data_2010255
_journal_name_full  'Acta Crystallographica'
_journal_year  1994
_journal_volume  C50
_journal_page_first  1974
_journal_page_last  1976
_publ_section_title
;
Aminoguanidinium Nitrate
;
loop_
_publ_author_name
  'Akella, Annapoorna'
  'Keszler, Douglas A.'
_chemical_formula_moiety  'C H7 N4 1+, N O3 1-'
_chemical_formula_sum  'C H7 N5 O3'
_chemical_formula_weight  137.10
_symmetry_cell_setting  triclinic
_symmetry_space_group_name_H-M  'P -1'
loop_
_symmetry_equiv_pos_as_xyz
  'x,y,z'
  '-x,-y,-z'
_cell_length_a  7.3410(10)
_cell_length_b  7.722(2)
_cell_length_c  6.0240(10)
_cell_angle_alpha  110.47(2)
_cell_angle_beta  102.64(2)
_cell_angle_gamma  104.87(2)
_cell_volume  290.70(10)
_cell_formula_units_Z  2
_cell_measurement_temperature  296
_exptl_crystal_density_diffrn  1.566
_refine_ls_R_factor_obs  0.044
_refine_ls_wR_factor_obs  0.054
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
  O1 0.8178(2) 0.4752(2) 0.2681(2)
  O2 0.6710(2) 0.4385(2) -0.1057(2)
  O3 0.5573(2) 0.2153(2) 0.0154(3)
  N1 0.0380(2) -0.1698(2) -0.8063(3)
  N2 0.2316(2) -0.1301(2) -0.4248(3)
  N3 0.2980(2) 0.1237(2) -0.5409(3)
  N4 0.2462(2) 0.2045(2) -0.7091(3)
  N5 0.6820(2) 0.3772(2) 0.0583(2)
  C1 0.1875(2) -0.0603(2) -0.5925(3)
  H1 -0.036(3) -0.286(3) -0.834(4)
  H2 0.007(3) -0.128(3) -0.901(4)
  H3 0.396(3) 0.192(3) -0.406(5)
  H4 0.338(3) -0.062(3) -0.286(5)
  H5 0.172(3) -0.254(3) -0.474(4)
  H6 0.352(3) 0.240(3) -0.768(5)
  H7 0.230(3) 0.328(3) -0.617(5)
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
  O1 0.0636(7) 0.0435(6) 0.0429(7) -0.0017(5) -0.0034(5) 0.0099(5)
  O2 0.0621(7) 0.0493(6) 0.0503(7) 0.0103(5) 0.0139(5) 0.0271(6)
  O3 0.0572(6) 0.0416(6) 0.0574(7) -0.0061(4) 0.0065(5) 0.0200(5)
  N1 0.0454(6) 0.0340(6) 0.0512(7) 0.0017(5) 0.0026(6) 0.0175(6)
  N2 0.0688(9) 0.0509(8) 0.0531(8) 0.0220(7) 0.0112(7) 0.0257(7)
  N3 0.0427(6) 0.0423(6) 0.0399(7) 0.0010(5) 0.0018(5) 0.0134(6)
  N4 0.0517(7) 0.0419(6) 0.0456(7) 0.0014(5) 0.0112(6) 0.0192(6)
  N5 0.0438(6) 0.0319(5) 0.0400(6) 0.0065(4) 0.0093(5) 0.0110(5)
  C1 0.0388(6) 0.0391(6) 0.0425(7) 0.0145(5) 0.0144(6) 0.0150(6)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
  O1 N5 . 1.248(2) yes
  O2 N5 . 1.232(2) yes
  O3 N5 . 1.246(2) yes
  N1 C1 . 1.312(2) yes
  N1 H1 . 0.86(2) yes
  N1 H2 . 0.77(2) yes
  N2 C1 . 1.320(3) yes
  N2 H4 . 0.88(2) yes
  N2 H5 . 0.85(2) yes
  N3 N4 . 1.399(3) yes
  N3 C1 . 1.328(2) yes
  N3 H3 . 0.84(2) yes
  N4 H6 . 0.94(2) yes
  N4 H7 . 0.97(2) yes
  O1 N1 1_666 3.038(2) yes
  O1 N2 2_655 3.088(2) yes
  O1 N4 2_665 3.153(2) yes
  O2 N1 1_666 3.087(2) yes
  O2 N3 . 3.043(2) yes
  O3 N2 2_655 2.983(2) yes
  O3 N2 . 2.977(2) yes
  O3 N4 1_556 3.104(2) yes