ #$Date: 2011-09-28 15:24:46 +0100 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: svn://www.crystallography.net/cod/hkl/2/01/01/2010175.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010175_Fobs loop_ _publ_author_name 'Blake, A. J.' 'McNab, H.' 'Morrow, M.' _publ_section_title ; 2,2-Dimethyl-5-(phenylthiomethylene)-1,3-dioxane-4,6-dione ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1716 _journal_page_last 1717 _journal_volume 50 _journal_year 1994 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _exptl_crystal_F_000 552.00 _[local]_cod_data_source_file ha1114sup2.hkl _[local]_cod_data_source_block melsph #BEGIN Tags that were not found in dictionaries: _shelx_title ' MELSPH #804 C13 H12 O4 S, 298K' _shelx_refln_list_code 4 _shelx_f_calc_maximum 174.49 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12301.39 13101.12 53.34 o 3 0 0 862.27 895.54 13.35 o 4 0 0 195.33 244.33 11.39 o 5 0 0 1502.03 1743.00 21.95 o 6 0 0 2538.78 2703.72 28.70 o 7 0 0 65.00 55.94 6.15 o 8 0 0 2030.59 2226.52 30.51 o 9 0 0 3288.56 3940.93 43.47 o 10 0 0 390.51 499.00 20.87 o 11 0 0 1150.72 1384.73 31.36 o 12 0 0 13.64 4.25 18.01 o 13 0 0 39.39 53.09 9.94 o 14 0 0 472.75 605.19 28.92 o 15 0 0 29.79 9.94 22.75 o 1 1 0 1445.74 1588.97 14.42 o 2 1 0 4301.21 4827.43 28.86 o 3 1 0 310.16 315.27 11.40 o 4 1 0 1884.10 2207.55 22.96 o 5 1 0 0.63 10.43 9.94 o 6 1 0 436.39 522.11 15.65 o 7 1 0 523.63 575.78 17.09 o 8 1 0 27.47 35.08 6.64 o 9 1 0 987.81 1170.04 25.66 o 10 1 0 40.55 31.29 8.05 o 11 1 0 354.84 447.24 15.64 o 12 1 0 202.11 261.23 14.23 o 13 1 0 168.92 204.31 10.89 o 14 1 0 68.41 101.91 10.89 o 15 1 0 18.45 26.54 9.94 o 0 2 0 15121.00 18409.63 80.78 x 1 2 0 1436.89 1686.45 20.06 o 2 2 0 2684.56 3038.19 26.89 o 3 2 0 325.95 383.48 13.29 o 4 2 0 348.91 432.33 13.75 o 5 2 0 405.05 512.55 15.19 o 6 2 0 36.59 6.64 11.84 o 7 2 0 332.31 353.87 15.64 o 8 2 0 6.81 9.94 6.15 o 9 2 0 765.51 867.35 23.74 o 10 2 0 62.34 92.89 8.53 o 11 2 0 727.09 834.33 28.48 o 12 2 0 124.04 152.64 9.48 o 13 2 0 0.47 -25.11 19.91 o 14 2 0 162.25 203.36 12.79 o 1 3 0 1516.53 1873.54 24.29 o 2 3 0 0.21 0.00 10.43 o 3 3 0 47.23 39.82 5.69 o 4 3 0 88.85 99.54 6.15 o 5 3 0 0.97 0.95 5.69 o 6 3 0 9.95 -8.53 12.78 o 7 3 0 304.06 391.76 18.03 o 8 3 0 10.40 13.27 14.22 o 9 3 0 63.26 83.90 8.53 o 10 3 0 67.60 89.58 8.53 o 11 3 0 17.90 -18.96 18.96 o 12 3 0 13.03 32.23 18.96 o 13 3 0 16.25 17.52 20.37 o 14 3 0 16.18 35.54 19.91 o 0 4 0 6073.19 7617.47 57.32 o 1 4 0 805.13 987.92 21.36 o 2 4 0 285.60 379.90 16.59 o 3 4 0 144.19 175.88 8.54 o 4 4 0 169.56 188.70 10.43 o 5 4 0 47.07 56.89 7.10 o 6 4 0 182.15 220.00 10.89 o 7 4 0 179.55 190.59 9.00 o 8 4 0 66.63 72.06 8.99 o 9 4 0 950.43 1148.94 31.80 o 10 4 0 86.27 99.53 9.94 o 11 4 0 215.43 283.99 14.23 o 12 4 0 220.28 276.86 12.33 o 13 4 0 1.40 -8.04 22.26 o 1 5 0 115.30 113.30 8.05 o 2 5 0 74.64 83.90 8.05 o 3 5 0 6.27 4.74 7.58 o 4 5 0 94.34 105.22 8.53 o 5 5 0 0.82 8.04 15.17 o 6 5 0 102.90 118.50 9.48 o 7 5 0 266.89 279.75 15.18 o 8 5 0 146.51 173.02 9.94 o 9 5 0 109.09 134.61 10.43 o 10 5 0 85.23 108.06 9.94 o 11 5 0 3.43 -43.12 22.75 o 0 6 0 16.99 27.95 8.99 o 1 6 0 182.51 244.15 12.33 o 2 6 0 2.30 16.58 15.63 o 3 6 0 8.41 17.06 17.06 o 4 6 0 24.84 19.91 8.53 o 5 6 0 12.58 27.95 8.04 o 6 6 0 65.62 69.67 10.43 o 7 6 0 14.93 25.60 19.91 o 8 6 0 5.43 18.47 18.47 o 9 6 0 57.39 72.52 10.89 o 1 7 0 130.20 169.70 11.84 o 2 7 0 296.03 331.42 16.12 o 3 7 0 5.79 13.27 10.43 o 4 7 0 2.59 36.02 18.01 o 5 7 0 29.94 34.59 21.81 o 6 7 0 123.47 150.27 11.38 o -15 1 1 79.97 96.22 10.89 o -14 1 1 48.55 55.45 9.48 o -13 1 1 0.35 4.25 17.52 o -12 1 1 158.13 140.81 9.48 o -11 1 1 11.35 20.86 15.17 o -10 1 1 94.42 120.88 8.53 o -9 1 1 426.53 464.47 20.39 o -8 1 1 154.16 152.21 7.59 o -7 1 1 345.90 282.76 12.34 o -6 1 1 0.57 -214.68 16.58 < -5 1 1 61.81 71.12 5.20 o -4 1 1 368.86 361.82 12.35 o -3 1 1 275.07 239.74 10.45 o -2 1 1 2210.35 1997.30 17.82 o -1 1 1 74.21 63.07 3.31 o 0 1 1 5972.81 5858.76 30.45 o 1 1 1 438.69 444.67 10.46 o 2 1 1 702.57 626.50 12.84 o 3 1 1 6595.92 6550.12 39.69 o 4 1 1 79.88 91.01 5.69 o 5 1 1 590.56 597.98 15.66 o 6 1 1 203.61 183.06 9.00 o 7 1 1 48.85 63.04 6.15 o 8 1 1 560.96 547.69 21.35 o 9 1 1 55.65 66.83 8.05 o 10 1 1 21.29 14.68 16.12 o 11 1 1 0.03 18.96 17.06 o 12 1 1 10.95 3.30 18.96 o 13 1 1 1.42 -19.91 21.32 o 14 1 1 62.28 71.57 11.38 o -15 2 1 54.67 81.05 10.89 o -14 2 1 191.80 202.91 12.33 o -13 2 1 229.37 209.56 11.84 o -12 2 1 15.64 10.89 17.53 o -11 2 1 9.15 -4.74 18.01 o -10 2 1 0.15 -60.18 18.96 < -9 2 1 238.60 217.19 10.89 o -8 2 1 216.35 168.32 7.59 o -7 2 1 1013.66 974.33 22.33 o -6 2 1 102.34 85.32 6.15 o -5 2 1 0.02 -13.27 10.43 o -4 2 1 926.48 850.95 17.13 o -3 2 1 260.86 238.17 11.85 o -2 2 1 805.54 768.39 15.23 o -1 2 1 88.50 87.23 5.20 o 0 2 1 310.99 257.76 12.34 o 1 2 1 137.80 115.71 5.69 o 2 2 1 54.92 46.46 5.20 o 3 2 1 28.34 32.24 5.20 o 4 2 1 122.58 137.49 7.10 o 5 2 1 93.13 97.65 6.15 o 6 2 1 496.36 466.05 17.55 o 7 2 1 70.46 100.97 7.10 o 8 2 1 50.18 51.66 7.10 o 9 2 1 226.65 201.05 9.48 o 10 2 1 108.68 111.86 8.99 o 11 2 1 12.25 18.96 16.58 o 12 2 1 0.48 2.84 19.91 o 13 2 1 14.62 47.86 9.94 o 14 2 1 2.17 18.47 21.80 o -14 3 1 11.21 17.52 21.80 o -13 3 1 21.40 6.15 11.84 o -12 3 1 65.54 17.07 24.65 o -11 3 1 4.28 -210.43 28.90 < -10 3 1 15.06 -98.11 21.32 < -9 3 1 5.28 -84.35 19.42 < -8 3 1 152.22 137.48 8.05 o -7 3 1 30.79 55.94 7.10 o -6 3 1 138.97 100.50 6.64 o -5 3 1 349.60 294.61 10.44 o -4 3 1 659.12 682.89 17.56 o -3 3 1 2192.17 2301.68 27.20 o -2 3 1 588.96 580.79 16.15 o -1 3 1 519.18 515.63 16.15 o 0 3 1 1292.52 1353.53 21.41 o 1 3 1 1272.83 1327.13 21.41 o 2 3 1 165.02 168.32 7.59 o 3 3 1 1381.64 1369.80 23.31 o 4 3 1 390.08 362.49 15.65 o 5 3 1 907.96 989.58 22.32 o 6 3 1 0.34 4.74 11.84 o 7 3 1 161.77 147.46 8.05 o 8 3 1 256.45 287.84 12.79 o 9 3 1 295.18 305.87 14.23 o 10 3 1 633.20 580.30 26.58 o 11 3 1 237.64 205.29 10.89 o 12 3 1 231.27 246.52 11.84 o 13 3 1 17.02 0.95 21.32 o -13 4 1 48.75 21.81 25.11 o -12 4 1 192.17 188.20 11.84 o -11 4 1 101.97 1.90 27.01 o -10 4 1 277.87 240.86 11.38 o -9 4 1 525.44 496.68 23.72 o -8 4 1 953.53 894.58 28.96 o -7 4 1 366.51 350.49 14.23 o -6 4 1 675.98 638.39 21.84 o -5 4 1 105.20 141.75 7.59 o -4 4 1 879.64 848.29 22.31 o -3 4 1 67.88 65.88 6.64 o -2 4 1 1386.70 1348.99 25.20 o -1 4 1 592.74 615.18 18.99 o 0 4 1 1071.59 1131.67 22.82 o 1 4 1 99.64 91.95 7.10 o 2 4 1 1571.53 1583.66 27.60 o 3 4 1 126.63 116.15 7.10 o 4 4 1 1250.56 1299.10 26.13 o 5 4 1 1.64 9.94 13.27 o 6 4 1 147.73 140.81 8.05 o 7 4 1 229.20 261.26 10.89 o 8 4 1 66.01 81.05 8.53 o 9 4 1 3.47 -19.42 18.96 o 10 4 1 223.27 219.99 11.84 o 11 4 1 0.09 -25.11 21.80 o 12 4 1 135.92 129.42 11.84 o -12 5 1 127.13 72.06 14.68 o -11 5 1 90.33 72.52 11.38 o -10 5 1 29.59 35.54 9.94 o -9 5 1 781.48 700.92 31.33 o -8 5 1 77.41 59.73 9.48 o -7 5 1 32.66 22.27 17.07 o -6 5 1 80.59 70.62 9.48 o -5 5 1 57.26 67.78 7.58 o -4 5 1 2.90 27.00 14.22 o -3 5 1 586.88 592.68 21.83 o -2 5 1 0.02 22.75 14.22 o -1 5 1 1071.99 1051.27 25.66 o 0 5 1 27.51 46.46 7.10 o 1 5 1 613.30 594.63 22.29 o 2 5 1 18.12 -1.41 15.63 o 3 5 1 77.14 72.52 8.53 o 4 5 1 0.03 11.84 13.73 o 5 5 1 508.08 574.01 23.24 o 6 5 1 77.99 79.62 8.99 o 7 5 1 42.66 53.55 9.48 o 8 5 1 114.04 119.93 9.94 o 9 5 1 2.61 28.44 17.52 o 10 5 1 8.36 3.30 20.86 o 11 5 1 210.90 211.45 12.33 o -9 6 1 205.92 173.03 12.79 o -8 6 1 409.39 392.68 19.43 o -7 6 1 195.24 182.51 10.89 o -6 6 1 330.37 305.38 14.69 o -5 6 1 1.65 -50.24 20.37 < -4 6 1 40.53 19.91 18.01 o -3 6 1 11.16 -72.05 21.80 < -2 6 1 120.30 124.68 8.99 o -1 6 1 5.81 -99.51 23.21 < 0 6 1 527.26 463.95 17.08 o 1 6 1 16.42 5.69 16.58 o 2 6 1 475.22 433.07 17.08 o 3 6 1 20.41 4.25 18.01 o 4 6 1 147.43 140.80 9.94 o 5 6 1 50.19 19.42 20.37 o 6 6 1 18.25 31.75 19.42 o 7 6 1 26.28 28.44 9.94 o 8 6 1 61.92 46.92 10.89 o 9 6 1 0.04 -13.73 21.32 o -6 7 1 105.29 76.31 12.33 o -5 7 1 22.29 21.32 21.32 o -4 7 1 0.16 -77.25 23.21 < -3 7 1 32.53 -22.75 22.75 o -2 7 1 1.56 -83.89 25.11 < -1 7 1 74.55 66.37 10.89 o 0 7 1 82.86 72.52 9.94 o 1 7 1 241.14 230.43 12.33 o 2 7 1 0.63 19.42 19.42 o 3 7 1 144.32 144.10 11.38 o 4 7 1 0.29 -2.36 19.42 o 5 7 1 36.42 38.87 10.89 o -16 0 2 11.68 22.26 20.37 o -15 0 2 107.28 180.59 12.33 o -14 0 2 284.34 302.05 15.64 o -13 0 2 133.78 117.55 9.94 o -12 0 2 246.30 380.28 16.12 o -11 0 2 16.95 92.88 10.43 o -10 0 2 374.27 281.29 12.80 o -9 0 2 3.00 -4.25 13.27 o -8 0 2 832.89 712.60 19.47 o -7 0 2 1782.00 1663.34 23.35 o -6 0 2 289.12 176.96 9.00 o -5 0 2 1639.99 1464.45 20.06 o -4 0 2 11958.56 11290.05 56.01 o -3 0 2 83.25 60.71 4.74 o -2 0 2 4546.25 4400.28 26.06 o -1 0 2 28.20 26.55 3.31 o 0 0 2 2111.43 2059.23 16.88 o 1 0 2 10297.52 10073.67 47.81 o 2 0 2 14807.96 13613.73 63.19 o 3 0 2 11317.78 10673.43 55.92 o 4 0 2 1911.28 1708.32 21.97 o 5 0 2 378.01 331.23 14.70 o 6 0 2 438.06 327.44 13.29 o 7 0 2 13.00 22.27 6.15 o 8 0 2 47.19 -0.95 18.01 o 9 0 2 907.89 835.29 25.16 o 10 0 2 1054.98 973.62 30.40 o 11 0 2 42.96 20.37 18.96 o 12 0 2 522.53 472.92 20.88 o 13 0 2 380.22 358.98 18.97 o 14 0 2 0.87 -21.80 20.86 o -15 1 2 5.50 -18.47 21.80 o -14 1 2 53.69 15.17 21.81 o -13 1 2 270.15 235.65 11.38 o -12 1 2 0.23 -261.13 28.44 < -11 1 2 290.83 219.56 10.43 o -10 1 2 526.99 513.41 20.39 o -9 1 2 253.92 242.79 11.38 o -8 1 2 6728.44 6485.21 51.20 o -7 1 2 2638.59 2500.91 29.64 o -6 1 2 1324.20 1310.06 20.47 o -5 1 2 2110.92 1962.80 22.96 o -4 1 2 2066.16 2128.13 22.03 o -3 1 2 0.95 6.15 9.48 o -2 1 2 682.45 580.34 12.38 o -1 1 2 2392.21 2230.82 19.28 o 0 1 2 3213.78 3138.40 23.25 o 1 1 2 30447.86 31702.41 123.14 o 2 1 2 244.51 204.51 8.54 o 3 1 2 19985.08 19734.76 89.45 o 4 1 2 269.66 260.91 12.80 o 5 1 2 757.55 705.54 17.57 o 6 1 2 5.95 6.64 13.27 o 7 1 2 96.66 82.96 7.10 o 8 1 2 0.11 -13.27 13.73 o 9 1 2 109.10 82.47 8.05 o 10 1 2 665.50 667.68 24.19 o 11 1 2 0.16 -71.10 19.91 < 12 1 2 102.40 89.59 9.94 o 13 1 2 25.85 23.21 19.42 o 14 1 2 103.23 91.00 12.33 o -15 2 2 467.02 493.70 21.82 o -14 2 2 83.70 63.99 11.84 o -13 2 2 1.65 -17.06 18.96 o -12 2 2 261.16 248.93 12.33 o -11 2 2 116.48 117.09 8.99 o -10 2 2 229.21 235.66 10.89 o -9 2 2 272.39 231.90 11.84 o -8 2 2 737.44 817.17 22.31 o -7 2 2 61.02 66.83 6.15 o -6 2 2 763.36 797.17 18.52 o -5 2 2 88.67 111.87 5.69 o -4 2 2 1143.07 1138.68 18.55 o -3 2 2 161.56 186.37 8.05 o -2 2 2 160.26 134.69 7.10 o -1 2 2 920.34 881.97 15.70 o 0 2 2 688.39 739.29 14.73 o 1 2 2 559.11 584.34 14.25 o 2 2 2 167.94 127.58 6.15 o 3 2 2 613.42 640.73 16.15 o 4 2 2 18.61 1.90 11.38 o 5 2 2 136.29 140.82 7.10 o 6 2 2 0.66 0.00 12.78 o 7 2 2 1.36 -4.25 13.27 o 8 2 2 13.72 9.94 14.22 o 9 2 2 3.73 5.20 16.12 o 10 2 2 146.55 148.39 9.48 o 11 2 2 47.38 44.56 8.99 o 12 2 2 110.93 92.43 10.43 o 13 2 2 83.73 45.51 24.16 o -14 3 2 10.55 28.44 10.43 o -13 3 2 17.01 -4.74 20.37 o -12 3 2 6.19 -21.32 18.47 o -11 3 2 126.52 133.67 9.94 o -10 3 2 163.19 142.22 9.00 o -9 3 2 89.23 81.52 8.05 o -8 3 2 1509.83 1432.43 27.59 o -7 3 2 23.08 -17.07 13.73 o -6 3 2 535.09 533.92 18.04 o -5 3 2 60.43 47.41 6.15 o -4 3 2 239.11 269.86 9.95 o -3 3 2 1.82 -0.46 10.89 o -2 3 2 12.80 17.53 5.20 o -1 3 2 1657.12 1539.34 22.88 o 0 3 2 294.60 323.54 13.75 o 1 3 2 2680.85 2651.27 29.64 o 2 3 2 1100.68 1105.62 21.88 o 3 3 2 2401.35 2351.83 29.59 o 4 3 2 542.21 531.10 18.50 o 5 3 2 24.35 21.81 6.15 o 6 3 2 1.70 12.78 6.64 o 7 3 2 3.16 9.48 14.68 o 8 3 2 42.72 49.30 8.05 o 9 3 2 114.40 124.68 9.48 o 10 3 2 624.54 619.17 25.14 o 11 3 2 4.69 15.17 19.91 o 12 3 2 229.69 217.61 12.33 o 13 3 2 1.18 -2.36 21.32 o -13 4 2 65.09 88.15 10.43 o -12 4 2 0.30 -16.58 20.86 o -11 4 2 91.67 89.59 8.99 o -10 4 2 8.01 9.48 17.06 o -9 4 2 283.00 290.19 13.28 o -8 4 2 152.89 142.71 8.53 o -7 4 2 61.60 27.96 16.12 o -6 4 2 0.26 7.10 13.27 o -5 4 2 78.65 77.75 7.10 o -4 4 2 587.47 527.78 19.45 o -3 4 2 123.74 136.07 7.10 o -2 4 2 181.04 159.77 8.54 o -1 4 2 1.99 8.04 12.32 o 0 4 2 363.55 365.74 16.59 o 1 4 2 1335.55 1384.80 25.20 o 2 4 2 14.26 3.79 12.32 o 3 4 2 46.60 52.61 7.10 o 4 4 2 2.28 -3.30 13.27 o 5 4 2 261.35 257.95 12.79 o 6 4 2 5.37 27.95 14.22 o 7 4 2 10.74 17.06 8.53 o 8 4 2 66.65 57.35 8.99 o 9 4 2 107.70 110.91 9.94 o 10 4 2 473.97 459.12 18.49 o 11 4 2 8.38 12.32 20.86 o 12 4 2 101.85 105.71 12.33 o -12 5 2 9.34 -36.49 23.21 o -11 5 2 19.98 28.90 10.43 o -10 5 2 1.39 13.73 18.47 o -9 5 2 78.37 40.28 19.91 o -8 5 2 306.27 287.84 15.64 o -7 5 2 34.02 21.81 17.07 o -6 5 2 106.24 98.59 8.53 o -5 5 2 89.87 95.28 8.99 o -4 5 2 21.67 18.01 8.04 o -3 5 2 147.99 150.75 8.53 o -2 5 2 12.80 12.78 15.17 o -1 5 2 100.72 97.18 8.05 o 0 5 2 98.10 98.13 8.05 o 1 5 2 309.43 311.58 13.28 o 2 5 2 79.01 78.21 8.53 o 3 5 2 86.17 87.69 8.05 o 4 5 2 171.83 141.76 9.00 o 5 5 2 31.89 28.90 16.58 o 6 5 2 20.53 9.94 17.53 o 7 5 2 27.58 28.90 8.99 o 8 5 2 1.90 12.32 18.01 o 9 5 2 3.21 -4.25 19.42 o 10 5 2 5.17 -3.30 20.86 o -10 6 2 29.57 18.01 21.32 o -9 6 2 5.16 -7.58 18.96 o -8 6 2 120.66 85.80 10.89 o -7 6 2 313.80 297.78 15.64 o -6 6 2 271.40 270.25 13.74 o -5 6 2 292.34 289.24 13.28 o -4 6 2 3.66 2.84 17.52 o -3 6 2 137.90 146.49 9.48 o -2 6 2 6.58 -0.95 16.58 o -1 6 2 154.17 147.90 9.00 o 0 6 2 17.77 21.80 8.53 o 1 6 2 84.56 88.15 9.48 o 2 6 2 222.44 221.41 10.43 o 3 6 2 193.92 167.34 9.94 o 4 6 2 99.12 93.84 9.94 o 5 6 2 17.92 14.22 9.48 o 6 6 2 15.21 -11.84 19.91 o 7 6 2 7.05 8.53 19.91 o 8 6 2 0.50 26.54 19.91 o -6 7 2 15.04 -26.54 22.27 o -5 7 2 3.28 -33.18 20.37 o -4 7 2 44.38 34.59 19.91 o -3 7 2 59.63 73.46 10.43 o -2 7 2 0.05 -4.25 19.42 o -1 7 2 35.14 54.99 9.94 o 0 7 2 264.01 252.71 13.28 o 1 7 2 83.66 109.96 10.43 o 2 7 2 16.32 20.86 18.96 o 3 7 2 2.60 0.95 20.37 o 4 7 2 45.44 51.66 10.89 o -16 1 3 14.18 25.60 21.32 o -15 1 3 10.11 8.04 21.32 o -14 1 3 50.06 35.54 19.42 o -13 1 3 227.16 199.60 10.89 o -12 1 3 101.62 97.18 8.99 o -11 1 3 24.60 16.58 7.58 o -10 1 3 11.06 -4.25 14.22 o -9 1 3 0.45 8.04 12.32 o -8 1 3 227.11 230.95 10.43 o -7 1 3 1301.12 1323.86 22.36 o -6 1 3 102.54 121.36 7.10 o -5 1 3 305.38 324.07 13.29 o -4 1 3 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