#------------------------------------------------------------------------------
#$Date: 2010-01-30 13:59:17 +0000 (Sat, 30 Jan 2010) $
#$Revision: 966 $
#$URL: svn://www.crystallography.net/cod/cif/2/2010373.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2010373
_journal_name_full 'Acta Crystallographica Section C'
_journal_year  1995
_journal_volume 51
_journal_page_first  20
_journal_page_last  23
_publ_section_title
;
cis-trans-[{N~3~P~3~Cl~4~(C~6~H~5~)(PPh~2~)}Mn(CO)~2~(bipy)
 {P(OPh)~3~}]PF~6~. A Cationic Manganese--Carbonyl Complex with a
Phosphazenylphosphine Ligand
;
loop_
_publ_author_name
  'Gabino A. Carriedo'
  'Luc\'ia Fern\'andez'
  'Paloma G\'omez'
  'Santiago Garc\'ia-Granda'
  'Amador Men\'endez Vel\'azquez'
_chemical_formula_sum  'C48 H38 Cl4 F6 Mn N5 O5 P6'
_chemical_formula_weight  1261.39
_symmetry_cell_setting  Triclinic
_symmetry_space_group_name_H-M  'P 1'
loop_
_symmetry_equiv_pos_as_xyz
  'x, y, z'
_cell_length_a  10.563(2)
_cell_length_b  10.603(3)
_cell_length_c  12.250(3)
_cell_angle_alpha  97.68(4)
_cell_angle_beta  99.34(3)
_cell_angle_gamma  93.11(2)
_cell_volume  1337.6(5)
_cell_formula_units_Z  1
_cell_measurement_temperature  293
_exptl_crystal_density_diffrn  1.566
_diffrn_ambient_temperature  293
_refine_ls_R_factor_obs  0.0442
_refine_ls_wR_factor_obs  0.1082
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_thermal_displace_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_group
_atom_site_type_symbol
  Mn1 0.0000 0.0000 0.0000 0.0295(2) Uani d . 1 . Mn
  Cl1 -0.4009(2) -0.4136(2) -0.2245(2) 0.0591(5) Uani d . 1 . Cl
  Cl2 -0.2239(2) -0.5486(2) -0.3713(2) 0.0771(7) Uani d . 1 . Cl
  Cl3 -0.3004(3) -0.2937(2) -0.6486(2) 0.0756(7) Uani d . 1 . Cl
  Cl4 -0.4416(2) -0.0979(2) -0.5158(2) 0.0705(6) Uani d . 1 . Cl
  P1 0.0908(2) 0.0135(2) 0.1773(2) 0.0373(4) Uani d . 1 . P
  P2 -0.0858(2) 0.0050(2) -0.1897(2) 0.0290(4) Uani d . 1 . P
  P3 -0.1010(2) -0.1726(2) -0.3148(2) 0.0299(4) Uani d . 1 . P
  P4 -0.2821(2) -0.3748(2) -0.3271(2) 0.0393(4) Uani d . 1 . P
  P5 -0.3084(2) -0.2227(2) -0.4901(2) 0.0398(4) Uani d . 1 . P
  P6 -0.5638(2) -0.5400(2) -0.9677(2) 0.0669(6) Uani d . 1 . P
  F1 -0.4183(7) -0.5677(8) -0.9821(8) 0.155(3) Uani d . 1 . F
  F2 -0.6994(6) -0.5224(8) -0.946(2) 0.203(5) Uani d . 1 . F
  F3 -0.5973(8) -0.6842(7) -0.9890(10)
  0.169(4) Uani d . 1 . F
  F4 -0.5930(9) -0.552(2) -1.0960(8) 0.190(4) Uani d . 1 . F
  F5 -0.5210(10)
  -0.4030(8) -0.9504(13) 0.235(6) Uani d . 1 . F
  F6 -0.5200(10)
  -0.542(2) -0.8444(8) 0.233(6) Uani d . 1 . F
  O1 0.2605(5) -0.0284(5) -0.0491(5) 0.069(2) Uani d . 1 . O
  O2 0.0296(5) 0.2814(5) 0.0241(5) 0.060(2) Uani d . 1 . O
  O3 0.2038(5) 0.1263(5) 0.2105(4) 0.052(2) Uani d . 1 . O
  O4 0.0095(5) 0.0287(4) 0.2772(4) 0.046(2) Uani d . 1 . O
  O5 0.1699(5) -0.1026(5) 0.2091(4) 0.056(2) Uani d . 1 . O
  N1 -0.1835(5) -0.0043(5) 0.0354(4) 0.029(2) Uani d . 1 . N
  N2 -0.0391(5) -0.1909(4) 0.0028(4) 0.035(2) Uani d . 1 . N
  N3 -0.1656(5) -0.2856(5) -0.2601(5) 0.036(2) Uani d . 1 . N
  N4 -0.3641(6) -0.3313(6) -0.4320(5) 0.050(2) Uani d . 1 . N
  N5 -0.1757(5) -0.1483(5) -0.4326(5) 0.040(2) Uani d . 1 . N
  C1 0.1590(7) -0.0146(6) -0.0316(6) 0.037(2) Uani d . 1 . C
  C2 0.0189(6) 0.1727(7) 0.0131(5) 0.035(2) Uani d . 1 . C
  C12 -0.2360(6) -0.1209(7) 0.0464(6) 0.044(2) Uani d . 1 . C
  C13 -0.3598(7) -0.1367(8) 0.0713(7) 0.054(2) Uani d . 1 . C
  H13 -0.387(8) -0.241(9) 0.093(7) 0.09(3) Uiso d . 1 . H
  C14 -0.4305(7) -0.0337(9) 0.0807(7) 0.061(2) Uani d . 1 . C
  H14 -0.5144(7) -0.0440(9) 0.0939(7) 0.065(4) Uiso calc R 1 . H
  C15 -0.3798(7) 0.0855(8) 0.0708(6) 0.049(2) Uani d . 1 . C
  H15 -0.4272(7) 0.1566(8) 0.0784(6) 0.065(4) Uiso calc R 1 . H
  C16 -0.2548(6) 0.0955(7) 0.0490(5) 0.039(2) Uani d . 1 . C
  H16 -0.2187(6) 0.1759(7) 0.0436(5) 0.065(4) Uiso calc R 1 . H
  C22 -0.1533(7) -0.2281(6) 0.0289(6) 0.042(2) Uani d . 1 . C
  C23 -0.1885(8) -0.3503(7) 0.0377(8) 0.059(2) Uani d . 1 . C
  H23 -0.260(8) -0.379(7) 0.064(6) 0.05(2) Uiso d . 1 . H
  C24 -0.1024(9) -0.4425(8) 0.0228(8) 0.070(2) Uani d . 1 . C
  H24 -0.1241(9) -0.5267(8) 0.0305(8) 0.065(4) Uiso calc R 1 . H
  C25 0.0136(9) -0.4092(7) -0.0029(7) 0.061(2) Uani d . 1 . C
  H25 0.0717(9) -0.4704(7) -0.0148(7) 0.065(4) Uiso calc R 1 . H
  C26 0.0442(7) -0.2827(7) -0.0111(6) 0.049(2) Uani d . 1 . C
  H26 0.1248(7) -0.2596(7) -0.0268(6) 0.065(4) Uiso calc R 1 . H
  C31 0.2781(6) 0.1700(7) 0.3148(6) 0.047(2) Uani d . 1 . C
  C32 0.3497(7) 0.2833(7) 0.3180(7) 0.053(2) Uani d . 1 . C
  H32 0.3463(7) 0.3236(7) 0.2547(7) 0.065(4) Uiso calc R 1 . H
  C33 0.4257(8) 0.3347(8) 0.4163(8) 0.068(2) Uani d . 1 . C
  H33 0.4727(8) 0.4123(8) 0.4198(8) 0.065(4) Uiso calc R 1 . H
  C34 0.4355(8) 0.2757(9) 0.5110(8) 0.067(2) Uani d . 1 . C
  H34 0.4891(8) 0.3108(9) 0.5772(8) 0.065(4) Uiso calc R 1 . H
  C35 0.3622(9) 0.1629(9) 0.5024(7) 0.066(2) Uani d . 1 . C
  H35 0.3665(9) 0.1209(9) 0.5647(7) 0.065(4) Uiso calc R 1 . H
  C36 0.2841(8) 0.1107(8) 0.4073(6) 0.063(2) Uani d . 1 . C
  H36 0.2348(8) 0.0346(8) 0.4047(6) 0.065(4) Uiso calc R 1 . H
  C41 -0.0797(7) 0.1206(7) 0.2916(6) 0.046(2) Uani d . 1 . C
  C42 -0.0562(7) 0.2442(7) 0.2725(6) 0.049(2) Uani d . 1 . C
  H42 0.0197(7) 0.2707(7) 0.2501(6) 0.065(4) Uiso calc R 1 . H
  C43 -0.1499(9) 0.3265(7) 0.2878(6) 0.056(2) Uani d . 1 . C
  H43 -0.1367(9) 0.4100(7) 0.2742(6) 0.065(4) Uiso calc R 1 . H
  C44 -0.2610(10)
  0.2914(9) 0.3220(7) 0.069(2) Uani d . 1 . C
  H44 -0.3230(10)
  0.3496(9) 0.3307(7) 0.065(4) Uiso calc R 1 . H
  C45 -0.2809(8) 0.1674(9) 0.3437(7) 0.064(2) Uani d . 1 . C
  H45 -0.3558(8) 0.1429(9) 0.3687(7) 0.065(4) Uiso calc R 1 . H
  C46 -0.1910(7) 0.0804(7) 0.3287(6) 0.051(2) Uani d . 1 . C
  H46 -0.2042(7) -0.0029(7) 0.3429(6) 0.065(4) Uiso calc R 1 . H
  C51 0.1579(7) -0.2105(6) 0.2613(5) 0.043(2) Uani d . 1 . C
  C52 0.2609(9) -0.2807(8) 0.2678(8) 0.075(3) Uani d . 1 . C
  H52 0.3324(9) -0.2562(8) 0.2380(8) 0.065(4) Uiso calc R 1 . H
  C53 0.260(2) -0.3880(10)
  0.319(2) 0.103(4) Uani d . 1 . C
  H53 0.331(2) -0.4370(10)
  0.325(2) 0.065(4) Uiso calc R 1 . H
  C54 0.151(2) -0.4236(9) 0.3609(9) 0.093(3) Uani d . 1 . C
  H54 0.148(2) -0.4980(9) 0.3933(9) 0.065(4) Uiso calc R 1 . H
  C55 0.0486(9) -0.3518(8) 0.3561(8) 0.073(3) Uani d . 1 . C
  H55 -0.0225(9) -0.3747(8) 0.3871(8) 0.065(4) Uiso calc R 1 . H
  C56 0.0511(8) -0.2443(7) 0.3044(8) 0.064(2) Uani d . 1 . C
  H56 -0.0191(8) -0.1949(7) 0.2988(8) 0.065(4) Uiso calc R 1 . H
  C61 -0.2531(6) 0.0461(6) -0.2080(5) 0.032(2) Uani d . 1 . C
  C62 -0.3509(6) -0.0415(7) -0.2045(5) 0.040(2) Uani d . 1 . C
  H62 -0.3334(6) -0.1263(7) -0.2031(5) 0.065(4) Uiso calc R 1 . H
  C63 -0.4779(7) -0.0079(9) -0.2029(6) 0.057(2) Uani d . 1 . C
  H63 -0.5445(7) -0.0687(9) -0.2023(6) 0.065(4) Uiso calc R 1 . H
  C64 -0.4983(8) 0.118(2) -0.2022(7) 0.069(3) Uani d . 1 . C
  H64 -0.5807(8) 0.143(2) -0.1991(7) 0.065(4) Uiso calc R 1 . H
  C65 -0.4033(9) 0.2075(9) -0.2059(7) 0.066(2) Uani d . 1 . C
  H65 -0.4214(9) 0.2923(9) -0.2062(7) 0.065(4) Uiso calc R 1 . H
  C66 -0.2812(7) 0.1734(7) -0.2091(6) 0.045(2) Uani d . 1 . C
  H66 -0.2163(7) 0.2351(7) -0.2120(6) 0.065(4) Uiso calc R 1 . H
  C71 -0.0081(6) 0.1185(6) -0.2636(5) 0.031(2) Uani d . 1 . C
  C72 -0.0666(7) 0.1461(6) -0.3651(6) 0.042(2) Uani d . 1 . C
  H72 -0.1463(7) 0.1047(6) -0.3975(6) 0.065(4) Uiso calc R 1 . H
  C73 -0.0110(8) 0.2333(7) -0.4209(6) 0.049(2) Uani d . 1 . C
  H73 -0.0526(8) 0.2502(7) -0.4897(6) 0.065(4) Uiso calc R 1 . H
  C74 0.1086(8) 0.2957(7) -0.3725(7) 0.056(2) Uani d . 1 . C
  H74 0.1467(8) 0.3551(7) -0.4090(7) 0.065(4) Uiso calc R 1 . H
  C75 0.1695(7) 0.2703(7) -0.2728(7) 0.056(2) Uani d . 1 . C
  H75 0.2498(7) 0.3115(7) -0.2418(7) 0.065(4) Uiso calc R 1 . H
  C76 0.1127(7) 0.1825(7) -0.2157(6) 0.045(2) Uani d . 1 . C
  H76 0.1545(7) 0.1664(7) -0.1466(6) 0.065(4) Uiso calc R 1 . H
  C81 0.0608(6) -0.2053(6) -0.3295(6) 0.033(2) Uani d . 1 . C
  C82 0.1279(7) -0.1356(7) -0.3911(6) 0.045(2) Uani d . 1 . C
  H82 0.0918(7) -0.0684(7) -0.4233(6) 0.065(4) Uiso calc R 1 . H
  C83 0.2509(7) -0.1675(8) -0.4045(7) 0.059(2) Uani d . 1 . C
  H83 0.2983(7) -0.1193(8) -0.4442(7) 0.065(4) Uiso calc R 1 . H
  C84 0.3022(7) -0.2665(8) -0.3614(7) 0.060(2) Uani d . 1 . C
  H84 0.3831(7) -0.2880(8) -0.3747(7) 0.065(4) Uiso calc R 1 . H
  C85 0.2386(7) -0.3369(7) -0.2979(7) 0.055(2) Uani d . 1 . C
  H85 0.2767(7) -0.4032(7) -0.2657(7) 0.065(4) Uiso calc R 1 . H
  C86 0.1148(7) -0.3060(7) -0.2831(7) 0.053(2) Uani d . 1 . C
  H86 0.0687(7) -0.3534(7) -0.2419(7) 0.065(4) Uiso calc R 1 . H
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
  Mn1 0.0264(5) 0.0267(5) 0.0354(5) 0.0025(4) 0.0048(4) 0.0051(4)
  Cl1 0.043(2) 0.065(2) 0.074(2) -0.0095(9) 0.0190(10)
  0.0180(10)
  Cl2 0.076(2) 0.0340(10)
  0.117(2) 0.0040(10)
  0.025(2) -0.013(2)
  Cl3 0.086(2) 0.091(2) 0.042(2) -0.019(2) 0.0110(10)
  -0.013(2)
  Cl4 0.041(2) 0.092(2) 0.088(2) 0.020(2) 0.012(2) 0.039(2)
  P1 0.0360(10)
  0.0410(10)
  0.0360(10)
  0.0003(8) 0.0022(8) 0.0125(8)
  P2 0.0264(9) 0.0290(8) 0.0308(9) 0.0004(7) 0.0042(7) 0.0025(7)
  P3 0.0236(9) 0.0296(9) 0.0361(9) 0.0019(7) 0.0071(7) 0.0013(7)
  P4 0.0340(10)
  0.0316(9) 0.051(2) -0.0030(8) 0.0113(9) 0.0022(8)
  P5 0.0310(10)
  0.048(2) 0.0390(10)
  -0.0037(8) 0.0050(8) 0.0021(8)
  P6 0.065(2) 0.069(2) 0.066(2) -0.017(2) 0.024(2) 0.002(2)
  F1 0.086(5) 0.181(8) 0.196(9) -0.013(5) 0.057(5) -0.007(6)
  F2 0.060(4) 0.145(7) 0.39(2) 0.012(4) 0.080(7) -0.055(8)
  F3 0.153(7) 0.089(5) 0.28(2) -0.010(5) 0.091(7) 0.012(6)
  F4 0.175(9) 0.24(2) 0.137(7) -0.029(8) -0.015(6) 0.035(7)
  F5 0.175(9) 0.090(6) 0.43(2) -0.051(6) 0.060(10)
  0.023(8)
  F6 0.179(9) 0.40(2) 0.109(7) -0.060(10)
  0.006(6) 0.061(9)
  O1 0.034(3) 0.076(4) 0.107(5) 0.014(3) 0.023(3) 0.033(4)
  O2 0.084(4) 0.025(3) 0.074(4) -0.004(3) 0.026(3) 0.006(2)
  O3 0.049(3) 0.058(3) 0.045(3) -0.016(2) -0.006(2) 0.015(2)
  O4 0.049(3) 0.048(3) 0.044(3) 0.004(2) 0.011(2) 0.012(2)
  O5 0.045(3) 0.070(3) 0.060(3) 0.021(3) 0.010(3) 0.031(3)
  N1 0.027(3) 0.029(3) 0.033(3) 0.000(2) 0.010(2) 0.001(2)
  N2 0.036(3) 0.024(3) 0.046(3) 0.001(3) 0.002(3) 0.012(2)
  N3 0.032(3) 0.032(3) 0.045(3) 0.000(2) 0.012(3) 0.008(2)
  N4 0.044(4) 0.049(4) 0.054(4) -0.015(3) 0.007(3) 0.003(3)
  N5 0.035(3) 0.035(3) 0.049(3) -0.004(2) 0.014(3) 0.001(3)
  C1 0.036(4) 0.037(4) 0.045(4) 0.007(3) 0.017(3) 0.013(3)
  C2 0.032(4) 0.040(4) 0.034(4) 0.005(3) 0.004(3) 0.009(3)
  C12 0.030(4) 0.063(5) 0.041(4) -0.001(4) 0.004(3) 0.015(4)
  C13 0.032(4) 0.059(5) 0.072(5) -0.006(4) 0.008(4) 0.022(4)
  C14 0.030(4) 0.090(7) 0.066(5) 0.006(4) 0.019(4) 0.009(5)
  C15 0.037(4) 0.073(5) 0.040(4) 0.018(4) 0.008(3) 0.006(4)
  C16 0.035(4) 0.052(4) 0.032(4) 0.008(3) 0.007(3) 0.003(3)
  C22 0.044(4) 0.040(4) 0.044(4) 0.000(3) 0.003(3) 0.021(3)
  C23 0.048(5) 0.035(4) 0.094(7) -0.011(4) 0.010(5) 0.020(4)
  C24 0.077(6) 0.040(5) 0.094(7) -0.005(5) 0.007(5) 0.029(4)
  C25 0.067(6) 0.035(4) 0.084(6) 0.011(4) 0.010(5) 0.022(4)
  C26 0.044(4) 0.043(4) 0.059(5) 0.010(4) -0.005(4) 0.012(4)
  C31 0.027(4) 0.051(4) 0.056(5) 0.001(3) -0.003(3) 0.001(4)
  C32 0.037(4) 0.057(5) 0.059(5) -0.003(4) -0.003(4) 0.008(4)
  C33 0.056(6) 0.052(5) 0.088(7) 0.001(4) -0.003(5) 0.002(5)
  C34 0.057(5) 0.072(6) 0.061(6) 0.008(5) -0.016(4) -0.003(5)
  C35 0.082(6) 0.072(6) 0.042(5) 0.012(5) -0.010(4) 0.014(4)
  C36 0.078(6) 0.060(5) 0.042(5) -0.018(4) -0.014(4) 0.022(4)
  C41 0.061(5) 0.042(4) 0.034(4) 0.000(4) 0.008(4) 0.000(3)
  C42 0.057(5) 0.051(5) 0.038(4) -0.006(4) 0.012(4) -0.001(3)
  C43 0.083(7) 0.043(4) 0.045(4) 0.016(5) 0.016(4) 0.001(4)
  C44 0.073(6) 0.075(7) 0.063(6) 0.025(5) 0.022(5) 0.002(5)
  C45 0.050(5) 0.076(6) 0.066(5) -0.005(5) 0.019(4) -0.002(5)
  C46 0.057(5) 0.044(4) 0.051(5) -0.007(4) 0.014(4) 0.008(4)
  C51 0.054(5) 0.035(4) 0.040(4) 0.002(4) 0.002(3) 0.010(3)
  C52 0.083(6) 0.065(6) 0.092(7) 0.033(5) 0.032(5) 0.037(5)
  C53 0.098(9) 0.072(7) 0.15(2) 0.036(6) 0.018(8) 0.047(7)
  C54 0.130(10)
  0.051(6) 0.110(8) 0.012(6) 0.032(7) 0.039(5)
  C55 0.083(7) 0.052(5) 0.096(7) 0.009(5) 0.032(6) 0.031(5)
  C56 0.067(6) 0.038(4) 0.088(6) 0.008(4) 0.013(5) 0.015(4)
  C61 0.022(3) 0.044(4) 0.029(4) 0.012(3) 0.003(3) -0.004(3)
  C62 0.031(4) 0.047(4) 0.040(4) 0.013(3) 0.005(3) -0.009(3)
  C63 0.037(5) 0.087(7) 0.042(4) -0.005(4) 0.004(3) -0.008(4)
  C64 0.040(5) 0.117(8) 0.055(5) 0.027(5) 0.013(4) 0.017(5)
  C65 0.083(7) 0.068(6) 0.065(5) 0.044(5) 0.034(5) 0.034(5)
  C66 0.047(4) 0.047(4) 0.052(4) 0.027(4) 0.018(3) 0.024(3)
  C71 0.027(3) 0.029(3) 0.038(4) -0.002(3) 0.008(3) 0.004(3)
  C72 0.054(5) 0.036(4) 0.037(4) 0.004(3) 0.014(3) 0.001(3)
  C73 0.063(5) 0.044(4) 0.041(4) 0.007(4) 0.011(4) 0.011(3)
  C74 0.060(5) 0.054(5) 0.060(5) -0.002(4) 0.029(4) 0.016(4)
  C75 0.042(4) 0.059(5) 0.071(6) -0.015(4) 0.011(4) 0.025(4)
  C76 0.040(4) 0.046(4) 0.051(4) 0.004(3) 0.002(4) 0.014(4)
  C81 0.021(3) 0.036(4) 0.044(4) 0.003(3) 0.015(3) -0.003(3)
  C82 0.039(4) 0.049(4) 0.052(4) 0.013(3) 0.017(3) 0.012(4)
  C83 0.035(4) 0.062(5) 0.085(6) -0.004(4) 0.031(4) 0.002(5)
  C84 0.026(4) 0.064(5) 0.093(7) 0.005(4) 0.021(4) 0.002(5)
  C85 0.030(4) 0.061(5) 0.082(6) 0.027(4) 0.016(4) 0.022(4)
  C86 0.034(4) 0.052(5) 0.077(6) 0.005(4) 0.018(4) 0.014(4)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
  Mn1 C1 . 1.793(7) yes
  Mn1 C2 . 1.814(7) yes
  Mn1 N2 . 2.050(5) yes
  Mn1 N1 . 2.053(5) yes
  Mn1 P1 . 2.210(2) yes
  Mn1 P2 . 2.362(2) yes
  Cl1 P4 . 1.979(3) yes
  Cl2 P4 . 2.008(2) yes
  Cl3 P5 . 2.004(3) yes
  Cl4 P5 . 2.000(3) yes
  P1 O5 . 1.581(5) yes
  P1 O4 . 1.603(5) yes
  P1 O3 . 1.606(5) yes
  P2 C61 . 1.829(6) ?
  P2 C71 . 1.836(6) ?
  P2 P3 . 2.245(2) yes
  P3 N5 . 1.588(6) yes
  P3 N3 . 1.621(5) yes
  P3 C81 . 1.794(6) ?
  P4 N3 . 1.556(5) yes
  P4 N4 . 1.566(7) yes
  P5 N4 . 1.569(6) yes
  P5 N5 . 1.579(6) yes
  P6 F5 . 1.474(7) ?
  P6 F6 . 1.510(9) ?
  P6 F2 . 1.516(7) ?
  P6 F3 . 1.528(7) ?
  P6 F4 . 1.539(9) ?
  P6 F1 . 1.613(7) ?
  O1 C1 . 1.141(7) yes
  O2 C2 . 1.139(7) yes
  O3 C31 . 1.392(8) ?
  O4 C41 . 1.405(8) ?
  O5 C51 . 1.394(8) ?
  N1 C16 . 1.340(8) ?
  N1 C12 . 1.360(8) ?
  N2 C22 . 1.348(8) ?
  N2 C26 . 1.360(8) ?
  C12 C13 . 1.396(9) ?
  C12 C22 . 1.490(10)
  ?
  C13 C14 . 1.360(10)
  ?
  C14 C15 . 1.37(2) ?
  C15 C16 . 1.390(9) ?
  C22 C23 . 1.351(9) ?
  C23 C24 . 1.39(2) ?
  C24 C25 . 1.35(2) ?
  C25 C26 . 1.380(10)
  ?
  C31 C36 . 1.360(10)
  ?
  C31 C32 . 1.380(10)
  ?
  C32 C33 . 1.36(2) ?
  C33 C34 . 1.38(2) ?
  C34 C35 . 1.37(2) ?
  C35 C36 . 1.35(2) ?
  C41 C42 . 1.380(10)
  ?
  C41 C46 . 1.390(10)
  ?
  C42 C43 . 1.370(10)
  ?
  C43 C44 . 1.36(2) ?
  C44 C45 . 1.39(2) ?
  C45 C46 . 1.38(2) ?
  C51 C52 . 1.350(10)
  ?
  C51 C56 . 1.370(10)
  ?
  C52 C53 . 1.37(2) ?
  C53 C54 . 1.39(2) ?
  C54 C55 . 1.35(2) ?
  C55 C56 . 1.38(2) ?
  C61 C62 . 1.362(9) ?
  C61 C66 . 1.399(9) ?
  C62 C63 . 1.410(10)
  ?
  C63 C64 . 1.36(2) ?
  C64 C65 . 1.35(2) ?
  C65 C66 . 1.360(10)
  ?
  C71 C72 . 1.371(9) ?
  C71 C76 . 1.410(9) ?
  C72 C73 . 1.380(10)
  ?
  C73 C74 . 1.40(2) ?
  C74 C75 . 1.35(2) ?
  C75 C76 . 1.400(10)
  ?
  C81 C82 . 1.372(9) ?
  C81 C86 . 1.380(10)
  ?
  C82 C83 . 1.390(10)
  ?
  C83 C84 . 1.34(2) ?
  C84 C85 . 1.37(2) ?
  C85 C86 . 1.400(10)
  ?
_cod_database_code 2010373