data_2010429
_journal_name_full  'Acta Crystallographica'
_journal_year  1995
_journal_volume  C51
_journal_page_first  313
_journal_page_last  315
_publ_section_title
;
2,4,7,9-Tetra-tert-butyl-1,3,7,9-decatetraene
;
loop_
_publ_author_name
  'Overby, J.S.'
  'Hanusa, T.P.'
_chemical_formula_moiety  'C26 H46'
_chemical_formula_sum  'C26 H46'
_chemical_formula_weight  358.65
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 21/n'
_symmetry_space_group_name_Hall  '-P 2yn'
loop_
_symmetry_equiv_pos_as_xyz
  'x,y,z'
  '1/2+x,1/2-y,1/2+z'
  '-x,-y,-z'
  '1/2-x,1/2+y,1/2-z'
_cell_length_a  9.559(2)
_cell_length_b  12.464(2)
_cell_length_c  10.478(2)
_cell_angle_alpha  90.
_cell_angle_beta  94.370(10)
_cell_angle_gamma  90.
_cell_volume  1244.7(3)
_cell_formula_units_Z  2
_cell_measurement_temperature  293.0(10)
_exptl_crystal_density_diffrn  0.957
_refine_ls_R_factor_obs  0.044
_refine_ls_wR_factor_obs  0.050
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
  C(1) .0688(4) .2622(3) .9057(4)
  C(2) .0727(4) .1914(3) .8127(4)
  C(3) -.0500(4) .1218(3) .7789(3)
  C(4) -.1148(3) .0522(3) .8493(3)
  C(5) -.0685(3) .0294(3) .9904(3)
  C(6) .1934(4) .1840(3) .7264(4)
  C(7) .1471(5) .2352(4) .5972(4)
  C(8) .3250(5) .2413(4) .7812(5)
  C(9) .2331(4) .0679(4) .7049(4)
  C(10) -.2425(4) -.0106(3) .7938(3)
  C(11) -.3678(5) .0111(4) .8723(5)
  C(12) -.2889(4) .0195(4) .6572(4)
  C(13) -.2112(5) -.1298(4) .7972(5)
  H(1) -.0130 .2686 .9514
  H(2) .1477 .3067 .9272
  H(3) -.0084 .1281 .6929
  H(4) -.0596 .0959 1.0345
  H(5) -.1389 -.0128 1.0255
  H(6) .1285 .3093 .6092
  H(7) .2196 .2275 .5407
  H(8) .0645 .2007 .5617
  H(9) .3580 .2082 .8594
  H(10) .3953 .2369 .7220
  H(11) .3038 .3144 .7962
  H(12) .1529 .0294 .6711
  H(13) .3040 .0648 .6463
  H(14) .2672 .0368 .7840
  H(15) -.3919 .0850 .8664
  H(16) -.4454 -.0310 .8400
  H(17) -.3439 -.0071 .9593
  H(18) -.3148 .0931 .6537
  H(19) -.2139 .0076 .6044
  H(20) -.3670 -.0234 .6279
  H(21) -.2932 -.1685 .7683
  H(22) -.1382 -.1450 .7432
  H(23) -.1825 -.1507 .8825
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
  C(1) C(2) . . 1.318(5) yes
  C(2) C(3) . . 1.479(5) yes
  C(2) C(6) . . 1.523(5) yes
  C(3) C(4) . . 1.323(4) yes
  C(4) C(5) . . 1.537(5) yes
  C(4) C(10) . . 1.528(5) yes
  C(5) C(5) . 3_557 1.500(6) yes
  C(6) C(7) . . 1.531(5) yes
  C(6) C(8) . . 1.520(5) yes
  C(6) C(9) . . 1.516(5) yes
  C(10) C(11) . . 1.528(5) yes
  C(10) C(12) . . 1.512(5) yes
  C(10) C(13) . . 1.515(5) yes