Crystallography Open Database

Information card for entry 2010529

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Structure parameters

Chemical name	trans-[hydrotetrakis(trimethylphosphine)Rhodiumchloride/bromide] [(tetrabromobenzene-1,2-diolato)borate] dichloromethane solvate
Formula	C25 H39 B Br8.27 Cl2.73 O4 P4 Rh
Calculated formula	C25 H39 B Br8.26 Cl2.74 O4 P4 Rh
Title of publication	Compositional disorder in <i>trans</i>-[RhBr~0.26~Cl~0.74~H(PMe~3~)~4~][B(1,2-O~2~C~6~Br~4~)]·CH~2~Cl~2~
Authors of publication	Norman, Nicholas C.; Orpen, A. Guy; Quayle, Michael J.; Robins, Edward G.
Journal of publication	Acta Crystallographica Section C
Year of publication	2000
Journal volume	56
Journal issue	1
Pages of publication	50 - 52
a	13.014 ± 0.0009 Å
b	16.399 ± 0.0015 Å
c	20.726 ± 0.003 Å
α	90 ± 0.008°
β	90 ± 0.01°
γ	90 ± 0.009°
Cell volume	4423.3 ± 0.8 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	8
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0703
Residual factor for significantly intense reflections	0.0486
Weighted residual factors for all reflections	0.1184
Weighted residual factors for all reflections included in the refinement	0.1126
Goodness-of-fit parameter for all reflections	1.031
Goodness-of-fit parameter for all reflections included in the refinement	1.154
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

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