#------------------------------------------------------------------------------ #$Date: 2011-09-28 15:24:46 +0100 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: svn://www.crystallography.net/cod/hkl/2/01/11/2011147.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011147_Fobs loop_ _publ_author_name 'Harvey, Miguel' 'Baggio, Sergio' 'Mombr\'u, Alvaro' 'Baggio, Ricardo' _publ_section_title ; Three new Zn^II^ sulfate complexes ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 771 _journal_page_last 774 _journal_volume 56 _journal_year 2000 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 103.738 _cell_angle_beta 99.385 _cell_angle_gamma 113.357 _cell_length_a 8.8044 _cell_length_b 10.4281 _cell_length_c 8.7719 _exptl_crystal_F_000 376.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file na1468IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_refln_list_code 4 _shelx_f_calc_maximum 163.87 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 54.55 58.54 4.80 o 2 0 0 798.67 795.24 54.74 o 3 0 0 1520.24 1415.87 31.73 o 4 0 0 520.66 506.02 13.60 o 5 0 0 17.59 20.38 1.27 o 6 0 0 702.66 684.21 18.85 o 7 0 0 591.93 598.82 17.75 o 8 0 0 10.88 13.99 1.35 o 9 0 0 404.52 409.64 14.89 o 10 0 0 62.93 67.33 4.02 o -10 1 0 255.24 271.06 11.83 o -9 1 0 167.84 168.84 8.69 o -8 1 0 82.69 87.25 5.77 o -7 1 0 142.62 146.75 7.05 o -6 1 0 180.80 185.54 7.53 o -5 1 0 175.00 175.82 6.66 o -4 1 0 1624.70 1540.57 34.79 o -3 1 0 6337.80 5926.78 123.99 o -2 1 0 27.24 32.54 1.18 o -1 1 0 12494.58 13995.36 619.94 o 0 1 0 5.79 7.77 0.58 o 1 1 0 249.39 271.89 24.74 o 2 1 0 309.84 351.84 23.56 o 3 1 0 1381.15 1271.96 29.05 o 4 1 0 1799.77 1770.96 40.17 o 5 1 0 418.44 425.60 12.74 o 6 1 0 2220.40 2301.08 52.72 o 7 1 0 325.10 337.25 12.11 o 8 1 0 77.78 81.70 5.31 o 9 1 0 72.37 71.37 4.06 o -10 2 0 12.82 13.76 1.63 o -9 2 0 485.31 507.66 16.86 o -8 2 0 83.65 86.57 5.55 o -7 2 0 425.38 394.17 12.83 o -6 2 0 1540.10 1499.25 35.38 o -5 2 0 46.41 48.98 2.99 o -4 2 0 1672.94 1662.60 36.42 o -3 2 0 3037.58 3228.08 68.17 o -2 2 0 1061.95 1246.39 20.92 o -1 2 0 340.08 292.84 8.32 o 0 2 0 569.07 448.35 15.67 o 1 2 0 514.75 426.51 22.75 o 2 2 0 211.68 204.15 14.56 o 3 2 0 2403.52 2218.63 48.99 o 4 2 0 202.01 206.61 7.43 o 5 2 0 1242.29 1295.22 31.41 o 6 2 0 712.65 778.81 21.31 o 7 2 0 142.73 139.90 7.26 o 8 2 0 182.27 184.57 8.89 o 9 2 0 53.45 58.76 3.88 o -10 3 0 379.45 333.79 13.37 o -9 3 0 7.70 8.71 1.25 o -8 3 0 7.63 8.62 1.05 o -7 3 0 2063.25 1941.62 44.69 o -6 3 0 546.80 568.69 14.95 o -5 3 0 278.55 333.11 9.47 o -4 3 0 7.93 12.93 0.82 o -3 3 0 1232.32 1278.19 28.63 o -2 3 0 455.75 456.26 27.60 o -1 3 0 1571.16 1334.08 29.20 o 0 3 0 1720.69 1419.73 52.28 o 1 3 0 502.58 462.83 41.53 o 2 3 0 849.29 707.78 39.20 o 3 3 0 1439.32 1356.79 31.65 o 4 3 0 76.49 75.98 4.19 o 5 3 0 655.27 658.53 18.39 o 6 3 0 27.45 23.70 1.62 o 7 3 0 398.24 431.91 14.53 o 8 3 0 71.93 68.80 3.93 o -11 4 0 36.18 32.68 2.25 o -10 4 0 342.18 282.63 11.62 o -9 4 0 27.41 25.67 1.63 o -8 4 0 479.51 486.24 14.35 o -7 4 0 461.06 482.53 13.67 o -6 4 0 291.75 296.49 9.38 o -5 4 0 412.81 543.96 14.50 o -4 4 0 987.37 1021.87 24.12 o -3 4 0 2250.78 2154.39 47.06 o -2 4 0 19.49 38.56 1.60 o -1 4 0 3758.85 3311.02 49.94 o 0 4 0 799.96 673.91 11.69 o 1 4 0 345.48 293.07 17.55 o 2 4 0 761.37 687.95 17.86 o 3 4 0 1.17 0.38 1.47 o 4 4 0 142.65 152.17 6.62 o 5 4 0 95.86 107.39 5.83 o 6 4 0 444.12 459.79 15.06 o 7 4 0 0.79 4.10 1.04 o 8 4 0 235.94 252.44 11.10 o -11 5 0 208.30 186.68 8.86 o -10 5 0 103.30 101.39 6.09 o -9 5 0 39.33 34.79 2.36 o -8 5 0 235.83 229.33 8.81 o -7 5 0 113.30 119.28 5.69 o -6 5 0 331.67 311.07 10.15 o -5 5 0 373.48 383.16 11.36 o -4 5 0 3312.53 3301.66 71.38 o -3 5 0 360.19 338.27 9.77 o -2 5 0 7814.08 8376.61 365.82 o -1 5 0 197.18 133.13 3.61 o 0 5 0 61.89 61.86 2.55 o 1 5 0 173.62 162.95 7.66 o 2 5 0 147.86 151.58 5.48 o 3 5 0 553.18 520.84 15.14 o 4 5 0 0.95 1.80 1.58 o 5 5 0 832.08 860.96 23.64 o 6 5 0 226.81 236.17 10.00 o 7 5 0 13.62 13.44 1.38 o -11 6 0 64.95 49.57 3.21 o -10 6 0 17.22 16.16 1.31 o -9 6 0 154.37 157.15 7.56 o -8 6 0 91.21 91.44 5.47 o -7 6 0 968.57 1080.50 27.49 o -6 6 0 0.76 -0.60 1.39 o -5 6 0 1870.53 1839.10 42.07 o -4 6 0 788.05 726.93 18.62 o -3 6 0 575.92 562.15 14.93 o -2 6 0 412.41 335.97 15.71 o -1 6 0 4.31 2.76 0.54 o 0 6 0 56.26 53.57 2.35 o 1 6 0 363.45 338.21 12.02 o 2 6 0 4330.99 4177.21 155.80 o 3 6 0 102.47 92.94 5.32 o 4 6 0 553.14 559.05 16.99 o 5 6 0 454.80 478.88 15.59 o 6 6 0 15.96 23.85 1.79 o -11 7 0 108.54 99.25 6.35 o -10 7 0 133.24 139.46 7.66 o -9 7 0 0.30 2.10 1.14 o -8 7 0 786.55 768.08 21.62 o -7 7 0 406.09 433.30 13.76 o -6 7 0 349.61 340.65 11.32 o -5 7 0 1090.49 1050.52 26.09 o -4 7 0 4.16 5.19 0.69 o -3 7 0 243.01 227.26 8.06 o -2 7 0 258.52 229.09 5.75 o -1 7 0 1213.48 1169.39 29.89 o 0 7 0 4.92 6.29 0.60 o 1 7 0 1972.23 1819.93 30.16 o 2 7 0 393.67 378.06 21.44 o 3 7 0 3.66 2.43 1.74 o 4 7 0 135.11 126.90 6.78 o 5 7 0 96.76 122.11 6.85 o -11 8 0 137.48 127.75 7.91 o -10 8 0 87.26 77.16 4.18 o -9 8 0 212.83 189.85 9.03 o -8 8 0 153.68 143.88 7.28 o -7 8 0 186.34 202.72 8.72 o -6 8 0 11.86 10.62 1.07 o -5 8 0 372.09 372.40 11.96 o -4 8 0 547.90 546.73 15.62 o -3 8 0 5.01 8.57 0.89 o -2 8 0 1361.85 1320.46 28.56 o -1 8 0 1137.07 1120.46 25.61 o 0 8 0 1.98 1.09 1.26 o 1 8 0 577.16 546.08 11.66 o 2 8 0 4.16 3.40 0.86 o 3 8 0 97.06 94.84 5.87 o 4 8 0 62.90 70.75 3.77 o -10 9 0 2.31 2.22 1.83 o -9 9 0 9.04 8.37 1.28 o -8 9 0 134.43 146.03 7.53 o -7 9 0 240.44 240.29 9.72 o -6 9 0 1.22 1.64 1.12 o -5 9 0 1266.50 1251.25 31.19 o -4 9 0 327.70 308.56 10.81 o -3 9 0 11.03 15.77 1.28 o -2 9 0 633.83 616.46 12.60 o -1 9 0 0.88 1.38 0.73 o 0 9 0 128.57 135.70 9.29 o 1 9 0 28.23 31.51 3.04 o 2 9 0 378.09 362.37 9.24 o 3 9 0 16.80 17.31 1.62 o -10 10 0 34.13 37.68 2.30 o -9 10 0 19.30 21.69 1.78 o -8 10 0 217.09 241.08 10.16 o -7 10 0 151.07 156.13 7.88 o -6 10 0 518.12 552.65 16.98 o -5 10 0 418.59 427.54 13.88 o -4 10 0 54.54 46.17 2.78 o -3 10 0 50.44 43.87 2.76 o -2 10 0 56.61 52.73 2.19 o -1 10 0 185.91 190.52 13.43 o 0 10 0 0.10 -0.33 1.20 o 1 10 0 570.97 553.20 23.97 o 2 10 0 222.15 224.98 7.13 o -9 11 0 302.49 276.16 11.53 o -8 11 0 82.69 73.70 4.18 o -7 11 0 36.48 40.23 2.37 o -6 11 0 134.13 139.52 7.40 o -5 11 0 6.13 4.67 1.06 o -4 11 0 196.86 196.43 8.72 o -3 11 0 76.90 74.76 3.80 o -2 11 0 359.75 354.34 8.99 o -1 11 0 50.20 50.96 2.60 o 0 11 0 458.73 505.88 11.76 o 1 11 0 98.01 101.69 4.68 o -8 12 0 10.11 9.54 1.20 o -7 12 0 81.15 84.51 5.74 o -6 12 0 43.06 38.90 2.35 o -5 12 0 236.40 221.65 9.91 o -4 12 0 0.16 3.56 1.78 o -3 12 0 252.11 220.77 9.86 o -2 12 0 84.41 88.16 5.09 o -1 12 0 43.12 46.61 3.19 o -6 13 0 139.85 140.64 7.88 o -5 13 0 98.91 115.62 7.00 o -4 13 0 111.24 107.08 6.90 o 3 -13 1 310.73 313.52 12.59 o 4 -13 1 114.68 122.35 7.12 o 5 -13 1 2.00 1.38 1.89 o 6 -13 1 53.03 52.10 3.57 o 7 -13 1 24.34 24.14 2.06 o 0 -12 1 177.94 178.89 6.35 o 1 -12 1 30.44 27.53 1.31 o 2 -12 1 108.19 113.22 4.72 o 3 -12 1 129.58 107.56 6.62 o 4 -12 1 0.86 -1.60 1.88 o 5 -12 1 40.16 39.41 2.46 o 6 -12 1 26.19 27.56 1.86 o 7 -12 1 267.47 264.75 10.90 o 8 -12 1 0.21 2.17 1.79 o -1 -11 1 107.39 98.96 4.74 o 0 -11 1 253.85 258.19 7.58 o 1 -11 1 34.69 32.98 3.16 o 2 -11 1 139.10 136.56 4.98 o 3 -11 1 90.51 81.52 5.28 o 4 -11 1 106.74 114.39 6.46 o 5 -11 1 53.25 52.41 3.38 o 6 -11 1 460.31 447.28 14.86 o 7 -11 1 61.68 59.41 3.56 o 8 -11 1 142.74 154.22 8.10 o 9 -11 1 153.35 130.86 7.86 o -3 -10 1 31.88 37.58 2.52 o -2 -10 1 92.61 91.29 4.34 o -1 -10 1 141.09 143.32 5.37 o 0 -10 1 107.94 113.98 4.63 o 1 -10 1 124.29 129.46 8.99 o 2 -10 1 541.59 508.16 15.08 o 3 -10 1 118.37 139.74 6.83 o 4 -10 1 0.32 2.22 1.23 o 5 -10 1 640.38 654.01 18.88 o 6 -10 1 291.85 285.19 10.93 o 7 -10 1 48.13 43.01 2.97 o 8 -10 1 101.01 102.20 6.39 o 9 -10 1 7.85 1.78 2.34 o 10 -10 1 9.96 6.97 1.22 o -4 -9 1 149.79 156.97 8.49 o -3 -9 1 65.63 62.61 3.68 o -2 -9 1 3.12 3.28 0.66 o -1 -9 1 224.94 236.81 6.79 o 0 -9 1 709.54 736.71 21.82 o 1 -9 1 59.69 48.09 2.04 o 2 -9 1 537.60 559.32 41.66 o 3 -9 1 533.11 476.48 14.48 o 4 -9 1 119.92 114.38 5.78 o 5 -9 1 402.90 382.57 12.58 o 6 -9 1 90.07 92.01 5.47 o 7 -9 1 30.29 32.41 1.96 o 8 -9 1 129.29 126.63 6.70 o 9 -9 1 218.27 204.95 8.99 o 10 -9 1 0.21 -0.86 1.53 o -5 -8 1 56.49 55.77 3.54 o -4 -8 1 123.88 121.86 6.85 o -3 -8 1 139.69 138.66 7.21 o -2 -8 1 341.55 329.66 8.23 o -1 -8 1 1897.81 1847.28 30.96 o 0 -8 1 564.32 538.42 11.21 o 1 -8 1 668.14 596.41 11.92 o 2 -8 1 740.02 618.68 44.50 o 3 -8 1 2.11 1.15 1.17 o 4 -8 1 320.18 302.72 10.19 o 5 -8 1 658.65 645.47 17.87 o 6 -8 1 191.15 190.90 7.84 o 7 -8 1 69.47 69.03 4.49 o 8 -8 1 558.15 576.88 17.06 o 9 -8 1 76.62 81.73 5.39 o 10 -8 1 12.69 7.58 1.07 o -6 -7 1 63.84 66.92 3.82 o -5 -7 1 253.49 248.49 10.39 o -4 -7 1 613.49 624.32 18.79 o -3 -7 1 15.69 17.59 1.36 o -2 -7 1 171.37 165.35 5.37 o -1 -7 1 1049.85 957.98 17.37 o 0 -7 1 37.83 31.40 1.46 o 1 -7 1 129.78 127.18 4.04 o 2 -7 1 427.34 439.64 35.81 o 3 -7 1 548.46 500.49 14.01 o 4 -7 1 229.58 212.51 7.65 o 5 -7 1 3438.65 3556.14 77.38 o 6 -7 1 1057.38 1111.59 27.20 o 7 -7 1 57.25 65.76 4.18 o 8 -7 1 263.06 282.46 10.16 o 9 -7 1 2.80 4.29 0.93 o 10 -7 1 93.19 87.93 5.81 o 11 -7 1 9.92 8.99 1.10 o -6 -6 1 3.37 5.13 1.00 o -5 -6 1 492.24 537.10 16.79 o -4 -6 1 80.12 81.72 5.16 o -3 -6 1 578.04 535.52 15.83 o -2 -6 1 1796.60 1684.25 47.40 o -1 -6 1 9.83 14.05 0.72 o 0 -6 1 190.41 178.89 4.72 o 1 -6 1 49.03 30.63 1.24 o 2 -6 1 3017.79 2795.78 187.38 o 3 -6 1 756.93 649.03 16.50 o 4 -6 1 1325.67 1250.81 29.04 o 5 -6 1 1672.25 1707.98 38.75 o 6 -6 1 36.03 39.88 2.18 o 7 -6 1 160.33 181.34 7.21 o 8 -6 1 76.85 73.47 4.47 o 9 -6 1 349.83 354.16 12.13 o 10 -6 1 5.38 6.85 1.07 o 11 -6 1 197.25 200.31 9.10 o -7 -5 1 145.96 150.80 7.95 o -6 -5 1 85.83 84.80 5.34 o -5 -5 1 46.80 46.81 2.82 o -4 -5 1 10.12 12.33 1.15 o -3 -5 1 1367.23 1324.05 31.86 o -2 -5 1 967.73 919.17 16.22 o -1 -5 1 2229.81 2092.73 33.02 o 0 -5 1 515.20 525.57 12.67 o 1 -5 1 3719.40 3629.96 161.51 o 2 -5 1 1986.63 1855.51 141.70 o 3 -5 1 22.73 32.89 2.14 o 4 -5 1 937.70 1002.25 23.43 o 5 -5 1 41.37 53.44 3.04 o 6 -5 1 425.08 454.67 12.68 o 7 -5 1 84.07 89.45 4.67 o 8 -5 1 602.41 639.17 17.87 o 9 -5 1 134.55 136.34 6.59 o 10 -5 1 278.79 285.67 10.99 o 11 -5 1 231.99 216.61 9.79 o -8 -4 1 135.57 133.15 7.71 o -7 -4 1 18.28 20.62 1.60 o -6 -4 1 48.18 53.88 3.11 o -5 -4 1 695.15 716.25 19.93 o -4 -4 1 665.65 646.30 17.72 o -3 -4 1 76.66 80.92 4.20 o -2 -4 1 4098.28 3854.19 134.45 o -1 -4 1 403.62 297.98 8.88 o 0 -4 1 404.49 372.48 6.93 o 1 -4 1 87.14 59.69 1.89 o 2 -4 1 805.43 858.36 65.66 o 3 -4 1 633.87 700.05 16.52 o 4 -4 1 692.15 788.88 18.67 o 5 -4 1 166.31 121.31 4.84 o 6 -4 1 35.71 29.37 1.74 o 7 -4 1 667.16 709.99 18.65 o 8 -4 1 226.51 222.65 8.50 o 9 -4 1 2.35 0.25 1.67 o 10 -4 1 130.59 124.39 6.67 o -8 -3 1 47.20 46.61 2.82 o -7 -3 1 182.16 190.67 8.72 o -6 -3 1 151.33 169.68 7.55 o -5 -3 1 1543.52 1513.14 36.08 o -4 -3 1 176.57 162.73 6.50 o -3 -3 1 2262.85 2260.77 49.89 o -2 -3 1 1440.68 1383.09 58.59 o -1 -3 1 180.60 167.40 3.67 o 0 -3 1 409.34 420.13 7.22 o 1 -3 1 1544.61 1532.93 85.71 o 2 -3 1 2994.24 3251.30 166.11 o 3 -3 1 196.42 208.97 5.98 o 4 -3 1 161.76 109.71 4.16 o 5 -3 1 1455.30 1529.76 34.44 o 6 -3 1 170.72 189.38 6.83 o 7 -3 1 165.25 179.10 7.03 o 8 -3 1 494.70 500.15 14.91 o 9 -3 1 105.54 104.81 6.06 o 10 -3 1 5.84 6.19 0.99 o -9 -2 1 11.17 11.47 1.43 o -8 -2 1 386.43 390.46 13.94 o -7 -2 1 0.62 0.69 1.31 o -6 -2 1 1078.46 1008.72 25.92 o -5 -2 1 729.97 675.59 18.01 o -4 -2 1 10.94 7.79 0.71 o -3 -2 1 1425.29 1388.05 31.19 o -2 -2 1 18.40 17.61 1.33 o -1 -2 1 734.58 715.09 11.39 o 0 -2 1 3516.32 3648.08 96.49 o 1 -2 1 6126.77 6964.79 269.49 o 2 -2 1 1783.11 1936.90 29.11 o 3 -2 1 2915.68 2943.11 62.31 o 4 -2 1 3258.45 3430.31 72.89 o 5 -2 1 95.89 106.81 4.49 o 6 -2 1 331.04 345.97 10.46 o 7 -2 1 2.05 2.01 0.76 o 8 -2 1 544.48 549.08 16.38 o 9 -2 1 0.40 -0.07 2.05 o 10 -2 1 273.48 271.69 11.29 o -9 -1 1 262.55 257.29 11.04 o -8 -1 1 145.63 148.72 7.62 o -7 -1 1 106.10 110.17 5.94 o -6 -1 1 768.42 770.69 20.31 o -5 -1 1 529.59 599.45 15.82 o -4 -1 1 2999.18 2972.53 64.00 o -3 -1 1 376.17 360.13 9.40 o -2 -1 1 3193.43 3163.04 47.00 o -1 -1 1 447.51 465.54 7.43 o 0 -1 1 6408.52 7279.34 105.97 o 1 -1 1 4822.26 4945.73 185.68 o 2 -1 1 17.80 14.85 1.21 o 3 -1 1 2495.87 2578.66 54.94 o 4 -1 1 1.39 1.24 0.63 o 5 -1 1 140.83 140.93 5.52 o 6 -1 1 525.37 534.87 14.96 o 7 -1 1 2010.59 1938.20 45.29 o 8 -1 1 216.64 215.89 9.18 o 9 -1 1 153.73 147.07 8.00 o 10 -1 1 109.94 105.84 7.06 o -10 0 1 54.88 56.06 3.68 o -9 0 1 227.56 231.02 10.08 o -8 0 1 2.22 0.79 1.94 o -7 0 1 58.38 63.52 4.16 o -6 0 1 111.33 126.71 5.59 o -5 0 1 2773.11 3013.07 65.15 o -4 0 1 35.07 44.70 2.41 o -3 0 1 3551.97 3439.41 72.40 o -2 0 1 5653.36 5649.22 102.10 o -1 0 1 559.56 582.28 8.99 o 0 0 1 6506.78 6326.17 882.18 o 1 0 1 3471.96 3529.54 154.65 o 2 0 1 315.76 333.01 5.93 o 3 0 1 2.11 7.78 0.55 o 4 0 1 2311.83 2132.81 46.98 o 5 0 1 176.88 222.86 7.79 o 6 0 1 1340.38 1393.32 33.58 o 7 0 1 1144.15 1126.28 29.02 o 8 0 1 1.21 0.97 0.95 o 9 0 1 61.92 64.04 3.88 o -10 1 1 39.90 35.78 2.49 o -9 1 1 0.25 1.82 1.68 o -8 1 1 51.21 50.36 2.95 o -7 1 1 255.96 258.18 9.07 o -6 1 1 1782.99 1904.86 42.79 o -5 1 1 1530.11 1755.06 38.91 o -4 1 1 262.73 232.13 6.74 o -3 1 1 310.82 268.73 7.09 o -2 1 1 145.67 153.82 3.00 o -1 1 1 790.79 756.36 11.62 o 0 1 1 807.70 715.77 11.09 o 1 1 1 1562.23 1404.55 21.46 o 2 1 1 2530.48 2476.61 37.53 o 3 1 1 8097.80 7684.80 160.78 o 4 1 1 2354.64 2211.09 49.23 o 5 1 1 14.26 9.67 0.84 o 6 1 1 692.36 718.28 19.99 o 7 1 1 36.85 32.67 2.10 o 8 1 1 70.73 73.84 4.04 o 9 1 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155.51 5.27 o 3 -4 9 57.61 54.26 3.25 o 4 -4 9 87.81 89.97 5.91 o 5 -4 9 163.55 165.90 8.39 o -7 -3 9 93.49 85.66 5.54 o -6 -3 9 84.57 85.67 5.59 o -5 -3 9 276.17 273.97 10.58 o -4 -3 9 23.56 24.33 1.50 o -3 -3 9 343.99 368.46 12.46 o -2 -3 9 15.50 17.92 0.90 o -1 -3 9 183.33 181.49 10.04 o 0 -3 9 1.37 0.49 1.12 o 1 -3 9 330.52 314.72 28.76 o 2 -3 9 332.51 322.42 8.28 o 3 -3 9 9.67 11.05 1.19 o 4 -3 9 68.57 59.75 3.51 o -7 -2 9 20.01 18.48 1.53 o -6 -2 9 149.03 149.24 7.50 o -5 -2 9 11.39 12.22 1.13 o -4 -2 9 195.99 196.92 8.42 o -3 -2 9 22.29 24.86 1.48 o -2 -2 9 91.36 85.42 3.73 o -1 -2 9 126.98 124.44 4.53 o 0 -2 9 250.71 248.74 7.83 o 1 -2 9 131.29 128.12 4.69 o 2 -2 9 72.74 71.15 2.63 o 3 -2 9 90.67 78.12 5.26 o 4 -2 9 4.36 3.78 1.04 o -8 -1 9 0.48 0.28 1.88 o -7 -1 9 37.57 35.50 2.30 o -6 -1 9 1.73 2.65 0.81 o -5 -1 9 37.52 44.63 2.67 o -4 -1 9 12.24 13.02 1.16 o -3 -1 9 13.80 18.41 1.33 o -2 -1 9 207.88 209.29 6.14 o -1 -1 9 2.73 5.66 0.63 o 0 -1 9 5.48 8.31 1.18 o 1 -1 9 119.09 119.38 6.21 o 2 -1 9 77.22 77.90 4.08 o 3 -1 9 20.70 18.66 1.51 o -8 0 9 41.82 39.26 2.34 o -7 0 9 1.61 -0.57 1.64 o -6 0 9 182.76 174.70 8.14 o -5 0 9 176.60 167.92 7.81 o -4 0 9 3.89 4.89 1.02 o -3 0 9 188.91 189.39 8.16 o -2 0 9 35.79 36.96 1.64 o -1 0 9 7.87 6.72 1.05 o 0 0 9 120.59 124.24 4.88 o 1 0 9 41.54 45.39 3.47 o 2 0 9 66.95 64.32 2.59 o 3 0 9 54.06 52.63 3.36 o -8 1 9 10.95 12.19 1.36 o -7 1 9 183.35 163.96 8.33 o -6 1 9 116.61 126.33 6.82 o -5 1 9 11.47 11.19 1.08 o -4 1 9 65.60 68.46 4.66 o -3 1 9 0.89 -1.44 1.94 o -2 1 9 57.88 53.34 2.16 o -1 1 9 85.49 78.63 3.70 o 0 1 9 112.86 107.01 7.30 o 1 1 9 151.12 151.33 5.41 o 2 1 9 3.40 2.28 0.84 o -8 2 9 1.93 0.29 1.87 o -7 2 9 115.04 114.49 6.61 o -6 2 9 32.77 33.12 2.19 o -5 2 9 1.43 1.66 0.69 o -4 2 9 27.07 28.84 1.92 o -3 2 9 152.41 151.99 7.26 o -2 2 9 70.42 71.65 3.43 o -1 2 9 64.81 61.65 2.41 o 0 2 9 217.30 224.79 6.84 o 1 2 9 14.57 14.93 1.80 o -8 3 9 50.21 52.37 3.37 o -7 3 9 10.90 10.92 1.19 o -6 3 9 7.63 5.09 1.03 o 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