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Information card for entry 2010668
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| Coordinates | 2010668.cif |
|---|---|
| Structure factors | 2010668.hkl |
| Original IUCr paper | HTML |
| Chemical name | Dimethyl[1,3-bis(diphenylphosphino)propane]palladium(II) hemitoluene |
|---|---|
| Formula | C32.5 H36 P2 Pd |
| Calculated formula | C32.5 H36 P2 Pd |
| Title of publication | An alkyl‒palladium(II) complex with a bidentate phosphine ligand: [1,3-bis(diphenylphosphino)propane-<i>P</i>,<i>P</i>']dimethylpalladium(II) toluene hemisolvate |
| Authors of publication | Abu-Surrah, Adnan S.; Debaerdemaeker, Tony; Huhn, Wolfgang; Rieger, Bernhard; Klinga, Martti; Repo, Timo; Leskelä, Markku |
| Journal of publication | Acta Crystallographica Section C |
| Year of publication | 2000 |
| Journal volume | 56 |
| Journal issue | 2 |
| Pages of publication | e42 - e43 |
| a | 12.26 ± 0.003 Å |
| b | 15.025 ± 0.002 Å |
| c | 16.347 ± 0.003 Å |
| α | 90° |
| β | 99 ± 0.02° |
| γ | 90° |
| Cell volume | 2974.2 ± 1 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.03 |
| Residual factor for significantly intense reflections | 0.023 |
| Weighted residual factors for all reflections included in the refinement | 0.062 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.036 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
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