#------------------------------------------------------------------------------ #$Date: 2011-09-28 15:24:46 +0100 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: svn://www.crystallography.net/cod/hkl/2/01/11/2011171.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011171_Fobs loop_ _publ_author_name 'Subramanian, Ramis Rao' 'Anandan, Shanmuga S.' 'Kwek, Kuan Hiang' 'Low, Kum Sang' 'Shanmuga Sundara Raj, S.' 'Fun, Hoong-Kun' 'Razak, Ibrahim Abdul' 'Hanna, John V.' 'Ng, Seik Weng' _publ_section_title ; Dicyclohexylammonium 2,4-dichlorophenoxyacetate and (2,4-dichlorophenoxyacetato-O,O')bis(triphenylphosphine-P)silver(I) ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first e292 _journal_page_last e294 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.790 _cell_angle_gamma 90.000 _cell_length_a 13.4500 _cell_length_b 25.8202 _cell_length_c 11.7071 _exptl_crystal_F_000 1736.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file qa0322IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' (2,6-Dichlorophenoxylacetato)silver-bis(triphenylphosphine) in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 480.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 608.82 579.76 54.89 o 3 0 0 11527.45 10040.08 810.76 o 4 0 0 3087.36 3327.76 212.12 o 5 0 0 157.90 120.20 22.14 o 6 0 0 9636.53 10127.65 550.14 o 7 0 0 29028.87 34154.61 1818.47 o 8 0 0 433.36 451.11 46.07 o 9 0 0 9805.28 10450.98 574.52 o 10 0 0 361.34 450.16 52.15 o 11 0 0 2523.28 2985.91 434.54 o 12 0 0 5789.24 6202.55 359.75 o 13 0 0 1474.09 1502.58 169.24 o 14 0 0 43.75 4.57 53.75 o 15 0 0 635.81 532.88 106.35 o 2 1 0 248.81 212.95 20.61 o 3 1 0 49472.41 42125.06 1577.77 o 4 1 0 3146.81 3408.92 135.12 o 5 1 0 2510.88 2679.44 151.52 o 6 1 0 4751.28 5272.67 207.09 o 7 1 0 91.21 120.30 21.14 o 8 1 0 9371.29 9615.45 372.83 o 9 1 0 115.17 189.66 22.66 o 10 1 0 3064.01 3462.00 158.29 o 11 1 0 1812.55 2169.22 165.22 o 12 1 0 191.11 284.94 36.00 o 13 1 0 15.21 55.93 32.97 o 14 1 0 18.08 -14.87 45.74 o 15 1 0 60.07 81.86 51.30 o 2 2 0 807.22 906.38 65.12 o 3 2 0 68879.98 66795.92 2885.29 o 4 2 0 1294.05 1527.21 66.19 o 5 2 0 2214.96 2557.47 126.10 o 6 2 0 657.66 772.38 40.69 o 7 2 0 1327.05 1367.91 56.49 o 8 2 0 46.22 73.77 15.18 o 9 2 0 2547.99 2610.79 101.04 o 10 2 0 35.19 60.16 22.52 o 11 2 0 183.69 195.87 30.64 o 12 2 0 1109.93 1190.67 68.95 o 13 2 0 274.10 349.20 46.04 o 14 2 0 1.78 62.89 60.61 o 15 2 0 168.98 208.04 56.58 o 1 3 0 31009.85 29378.88 1270.99 o 2 3 0 61.37 43.45 9.90 o 3 3 0 2406.78 2974.62 293.17 o 4 3 0 4530.67 4694.89 322.02 o 5 3 0 21083.87 22238.71 998.90 o 6 3 0 10459.47 12039.60 459.62 o 7 3 0 78.39 35.85 16.43 o 8 3 0 18398.16 19068.33 724.87 o 9 3 0 472.97 555.33 38.30 o 10 3 0 4617.01 4771.21 229.29 o 11 3 0 3633.25 3820.94 163.29 o 12 3 0 428.50 412.44 48.27 o 13 3 0 277.94 385.04 77.76 o 14 3 0 602.81 623.81 61.05 o 15 3 0 113.72 101.77 49.33 o 1 4 0 486.31 428.42 98.91 o 2 4 0 1510.08 1520.16 73.89 o 3 4 0 70647.34 68681.95 4005.75 o 4 4 0 5205.62 4985.33 237.13 o 5 4 0 1200.14 1326.54 59.32 o 6 4 0 6834.91 6944.62 269.38 o 7 4 0 10970.64 11527.69 441.71 o 8 4 0 93.12 121.91 31.53 o 9 4 0 4086.81 4542.67 185.78 o 10 4 0 59.25 58.60 28.55 o 11 4 0 3688.70 3704.07 199.77 o 12 4 0 1772.18 2019.18 116.33 o 13 4 0 1203.28 1301.35 113.21 o 14 4 0 409.08 480.91 55.35 o 15 4 0 316.62 295.63 62.82 o 1 5 0 3209.44 3003.73 638.66 o 2 5 0 2855.72 3215.08 146.92 o 3 5 0 3700.08 4510.88 204.00 o 4 5 0 6688.81 7171.97 328.34 o 5 5 0 3360.30 3811.18 151.65 o 6 5 0 918.28 871.93 44.18 o 7 5 0 511.73 534.28 33.58 o 8 5 0 516.34 645.19 39.95 o 9 5 0 787.44 923.61 52.29 o 10 5 0 303.85 344.17 32.97 o 11 5 0 167.46 129.99 32.46 o 12 5 0 14.99 57.22 32.96 o 13 5 0 46.86 51.11 29.83 o 14 5 0 564.59 663.52 63.36 o 15 5 0 48.44 22.26 43.31 o 0 6 0 230454.31 141459.06 8021.79 o 1 6 0 20060.65 14454.70 986.63 o 2 6 0 22421.00 23267.89 873.91 o 3 6 0 8175.71 8556.52 495.95 o 4 6 0 4139.06 4475.83 199.69 o 5 6 0 251.34 254.03 20.01 o 6 6 0 5711.44 6046.84 273.52 o 7 6 0 3327.36 3378.50 171.17 o 8 6 0 2977.24 3000.34 126.77 o 9 6 0 3674.80 3910.61 162.29 o 10 6 0 925.96 1003.76 68.37 o 11 6 0 465.02 507.32 49.41 o 12 6 0 3338.36 3396.59 173.67 o 13 6 0 615.62 630.15 57.69 o 14 6 0 3.10 -3.53 37.22 o 15 6 0 1007.95 918.49 95.90 o 1 7 0 14154.67 11598.09 454.79 o 2 7 0 16861.29 16996.63 1517.60 o 3 7 0 861.39 1019.29 51.21 o 4 7 0 5735.73 5882.91 315.39 o 5 7 0 7303.14 7408.83 347.78 o 6 7 0 659.75 716.28 44.69 o 7 7 0 782.54 811.10 65.03 o 8 7 0 12527.61 12426.57 542.05 o 9 7 0 986.52 1219.27 63.07 o 10 7 0 4722.36 5171.51 245.80 o 11 7 0 1744.63 2015.07 119.90 o 12 7 0 453.37 426.91 49.05 o 13 7 0 330.65 359.42 47.46 o 14 7 0 146.50 112.55 38.06 o 15 7 0 228.94 241.14 55.72 o 0 8 0 2876.13 3276.94 157.60 o 1 8 0 3216.61 2803.15 245.36 o 2 8 0 837.13 903.85 58.88 o 3 8 0 364.58 395.93 24.19 o 4 8 0 8827.30 8902.04 393.35 o 5 8 0 3099.72 3232.02 133.57 o 6 8 0 6274.33 6247.36 243.62 o 7 8 0 84.18 50.72 27.23 o 8 8 0 1650.45 1834.68 114.38 o 9 8 0 28.61 24.51 20.19 o 10 8 0 84.51 109.27 33.54 o 11 8 0 804.83 852.91 75.57 o 12 8 0 217.65 236.86 38.96 o 13 8 0 1.06 7.37 34.07 o 14 8 0 275.39 280.80 58.21 o 15 8 0 85.89 139.91 33.89 o 1 9 0 20826.90 22795.45 887.92 o 2 9 0 5934.45 5743.69 231.00 o 3 9 0 6.47 15.17 11.23 o 4 9 0 2815.33 2685.94 109.89 o 5 9 0 10141.42 10535.69 403.33 o 6 9 0 7713.55 8212.13 317.64 o 7 9 0 9493.10 9037.77 350.21 o 8 9 0 1643.87 1778.26 81.35 o 9 9 0 784.71 769.43 56.90 o 10 9 0 391.14 397.98 41.95 o 11 9 0 1188.42 1200.37 101.96 o 12 9 0 253.68 283.82 41.99 o 13 9 0 171.90 202.83 39.94 o 14 9 0 1374.56 1360.80 116.30 o 15 9 0 74.26 113.74 34.82 o 0 10 0 48465.95 53406.93 3996.60 o 1 10 0 7542.08 8089.35 335.86 o 2 10 0 3213.98 3311.59 122.21 o 3 10 0 6180.91 6033.21 465.41 o 4 10 0 33.79 53.23 13.18 o 5 10 0 1056.89 987.80 51.00 o 6 10 0 3655.94 3346.96 156.51 o 7 10 0 4110.71 4190.56 169.65 o 8 10 0 42.17 53.35 24.30 o 9 10 0 7133.59 6727.09 310.93 o 10 10 0 387.82 450.85 44.95 o 11 10 0 599.51 613.28 54.73 o 12 10 0 2266.54 2197.81 123.11 o 13 10 0 548.63 481.99 65.77 o 14 10 0 3.90 9.48 25.67 o 15 10 0 828.57 852.15 60.99 o 1 11 0 12696.95 12198.45 617.64 o 2 11 0 331.44 396.85 23.56 o 3 11 0 14015.72 14598.46 509.45 o 4 11 0 819.37 791.02 89.19 o 5 11 0 1295.16 1314.46 60.96 o 6 11 0 138.60 113.48 17.39 o 7 11 0 57.11 72.68 17.15 o 8 11 0 1869.34 1809.20 98.28 o 9 11 0 0.92 20.64 26.94 o 10 11 0 1182.94 1259.56 80.46 o 11 11 0 348.86 342.93 43.22 o 12 11 0 63.60 61.18 41.24 o 13 11 0 5.39 9.49 36.78 o 14 11 0 95.96 69.46 29.48 o 0 12 0 4809.17 6280.21 487.14 o 1 12 0 878.33 773.83 41.16 o 2 12 0 8180.20 8007.35 352.43 o 3 12 0 5033.62 4526.90 165.44 o 4 12 0 9486.46 9357.91 474.39 o 5 12 0 345.61 394.48 44.03 o 6 12 0 785.28 672.67 37.77 o 7 12 0 166.11 162.48 20.25 o 8 12 0 1909.30 1849.07 99.87 o 9 12 0 367.72 390.92 41.74 o 10 12 0 1394.51 1263.91 78.69 o 11 12 0 100.28 101.38 42.40 o 12 12 0 298.08 274.16 54.10 o 13 12 0 225.24 257.62 35.77 o 14 12 0 181.30 212.46 36.06 o 1 13 0 7223.72 7755.42 310.81 o 2 13 0 13025.87 13091.35 552.50 o 3 13 0 15.06 -1.57 11.14 o 4 13 0 11123.72 10681.71 431.91 o 5 13 0 4264.43 4140.99 184.20 o 6 13 0 8.92 3.43 28.59 o 7 13 0 759.19 750.82 64.28 o 8 13 0 4975.33 4874.50 283.14 o 9 13 0 1051.39 1002.24 82.18 o 10 13 0 1376.72 1239.44 98.34 o 11 13 0 969.34 930.45 116.64 o 12 13 0 129.08 146.52 30.03 o 13 13 0 666.99 675.65 50.59 o 14 13 0 895.66 890.58 71.30 o 0 14 0 10732.83 10776.53 824.48 o 1 14 0 179.54 269.46 24.03 o 2 14 0 860.89 717.77 74.93 o 3 14 0 819.03 806.17 54.47 o 4 14 0 411.28 425.47 27.44 o 5 14 0 44.57 65.24 15.55 o 6 14 0 614.43 555.05 47.41 o 7 14 0 1501.16 1451.68 66.11 o 8 14 0 1.18 51.46 45.74 o 9 14 0 2129.45 2152.63 143.59 o 10 14 0 3.17 6.74 23.39 o 11 14 0 182.08 183.59 30.48 o 12 14 0 1103.82 1052.20 61.33 o 13 14 0 186.96 223.14 33.40 o 14 14 0 53.40 90.58 30.93 o 1 15 0 2839.13 2366.44 141.97 o 2 15 0 461.83 427.82 26.91 o 3 15 0 1529.16 1645.04 68.97 o 4 15 0 448.99 448.05 29.94 o 5 15 0 318.86 300.23 24.90 o 6 15 0 391.04 384.37 34.12 o 7 15 0 1251.82 1206.32 66.47 o 8 15 0 22.26 19.44 18.81 o 9 15 0 163.91 152.96 27.59 o 10 15 0 225.13 196.31 28.80 o 11 15 0 310.75 299.81 33.82 o 12 15 0 2.01 67.99 27.05 o 13 15 0 686.38 662.28 55.62 o 0 16 0 2120.43 1764.45 155.52 o 1 16 0 2716.64 2432.64 178.96 o 2 16 0 3654.30 2829.22 243.45 o 3 16 0 6271.52 5669.85 206.93 o 4 16 0 5803.47 5246.94 195.26 o 5 16 0 618.64 567.44 33.67 o 6 16 0 94.52 152.02 24.91 o 7 16 0 80.92 135.24 26.20 o 8 16 0 262.60 209.04 32.97 o 9 16 0 2691.87 2476.76 105.80 o 10 16 0 2141.18 2083.89 127.75 o 11 16 0 219.54 196.76 30.69 o 12 16 0 1248.85 1264.77 69.87 o 13 16 0 288.87 249.88 37.31 o 1 17 0 5066.07 4437.03 253.05 o 2 17 0 331.95 248.71 23.60 o 3 17 0 350.04 373.21 31.50 o 4 17 0 1290.18 1286.26 58.31 o 5 17 0 1366.65 1142.59 103.18 o 6 17 0 159.54 166.56 26.92 o 7 17 0 2513.16 2468.21 116.11 o 8 17 0 2224.22 2318.75 112.05 o 9 17 0 549.27 575.43 48.62 o 10 17 0 12.45 47.07 22.15 o 11 17 0 133.06 148.76 29.60 o 12 17 0 196.64 217.58 33.97 o 13 17 0 437.74 379.51 43.19 o 0 18 0 472.50 452.83 65.18 o 1 18 0 53.12 63.56 25.03 o 2 18 0 144.19 135.29 24.77 o 3 18 0 249.15 267.60 25.87 o 4 18 0 533.57 497.94 33.69 o 5 18 0 140.05 178.84 26.28 o 6 18 0 143.47 149.95 26.65 o 7 18 0 16.90 43.21 24.21 o 8 18 0 13.69 27.88 22.87 o 9 18 0 0.45 0.07 27.47 o 10 18 0 156.52 144.27 33.76 o 11 18 0 211.85 262.60 35.25 o 12 18 0 0.82 -24.42 21.03 o 1 19 0 541.88 629.30 58.32 o 2 19 0 1712.73 1901.00 99.84 o 3 19 0 204.41 209.16 24.00 o 4 19 0 5355.55 4945.83 185.24 o 5 19 0 2221.51 2341.93 212.69 o 6 19 0 265.60 223.09 31.01 o 7 19 0 640.33 557.75 44.91 o 8 19 0 598.35 556.83 46.73 o 9 19 0 42.27 29.09 26.62 o 10 19 0 72.87 17.10 26.54 o 11 19 0 222.95 225.88 39.98 o 12 19 0 60.83 75.65 33.48 o 0 20 0 306.62 378.50 62.89 o 1 20 0 505.29 482.44 49.68 o 2 20 0 1101.70 1251.63 74.32 o 3 20 0 1590.94 1681.74 92.46 o 4 20 0 4726.56 4673.59 199.01 o 5 20 0 24.79 32.70 21.40 o 6 20 0 378.25 403.49 38.02 o 7 20 0 76.56 87.04 25.37 o 8 20 0 1304.84 1327.85 76.54 o 9 20 0 891.03 1055.12 68.97 o 10 20 0 154.24 169.23 35.33 o 11 20 0 69.89 29.40 30.27 o 12 20 0 598.85 597.16 56.82 o 1 21 0 7.61 20.81 26.54 o 2 21 0 48.20 52.99 25.02 o 3 21 0 119.42 127.13 29.69 o 4 21 0 174.19 181.14 30.73 o 5 21 0 146.25 129.92 27.43 o 6 21 0 225.88 325.81 42.04 o 7 21 0 113.17 109.01 27.20 o 8 21 0 51.90 45.57 25.14 o 9 21 0 148.91 148.39 31.94 o 10 21 0 22.87 14.10 26.18 o 11 21 0 7.63 -7.74 24.13 o 0 22 0 279.50 362.50 65.18 o 1 22 0 533.33 571.16 57.61 o 2 22 0 46.00 84.94 27.93 o 3 22 0 1265.93 1327.12 79.11 o 4 22 0 2041.80 2287.52 149.17 o 5 22 0 396.47 369.58 38.42 o 6 22 0 165.99 194.22 31.45 o 7 22 0 71.49 98.58 36.06 o 8 22 0 56.39 76.51 33.20 o 9 22 0 414.30 369.30 42.91 o 10 22 0 273.52 260.87 40.15 o 11 22 0 51.54 12.75 27.60 o 1 23 0 756.23 746.34 68.96 o 2 23 0 1031.51 1088.43 71.17 o 3 23 0 26.40 2.21 19.71 o 4 23 0 971.05 966.87 82.00 o 5 23 0 934.94 936.43 82.37 o 6 23 0 20.64 18.68 22.97 o 7 23 0 1811.13 1805.62 97.15 o 8 23 0 610.03 637.73 53.30 o 9 23 0 90.41 106.45 32.58 o 10 23 0 0.94 2.38 26.97 o 0 24 0 164.37 166.95 51.46 o 1 24 0 64.96 41.19 24.88 o 2 24 0 232.49 300.26 41.39 o 3 24 0 388.06 358.57 49.68 o 4 24 0 128.81 145.41 39.52 o 5 24 0 14.90 44.51 32.89 o 6 24 0 1.64 -21.98 25.00 o 7 24 0 9.74 42.86 26.83 o 8 24 0 47.19 62.82 30.16 o 9 24 0 217.05 205.90 38.49 o 1 25 0 36.23 65.35 28.21 o 2 25 0 259.24 305.66 41.52 o 3 25 0 18.65 14.19 38.88 o 4 25 0 410.01 339.78 52.04 o 5 25 0 506.11 553.20 90.91 o 6 25 0 31.12 63.95 35.33 o 7 25 0 129.92 120.22 59.46 o 8 25 0 76.55 48.96 28.51 o 9 25 0 2.59 4.48 26.48 o 0 26 0 375.35 421.96 78.90 o 1 26 0 158.83 186.91 39.47 o 2 26 0 254.26 279.36 41.10 o 3 26 0 1189.53 1386.22 108.31 o 4 26 0 686.44 718.09 80.05 o 5 26 0 0.54 -11.98 27.68 o 6 26 0 405.20 511.69 64.14 o 7 26 0 8.10 -17.42 29.79 o 8 26 0 224.03 165.22 48.50 o 1 27 0 62.90 72.19 31.84 o 2 27 0 137.97 156.71 45.09 o 3 27 0 1.62 49.17 50.31 o 4 27 0 202.19 247.34 49.96 o 5 27 0 84.67 51.66 35.45 o 6 27 0 115.69 107.49 39.97 o 7 27 0 125.80 87.32 46.56 o 0 28 0 180.97 306.46 81.19 o 1 28 0 91.64 107.95 34.11 o 2 28 0 2.30 -7.00 32.74 o 3 28 0 7.59 -3.50 34.19 o 4 28 0 51.88 50.89 37.20 o 5 28 0 18.91 16.63 35.47 o 6 28 0 111.45 136.04 46.88 o 1 29 0 301.12 295.44 55.35 o 2 29 0 212.33 194.31 49.24 o 3 29 0 21.59 68.56 42.76 o 4 29 0 215.00 285.09 53.20 o 5 29 0 274.14 253.32 54.70 o 0 30 0 144.58 157.64 49.96 o 1 30 0 32.14 51.13 42.83 o 2 30 0 33.62 -5.72 35.58 o 3 30 0 405.08 406.78 65.26 o -15 1 1 2.08 -16.07 39.52 o -14 1 1 913.86 996.48 76.71 o -13 1 1 82.01 112.11 30.71 o -12 1 1 6.87 43.95 28.37 o -11 1 1 3126.90 3316.93 220.22 o -10 1 1 2959.09 2977.43 129.15 o -9 1 1 14.87 36.33 20.17 o -8 1 1 7981.77 8837.18 343.84 o -7 1 1 10558.68 10804.54 608.55 o -6 1 1 1041.34 1197.69 56.11 o -5 1 1 4766.44 5139.34 201.10 o -4 1 1 44021.28 44373.51 1661.05 o -3 1 1 8184.42 7562.79 537.74 o -2 1 1 1815.46 1616.49 162.41 o 2 1 1 4670.06 4014.82 145.41 o 3 1 1 69.05 36.19 12.24 o 4 1 1 6039.68 6984.39 242.12 o 5 1 1 5004.12 5273.10 201.64 o 6 1 1 3629.20 3807.47 137.62 o 7 1 1 1305.22 1298.18 54.90 o 8 1 1 3495.58 3491.88 129.61 o 9 1 1 1092.29 1050.91 49.54 o 10 1 1 4936.31 5248.17 287.42 o 11 1 1 3416.26 4031.67 236.41 o 12 1 1 897.38 1010.81 74.40 o 13 1 1 107.30 81.80 42.17 o 14 1 1 88.32 79.72 42.83 o 15 1 1 16.01 13.72 39.52 o -15 2 1 964.50 867.69 92.72 o -14 2 1 52.10 52.96 32.85 o -13 2 1 857.35 960.30 73.25 o -12 2 1 7818.77 8029.51 321.78 o -11 2 1 1176.55 1274.88 83.64 o -10 2 1 874.18 855.06 56.03 o -9 2 1 11833.31 12057.93 488.23 o -8 2 1 863.85 968.35 50.99 o -7 2 1 6384.70 6944.88 271.59 o -6 2 1 18340.59 18657.81 705.46 o -5 2 1 3039.23 3154.67 127.14 o -4 2 1 40.89 23.79 19.48 o -3 2 1 298.51 319.60 26.91 o -2 2 1 415.26 398.03 31.86 o 1 2 1 48090.12 42575.51 3182.41 o 2 2 1 474.59 412.62 20.35 o 3 2 1 2578.69 2351.37 90.31 o 4 2 1 1860.79 2091.41 83.58 o 5 2 1 9359.14 10925.52 394.48 o 6 2 1 12494.70 12586.57 458.31 o 7 2 1 10308.18 9744.90 339.06 o 8 2 1 1671.08 1662.19 86.84 o 9 2 1 6606.48 7323.57 260.04 o 10 2 1 1081.92 1278.27 87.92 o 11 2 1 271.46 217.86 37.36 o 12 2 1 6352.06 7074.83 553.86 o 13 2 1 973.39 1151.83 103.46 o 14 2 1 110.02 86.62 48.01 o 15 2 1 505.59 552.00 77.95 o -15 3 1 0.54 30.50 41.50 o -14 3 1 25.26 60.18 33.01 o -13 3 1 10.34 26.81 30.38 o -12 3 1 241.04 351.13 51.99 o -11 3 1 2.18 37.39 33.18 o -10 3 1 1838.67 2153.80 145.41 o -9 3 1 66.99 78.39 24.59 o -8 3 1 87.41 61.28 17.38 o -7 3 1 3741.98 3922.16 158.34 o -6 3 1 1222.38 1412.01 64.06 o -5 3 1 427.54 597.34 33.14 o -4 3 1 654.15 771.79 37.86 o -3 3 1 2909.96 2980.81 186.34 o -2 3 1 9127.02 8585.57 601.78 o -1 3 1 11458.11 11501.78 785.35 o 0 3 1 925.46 687.26 61.75 o 1 3 1 2171.44 1984.66 152.01 o 2 3 1 9831.30 9237.74 331.89 o 3 3 1 46.40 37.97 9.14 o 4 3 1 5787.94 6492.49 274.93 o 5 3 1 569.56 693.03 32.16 o 6 3 1 1978.14 2197.74 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