#------------------------------------------------------------------------------
#$Date: 2008-11-20 19:58:43 +0000 (Thu, 20 Nov 2008) $
#$Revision: 481 $
#$URL: svn://www.crystallography.net/cod/cif/2/2010376.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2010376
_journal_name_full 'Acta Crystallographica Section C'
_journal_year  1995
_journal_volume 51
_journal_page_first  40
_journal_page_last  42
_publ_section_title
;
trans-Dichlorotetrakis(pyridine)ruthenium(II)
;
loop_
_publ_author_name
  'Elsegood, M.R.J.'
  'Tocher, D.A.'
_chemical_formula_sum  'C20 H20 Cl2 N4 Ru1'
_chemical_formula_weight  488.4
_symmetry_cell_setting  tetragonal
_symmetry_space_group_name_H-M  'I 41/a c d'
_symmetry_space_group_name_Hall  'I -4 2aw -bw'
_cell_length_a  15.664(2)
_cell_length_b  15.664(2)
_cell_length_c  16.970(2)
_cell_angle_alpha  90
_cell_angle_beta  90
_cell_angle_gamma  90
_cell_volume  4164.0(10)
_cell_formula_units_Z  8
_cell_measurement_temperature  293
_exptl_crystal_density_diffrn  1.56
_refine_ls_R_factor_obs  0.0453
_refine_ls_wR_factor_obs  0.0320
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
  Ru(1) .0 .2500 .1250 0.0290(10)
  Cl(1) .10860(10)
  .14140(10)
  .1250 0.0450(10)
  N(1) .0668(2) .3155(2) .0386(2) 0.0340(10)
  C(1) .1042(3) .2752(3) -.0221(3) 0.043(2)
  C(2) .1487(3) .3173(3) -.0798(3) 0.055(2)
  C(3) .1566(4) .4040(4) -.0771(3) 0.059(2)
  C(4) .1188(3) .4466(3) -.0154(3) 0.0500(10)
  C(5) .0749(3) .4016(3) .0402(3) 0.0400(10)
  H(1) .099(3)  .214(3)  -.024(2)  0.051(12)
  H(2) .174(3)  .285(3)  -.123(3)  0.060(13)
  H(3) .180(3)  .432(3)  -.114(3)  0.079(15)
  H(4) .122(3)  .508(3)  -.013(3)  0.073(16)
  H(5) .049(2)  .428(3)  .077(2)  0.037(12)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_publ_flag
  Ru(1) Cl(1) 2.4060(10)
  yes
  N(1) C(1) 1.341(5) yes
  C(1) C(2) 1.371(6) yes
  C(2) C(3) 1.365(7) yes
  C(3) C(4) 1.375(7) yes
  C(4) C(5) 1.365(6) yes
  C(5) H(5) 0.85(4)  yes
  Ru(1) N(1) 2.073(3) yes
  N(1) C(5) 1.355(5) yes
  C(1) H(1) 0.97(4)  yes
  C(2) H(2) 0.97(4)  yes
  C(3) H(3) 0.84(5)  yes
  C(4) H(4) 0.96(5)  yes