#------------------------------------------------------------------------------ #$Date: 2011-09-28 15:24:46 +0100 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: svn://www.crystallography.net/cod/hkl/2/01/11/2011148.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011148_Fobs loop_ _publ_author_name 'Harvey, Miguel' 'Baggio, Sergio' 'Mombr\'u, Alvaro' 'Baggio, Ricardo' _publ_section_title ; Three new Zn^II^ sulfate complexes ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 771 _journal_page_last 774 _journal_volume 56 _journal_year 2000 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.130 _cell_angle_gamma 90.000 _cell_length_a 15.4210 _cell_length_b 12.7010 _cell_length_c 6.6940 _exptl_crystal_F_000 720.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file na1468IIIsup4.hkl _[local]_cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_refln_list_code 4 _shelx_f_calc_maximum 384.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x, y, -z-1/2' '-x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 63831.69 54423.04 2539.85 o 4 0 0 14831.40 14054.65 670.22 o 6 0 0 862.70 748.57 51.02 o 8 0 0 3111.03 2904.52 171.05 o 10 0 0 19326.58 19188.47 939.72 o 12 0 0 10973.81 11078.55 574.85 o 14 0 0 1614.45 1667.42 116.25 o 16 0 0 931.05 1006.51 76.62 o 18 0 0 1009.53 941.62 77.07 o 1 1 0 245.71 248.47 17.04 o 3 1 0 11732.52 10603.37 506.52 o 5 1 0 847.81 926.62 68.16 o 7 1 0 2823.83 3214.87 179.25 o 9 1 0 1048.67 1003.16 71.42 o 11 1 0 1064.20 1035.90 78.70 o 13 1 0 792.11 833.11 64.58 o 15 1 0 637.99 553.70 55.38 o 17 1 0 0.87 -88.94 88.94 o 19 1 0 86.12 47.90 96.39 o 0 2 0 1231.29 1334.56 73.34 o 2 2 0 29290.91 25548.08 1201.12 o 4 2 0 21444.73 21055.45 998.42 o 6 2 0 28009.25 27456.35 1304.38 o 8 2 0 12520.25 12858.77 634.80 o 10 2 0 4222.21 4226.46 244.13 o 12 2 0 3700.55 3747.27 234.32 o 14 2 0 1994.10 1895.88 128.66 o 16 2 0 1021.83 1103.55 85.28 o 18 2 0 477.82 586.27 62.81 o 1 3 0 24488.45 20780.08 981.63 o 3 3 0 14343.77 13463.80 645.38 o 5 3 0 6954.50 7021.18 352.05 o 7 3 0 3702.38 4013.22 221.02 o 9 3 0 6458.08 6684.38 354.79 o 11 3 0 1185.91 1214.01 88.05 o 13 3 0 473.97 477.34 48.98 o 15 3 0 728.32 741.43 62.83 o 17 3 0 486.63 535.06 56.34 o 19 3 0 649.74 788.66 74.48 o 0 4 0 291.08 309.86 25.14 o 2 4 0 1948.53 2028.46 116.76 o 4 4 0 15818.45 15856.28 763.42 o 6 4 0 13800.37 14054.12 686.48 o 8 4 0 2964.12 3041.61 182.04 o 10 4 0 184.22 199.00 30.61 o 12 4 0 119.99 9.47 61.44 o 14 4 0 372.73 401.14 46.41 o 16 4 0 602.26 462.99 58.68 o 18 4 0 214.85 144.31 98.06 o 1 5 0 1085.88 860.65 64.86 o 3 5 0 14036.84 13175.60 640.28 o 5 5 0 17074.93 16480.75 800.87 o 7 5 0 9466.73 9456.56 481.39 o 9 5 0 2105.30 2339.29 157.37 o 11 5 0 81.26 66.47 62.94 o 13 5 0 1086.01 1250.22 96.97 o 15 5 0 536.17 574.46 57.63 o 17 5 0 696.07 681.06 72.15 o 0 6 0 4836.11 5052.18 264.45 o 2 6 0 2549.29 2271.23 137.04 o 4 6 0 1480.66 1556.05 107.47 o 6 6 0 592.15 592.20 46.44 o 8 6 0 361.34 381.03 35.96 o 10 6 0 8.60 45.71 53.46 o 12 6 0 60.17 -76.77 76.77 o 14 6 0 323.39 360.42 43.10 o 16 6 0 14.35 139.32 70.82 o 18 6 0 51.72 24.14 81.95 o 1 7 0 9070.50 8976.85 453.75 o 3 7 0 2835.06 2748.96 165.11 o 5 7 0 1445.80 1564.57 115.56 o 7 7 0 988.89 998.61 77.64 o 9 7 0 256.23 271.97 34.67 o 11 7 0 3047.90 3094.38 208.25 o 13 7 0 634.64 647.97 58.91 o 15 7 0 510.18 646.94 56.27 o 17 7 0 13.72 123.00 74.36 o 0 8 0 347.21 342.08 31.22 o 2 8 0 986.67 894.92 65.90 o 4 8 0 53.18 90.60 23.46 o 6 8 0 283.01 280.26 33.32 o 8 8 0 590.64 528.16 46.13 o 10 8 0 1517.63 1457.61 106.67 o 12 8 0 480.24 447.98 51.91 o 14 8 0 33.91 108.64 65.34 o 16 8 0 2.43 -15.04 102.02 o 1 9 0 13757.19 13352.13 670.35 o 3 9 0 1777.26 1897.18 136.54 o 5 9 0 561.89 608.37 46.73 o 7 9 0 213.68 320.76 37.15 o 9 9 0 1228.14 1263.51 96.61 o 11 9 0 1501.39 1515.25 117.12 o 13 9 0 395.12 356.53 50.09 o 15 9 0 25.36 62.48 95.71 o 0 10 0 2460.85 2504.72 169.25 o 2 10 0 201.38 161.99 31.29 o 4 10 0 428.12 420.46 41.68 o 6 10 0 688.41 803.63 64.04 o 8 10 0 28.56 59.70 56.01 o 10 10 0 199.16 193.64 43.62 o 12 10 0 213.49 209.51 45.20 o 14 10 0 1.32 -101.72 101.72 o 1 11 0 760.38 776.48 56.52 o 3 11 0 5004.93 5279.94 308.95 o 5 11 0 5747.55 5510.76 329.69 o 7 11 0 6163.33 6117.24 357.84 o 9 11 0 2658.52 2492.60 201.88 o 11 11 0 448.43 428.68 53.33 o 13 11 0 622.91 653.69 65.30 o 0 12 0 467.73 378.78 45.81 o 2 12 0 128.49 156.03 34.59 o 4 12 0 32.40 28.57 66.24 o 6 12 0 9.74 9.62 60.52 o 8 12 0 8.43 -96.84 96.84 o 10 12 0 96.61 141.51 74.06 o 12 12 0 82.05 85.72 94.21 o 1 13 0 3886.82 3974.88 263.44 o 3 13 0 4975.82 4481.42 297.41 o 5 13 0 4103.62 4497.22 290.27 o 7 13 0 2568.60 2466.16 167.68 o 9 13 0 1295.19 1261.42 100.58 o 11 13 0 772.49 661.23 71.40 o 0 14 0 939.46 953.80 72.25 o 2 14 0 978.43 1012.32 74.14 o 4 14 0 1768.11 1809.31 133.03 o 6 14 0 938.65 888.88 73.98 o 8 14 0 511.38 477.67 64.84 o 10 14 0 108.06 23.16 101.06 o 1 15 0 1423.82 1535.67 107.67 o 3 15 0 1775.17 1650.17 133.92 o 5 15 0 772.36 730.61 73.81 o 7 15 0 584.76 619.27 66.05 o 0 16 0 3491.97 3357.27 256.97 o 2 16 0 2001.68 1906.92 150.67 o 4 16 0 1223.16 1054.14 83.40 o -19 1 1 371.91 343.04 60.17 o -17 1 1 519.38 550.14 56.72 o -15 1 1 145.24 180.32 37.15 o -13 1 1 2016.33 2180.50 157.58 o -11 1 1 5224.14 5928.43 327.92 o -9 1 1 5962.84 5367.73 290.30 o -7 1 1 3484.40 3423.17 189.64 o -5 1 1 1579.82 1670.96 101.95 o -3 1 1 35.28 38.50 28.20 o -1 1 1 12294.22 12292.25 582.24 o 1 1 1 5826.69 5771.84 280.79 o 3 1 1 64.23 59.71 31.89 o 5 1 1 111.03 101.08 20.16 o 7 1 1 27.91 61.65 41.88 o 9 1 1 788.43 780.07 54.51 o 11 1 1 1420.42 1658.33 128.69 o 13 1 1 458.61 498.02 46.04 o 15 1 1 45.92 56.69 56.47 o 17 1 1 427.14 169.09 115.08 o -18 2 1 15.50 -87.44 87.44 o -16 2 1 18.57 131.65 79.47 o -14 2 1 432.13 443.16 44.83 o -12 2 1 52.26 -28.87 53.61 o -10 2 1 1952.21 1867.10 130.51 o -8 2 1 3208.97 3641.30 205.35 o -6 2 1 14.50 0.75 30.90 o -4 2 1 4527.41 4438.93 227.48 o -2 2 1 2890.30 3101.96 159.65 o 0 2 1 8741.39 9646.79 326.67 o 2 2 1 127.74 116.07 16.25 o 4 2 1 1193.35 1031.24 75.01 o 6 2 1 3.53 17.82 37.07 o 8 2 1 222.90 253.93 29.86 o 10 2 1 63.48 91.28 54.36 o 12 2 1 491.92 449.08 45.44 o 14 2 1 44.02 38.72 77.74 o 16 2 1 22.99 8.80 78.42 o 18 2 1 16.15 58.04 94.51 o -19 3 1 303.58 214.87 59.41 o -17 3 1 1029.82 1010.10 75.19 o -15 3 1 4157.25 4383.93 283.04 o -13 3 1 3059.39 3052.25 210.63 o -11 3 1 5808.80 5690.28 317.17 o -9 3 1 2020.26 1798.71 130.40 o -7 3 1 7605.31 7234.57 371.07 o -5 3 1 12030.08 11602.04 565.42 o -3 3 1 14700.09 15527.77 742.36 o -1 3 1 5149.84 5658.54 280.74 o 1 3 1 2093.67 2269.41 125.50 o 3 3 1 346.62 231.74 22.43 o 5 3 1 3374.54 3219.70 180.13 o 7 3 1 2516.58 2438.03 151.89 o 9 3 1 2204.00 1904.31 137.95 o 11 3 1 3262.72 3201.49 206.90 o 13 3 1 1122.66 1001.00 78.23 o 15 3 1 1977.11 1827.33 131.64 o 17 3 1 193.77 112.72 49.56 o -18 4 1 456.48 451.47 58.90 o -16 4 1 353.94 329.44 47.46 o -14 4 1 1603.62 1590.08 115.34 o -12 4 1 81.52 115.50 60.98 o -10 4 1 194.63 226.75 31.59 o -8 4 1 613.56 564.01 42.00 o -6 4 1 376.41 415.60 31.30 o -4 4 1 12475.45 13690.29 663.16 o -2 4 1 1516.58 1516.02 96.16 o 0 4 1 92.22 46.75 24.04 o 2 4 1 453.39 380.56 30.49 o 4 4 1 1366.57 1446.70 98.75 o 6 4 1 274.72 378.84 30.39 o 8 4 1 254.57 201.43 29.56 o 10 4 1 994.37 925.24 68.22 o 12 4 1 49.22 -69.85 69.85 o 14 4 1 534.34 549.42 53.19 o 16 4 1 164.34 256.72 48.50 o 18 4 1 190.81 247.25 48.88 o -19 5 1 1068.35 1069.63 91.97 o -17 5 1 1481.92 1398.65 108.89 o -15 5 1 2556.01 2675.40 205.25 o -13 5 1 2332.35 2303.35 175.70 o -11 5 1 32.71 99.10 59.77 o -9 5 1 6952.41 6770.43 365.46 o -7 5 1 8956.23 8702.08 445.07 o -5 5 1 20258.36 21396.18 1029.15 o -3 5 1 17939.37 18612.24 894.06 o -1 5 1 520.96 405.89 31.85 o 1 5 1 1448.16 1222.62 87.02 o 3 5 1 21030.93 22029.53 1055.19 o 5 5 1 9485.82 9894.34 498.02 o 7 5 1 6336.33 6480.06 345.77 o 9 5 1 1077.57 1103.50 82.01 o 11 5 1 185.77 237.94 33.47 o 13 5 1 2026.98 2009.80 138.38 o 15 5 1 1195.79 1243.23 93.13 o 17 5 1 1330.47 1386.38 110.52 o -18 6 1 132.63 -18.27 121.66 o -16 6 1 1480.96 1352.01 103.02 o -14 6 1 1680.66 1649.04 122.27 o -12 6 1 6527.88 6417.21 369.41 o -10 6 1 5610.13 5379.09 311.08 o -8 6 1 2901.83 3097.99 191.66 o -6 6 1 8281.58 8234.11 424.69 o -4 6 1 3662.66 3279.24 188.03 o -2 6 1 6345.30 6263.20 323.25 o 0 6 1 5254.02 5179.85 204.79 o 2 6 1 946.80 830.02 58.09 o 4 6 1 1009.12 792.22 59.89 o 6 6 1 4071.67 3821.49 222.40 o 8 6 1 1214.12 1114.83 84.97 o 10 6 1 4752.58 4654.37 279.32 o 12 6 1 1940.22 2030.26 139.35 o 14 6 1 782.12 762.06 68.78 o 16 6 1 683.41 599.64 66.96 o -17 7 1 150.50 171.90 47.52 o -15 7 1 138.15 252.51 40.83 o -13 7 1 226.59 174.70 45.50 o -11 7 1 4200.42 4360.65 265.35 o -9 7 1 5087.88 5356.91 308.65 o -7 7 1 2680.57 2955.88 186.74 o -5 7 1 325.41 290.15 29.94 o -3 7 1 90.17 64.52 43.09 o -1 7 1 2383.49 2283.61 142.17 o 1 7 1 3036.52 3084.52 179.86 o 3 7 1 728.23 601.77 47.58 o 5 7 1 766.49 804.92 56.91 o 7 7 1 1116.47 1276.11 89.77 o 9 7 1 2761.05 2732.24 188.23 o 11 7 1 1556.31 1469.78 110.06 o 13 7 1 52.26 68.80 87.90 o 15 7 1 163.46 157.61 43.61 o 17 7 1 42.85 -71.43 107.67 o -16 8 1 837.24 827.66 76.45 o -14 8 1 1988.03 1833.48 138.94 o -12 8 1 4860.58 4938.91 305.59 o -10 8 1 5485.67 5425.07 321.91 o -8 8 1 8870.37 8433.51 452.34 o -6 8 1 8559.69 8803.61 462.31 o -4 8 1 6263.77 6413.27 344.01 o -2 8 1 8349.65 8251.15 428.88 o 0 8 1 8710.62 8360.53 305.63 o 2 8 1 9732.50 9960.46 507.74 o 4 8 1 5658.46 5721.82 315.19 o 6 8 1 4780.76 4542.61 268.67 o 8 8 1 2392.65 2401.37 169.57 o 10 8 1 1832.36 1888.61 127.73 o 12 8 1 2438.40 2792.35 207.19 o 14 8 1 977.97 1038.32 84.07 o 16 8 1 793.91 782.83 75.77 o -15 9 1 1.28 -77.67 94.88 o -13 9 1 69.11 29.02 95.72 o -11 9 1 13.26 54.51 72.93 o -9 9 1 743.30 676.25 54.64 o -7 9 1 499.72 489.26 45.07 o -5 9 1 695.51 687.14 51.63 o -3 9 1 146.79 187.85 27.82 o -1 9 1 304.44 327.96 31.97 o 1 9 1 219.16 85.81 60.02 o 3 9 1 217.28 234.28 32.87 o 5 9 1 1051.82 1032.04 81.40 o 7 9 1 371.57 355.05 39.57 o 9 9 1 210.25 240.20 33.99 o 11 9 1 82.39 98.73 80.15 o 13 9 1 16.16 7.82 82.10 o 15 9 1 47.48 152.33 86.69 o -14 10 1 1108.30 1099.40 87.01 o -12 10 1 2376.82 2556.87 206.32 o -10 10 1 4257.21 4373.85 279.20 o -8 10 1 2769.50 2466.52 190.96 o -6 10 1 2830.27 2758.05 194.94 o -4 10 1 3232.98 3201.73 207.62 o -2 10 1 4890.89 5027.41 290.98 o 0 10 1 10996.93 11106.21 404.76 o 2 10 1 2109.68 2258.13 160.63 o 4 10 1 1560.01 1697.40 111.66 o 6 10 1 601.62 644.16 53.27 o 8 10 1 1621.67 1718.43 124.30 o 10 10 1 2533.75 2553.64 198.08 o 12 10 1 1350.03 1309.34 102.40 o 14 10 1 462.92 516.68 59.72 o -13 11 1 266.84 177.56 96.11 o -11 11 1 553.37 576.41 58.15 o -9 11 1 1582.87 1686.16 124.06 o -7 11 1 1800.18 1611.13 120.79 o -5 11 1 336.88 308.54 40.09 o -3 11 1 2384.96 2361.00 169.77 o -1 11 1 315.16 299.66 38.06 o 1 11 1 1211.54 1142.24 88.56 o 3 11 1 1473.30 1455.73 106.44 o 5 11 1 127.64 183.33 34.44 o 7 11 1 1138.97 992.20 74.76 o 9 11 1 675.04 689.13 63.65 o 11 11 1 435.85 462.37 54.76 o 13 11 1 379.99 459.85 63.25 o -12 12 1 342.56 328.14 54.75 o -10 12 1 231.18 196.13 48.51 o -8 12 1 1376.47 1179.74 94.05 o -6 12 1 1259.36 1217.00 91.03 o -4 12 1 1528.66 1390.18 109.37 o -2 12 1 597.18 696.95 53.27 o 0 12 1 351.05 327.48 28.53 o 2 12 1 615.18 556.03 56.21 o 4 12 1 345.53 403.68 46.03 o 6 12 1 1038.77 946.42 73.02 o 8 12 1 568.52 547.31 56.27 o 10 12 1 40.54 -15.34 80.07 o 12 12 1 87.54 32.48 99.48 o -11 13 1 337.71 301.29 51.29 o -9 13 1 307.40 309.63 46.63 o -7 13 1 65.15 5.19 81.35 o -5 13 1 883.28 869.54 70.44 o -3 13 1 953.55 1049.00 82.87 o -1 13 1 2514.99 2361.38 189.72 o 1 13 1 1234.88 1122.08 87.19 o 3 13 1 316.32 311.68 46.33 o 5 13 1 133.60 171.07 43.46 o 7 13 1 7.86 -54.36 81.42 o 9 13 1 330.58 258.12 55.43 o 11 13 1 210.00 154.16 115.81 o -10 14 1 22.49 54.21 70.82 o -8 14 1 161.57 177.01 46.25 o -6 14 1 379.78 267.54 48.81 o -4 14 1 549.11 579.94 60.94 o -2 14 1 9.00 -82.40 82.40 o 0 14 1 32.88 69.49 52.77 o 2 14 1 92.42 140.31 74.51 o 4 14 1 691.17 781.36 67.04 o 6 14 1 141.29 83.84 95.80 o 8 14 1 18.96 96.01 86.39 o -7 15 1 412.92 359.98 57.61 o -5 15 1 176.17 123.02 50.23 o -3 15 1 11.47 37.07 77.89 o -1 15 1 24.78 -59.02 102.25 o 1 15 1 7.03 -97.44 97.44 o 3 15 1 6.49 -58.79 86.91 o 5 15 1 182.60 23.31 103.32 o 7 15 1 147.94 127.91 102.34 o -4 16 1 3.05 -33.61 93.45 o -2 16 1 309.98 325.72 51.37 o 0 16 1 857.36 878.43 54.90 o 2 16 1 125.01 157.30 43.09 o -20 0 2 791.39 942.86 84.42 o -18 0 2 2428.77 2353.96 162.36 o -16 0 2 1083.39 1175.93 91.24 o -14 0 2 2486.04 2798.42 190.23 o -12 0 2 7599.66 7295.85 399.83 o -10 0 2 7834.59 7707.92 404.99 o -8 0 2 71.34 6.24 42.64 o -6 0 2 1905.57 1934.33 120.20 o -4 0 2 2436.90 2379.00 134.85 o -2 0 2 57446.37 62705.64 2935.28 o 0 0 2 147781.02 167487.80 5519.59 o 2 0 2 4792.13 4542.66 234.22 o 4 0 2 5007.98 4734.30 248.84 o 6 0 2 324.59 259.18 27.61 o 8 0 2 9153.81 9076.50 469.62 o 10 0 2 17917.39 17679.58 883.03 o 12 0 2 7698.76 7384.57 412.26 o 14 0 2 807.69 914.50 70.44 o 16 0 2 1050.36 1057.44 83.10 o 18 0 2 524.87 458.41 65.67 o -19 1 2 142.87 173.17 114.90 o -17 1 2 161.28 112.12 92.04 o -15 1 2 871.24 874.19 67.89 o -13 1 2 261.39 248.80 38.28 o -11 1 2 138.86 136.11 28.50 o -9 1 2 1359.71 1430.62 108.69 o -7 1 2 2347.80 2492.42 151.69 o -5 1 2 5.10 -38.42 38.42 o -3 1 2 10393.03 11096.94 537.08 o -1 1 2 4516.10 4646.59 235.75 o 1 1 2 2741.27 2690.25 146.90 o 3 1 2 365.32 275.68 25.66 o 5 1 2 1.12 -42.78 42.78 o 7 1 2 2805.60 2915.90 177.84 o 9 1 2 1150.96 1105.96 81.27 o 11 1 2 1231.39 1186.17 92.78 o 13 1 2 732.94 660.26 57.19 o 15 1 2 128.37 66.85 86.25 o 17 1 2 8.85 -0.60 98.42 o -18 2 2 541.60 703.30 63.12 o -16 2 2 1387.51 1372.57 95.64 o -14 2 2 2268.02 2363.28 173.20 o -12 2 2 3808.10 3712.74 235.04 o -10 2 2 2674.27 2637.41 171.97 o -8 2 2 7891.20 8173.39 419.83 o -6 2 2 5435.12 5512.85 287.13 o -4 2 2 3730.71 3695.54 196.97 o -2 2 2 1520.01 1245.52 81.30 o 0 2 2 148.43 99.52 12.72 o 2 2 2 13772.53 14136.64 681.68 o 4 2 2 10769.80 10801.01 532.67 o 6 2 2 16322.71 17127.26 834.40 o 8 2 2 5555.11 5866.35 319.88 o 10 2 2 3995.03 3911.59 242.14 o 12 2 2 3270.12 2788.31 201.59 o 14 2 2 2200.76 2112.69 145.10 o 16 2 2 939.63 932.15 79.77 o -19 3 2 785.35 897.35 80.21 o -17 3 2 800.80 686.58 67.72 o -15 3 2 909.17 1077.28 83.32 o -13 3 2 267.50 268.50 38.88 o -11 3 2 1735.31 1863.84 137.80 o -9 3 2 4611.57 4708.37 261.72 o -7 3 2 1866.79 1895.71 123.10 o -5 3 2 4015.69 4131.72 222.37 o -3 3 2 3999.44 3743.69 200.86 o -1 3 2 9621.29 9871.26 482.74 o 1 3 2 8631.04 8956.93 441.42 o 3 3 2 7996.17 7932.78 398.67 o 5 3 2 3206.28 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