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Information card for entry 2011109
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| Coordinates | 2011109.cif |
|---|---|
| Structure factors | 2011109.hkl |
| Original IUCr paper | HTML |
| Chemical name | cis(6,13-dimethyl-1,4,8,11-tetraazacyclotetradecan-6,13-diamine)nickel(II) perchlorate |
|---|---|
| Formula | C12 H30 Cl2 N6 Ni O8 |
| Calculated formula | C12 H30 Cl2 N6 Ni O8 |
| Title of publication | Ni^II^ and Zn^II^ complexes of the hexadentate macrocyclic ligand <i>cis</i>-6,13-dimethyl-1,4,8,11-tetraazacyclotetradecane-6,13-diamine |
| Authors of publication | Bernhardt, Paul V. |
| Journal of publication | Acta Crystallographica Section C |
| Year of publication | 2000 |
| Journal volume | 56 |
| Journal issue | 7 |
| Pages of publication | 744 - 746 |
| a | 9.198 ± 0.004 Å |
| b | 12.771 ± 0.001 Å |
| c | 9.88 ± 0.005 Å |
| α | 90° |
| β | 113.09 ± 0.02° |
| γ | 90° |
| Cell volume | 1067.6 ± 0.7 Å3 |
| Cell temperature | 295 ± 2 K |
| Ambient diffraction temperature | 295 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.046 |
| Residual factor for significantly intense reflections | 0.0436 |
| Weighted residual factors for all reflections included in the refinement | 0.1173 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.084 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
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